1 bromohexane

Manufactured by Thermo Fisher Scientific

Sourced in United States

1-bromohexane is a colorless liquid organic compound with the chemical formula C6H13Br. It is commonly used as a chemical building block and intermediate in organic synthesis reactions.

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6 protocols using 1 bromohexane

Synthesis of 1-Bromohexane and 1-Vinylimidazole Derivatives

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1-Bromohexane (99%) and 1-vinylimidazole (>99%) were purchased from Alfa Assar (Alfa Aesar GmbH & Co KG, Haverhill, MA, USA). Propylene carbonate (99.7%), lithium bis(trifluoromethylsulfonyl)imide (LiTFSI, 99%) and α,α^’-azoisobutyronitrile (AIBN, 98%) were obtained from Sigma-Aldrich (Taufkirchen, Germany) and used as received. All other solvents, diethylether, acetonitrile, acetone and methanol, were HPLC grade and purchased from Sigma-Aldrich (Taufkirchen, Germany). Milli-Q+ water (high-resistance ultra-purified water, Tallinn, Estonia) was used as supplied.

Kesküla A., Peikolainen A.L., Kilmartin P.A, & Kiefer R. (2021). Solvent Effect in Imidazole-Based Poly(Ionic liquid) Membranes: Energy Storage and Sensing. Polymers, 13(20), 3466.

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Synthesis of Polymerized Acrylamide Compounds

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Acrylamide, polyAcrylamide (average MW 10,000) and trifluoroacetic acid were obtained from Acros Organics (Geel, Antwerp, Belgium). Potassium persulfate, sodium alginate and methacrylic anhydride were purchased from Sigma-Aldrich (St. Louis, MO, USA). N,N′-MethylenebisAcrylamide, 1-vinylimidazole, bromoethane, 1-bromobutane, 1-bromohexane and 1-bromooctane were gained from Alfa Aesar (Ward Hill, MA, USA). Calcium chloride and Boc-Lys-OH were obtained from Merck (Darmstadt, Germany) and Carbosynth (Compton, UK), respectively. Deionized water was used in all the experiments.

Chen C.K., Chen P.W., Wang H.J, & Yeh M.Y. (2021). Alkyl Chain Length Effects of Imidazolium Ionic Liquids on Electrical and Mechanical Performances of Polyacrylamide/Alginate-Based Hydrogels. Gels, 7(4), 164.

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Synthesis and Characterization of Surfactant-Coated Microparticles

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All chemicals were used as received. 1-bromopentane (99%) (Alfa Aesar); 1-bromohexane (99%) (Alfa Aesar); 1-bromoheptane (>98%) (Toyoko Chemical Industry); 1-bromooctane (>98%) (Toyoko Chemical Industry); 1-bromononane (99%) (Alfa Aesar); 1-bromodecane (>98%) (Toyoko Chemical Industry); 1bromododecane (>98%) (Alfa Aesar); 1-iodohexadecane (>98%, stabilized with copper) (Alfa Aesar); Tergitol NP-9 (Sigma); Tergitol NP-12 (The Dow Chemical Company); Tergitol NP-15 (The Dow Chemical Company); Tergitol NP-30 (The Dow Chemical Company); Makon TD-12 (Stepan Company); polybead carboxylate 1.0 micron microspheres (Polysciences Inc.); 1-(ethoxy)nonafluorobutane, mixture of n-and iso-butyl (Synquest); sodium dodecyl sulfate (Sigma-Aldrich); N-(triethoxysilylpropyl)-o-polyethylene oxide urethane (95%) (Gelest); hexadecyltrimethoxysilane (>85%) (Sigma-Aldrich).

Wentworth C.M., Castonguay A.C., Moerman P.G., Meredith C.H., Balaj R.V., Cheon S.I, & Zarzar L.D. (2022). Chemically Tuning Attractive and Repulsive Interactions between Solubilizing Oil Droplets. Angewandte Chemie (International ed. in English), 61(32).

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Photopolymerization of Acrylate Coatings

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p-Coumaric acid, potassium hydroxide and Darocur (Speedcure 73) were obtained from Sigma Aldrich, city, country. 1-Bromohexane was obtained from Acros, Geel, Belgium. Oxybis(propane-1,2-diyl) diacrylate, dipropylene glycol diacrylate, trimetylpropyl triacrylate, cyclic trimethylolpropane formal acrylate and acid-based adhesion promotors were gifted by Arkema/Sartomer, Colombes, France. Mild Steel AS1020, NaCl aqueous solution, HCl aqueous solution, MiliQ water, methanol, and ethanol were used without further purification.

Udabe E., Sommers A., Forsyth M, & Mecerreyes D. (2020). Cation Effect in the Corrosion Inhibition Properties of Coumarate Ionic Liquids and Acrylic UV-Coatings. Polymers, 12(11), 2611.

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Polymer Functionalization and Characterization

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Polyvinyl alcohol (22,000 g/mol and 88% degree of hydrolysis) was purchased from MP Biomedicals LLC. Glutaraldehyde (8% by mass aqueous solution), sodium sulfate (anhydrous, 99%), tributylhexadecylphosphonium bromide (97%), sodium bicarbonate (ACS reagent, 99.7%), and triphenylphosphine (ReagentPlus, 99%) were obtained from the Sigma – Aldrich Company. Sulfuric acid (95–98%), ethyl acetate (certified ACS, 99.5%), acetonitrile (certified ACS, 99.8%), malachite green chloride (95% dye content), activated carbon (Darco G-60), heptane (Reagent grade) and hydrochloric acid (certified, 1 N) were purchased from Fisher Scientific. Water (HPLC grade) and methanol (HPLC grade, 99.9%) were obtained from JT Baker. 1-Bromohexane (99%), ethanol (OmniPur, 200 proof), and 1-hexadecyltriphenylphosphonium bromide (98% were purchased from Acros Organics, Calbiochemical, and Alfa Aesar. Sodium montmorillonite (Na-MT) was kindly donated by Southern Clay Products Inc. (now BYK Additives).

Brown K., Mendoza M., Tinsley T., Bee-DiGregorio M.Y., Bible M., Brooks J.L., Colorado M., Esenther J., Farag A., Gill R., Kalivas E.N., Lara R., Lutz A., Nazaire J., Rasines Mazo A., Rodriguez R.S., Schwabacher J.C., Zestos A.G., Hartings M.R, & Fox D.M. (2021). Polyvinyl alcohol-montmorillonite composites for water purification: Analysis of clay mineral cation exchange and composite particle synthesis. Polyhedron, 205, 115297.

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Photocurable Polymer Coatings for Corrosion Protection

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p-Coumaric acid, 2-(dimethylamino)ethyl
methacrylate, potassium hydroxide, potassium iodide, 2-bromoethyl
methacrylate, triethylamine, and Darocur (Speedcure 73) were obtained
from Sigma-Aldrich. 1-Bromohexane was obtained from Acros Organics.
Oxybis(propane-1,2-diyl) diacrylate, dipropylene glycol diacrylate,
trimethylpropyl triacrylate, cyclic trimethylolpropane formal acrylate,
and acid-based adhesion promoters were obtained from Arkema/Sartomer.
Mild steel AS1020, NaCl aqueous solution, concentrated HCl, Milli-Q
water, methanol, and ethanol were used without further purification.

Udabe E., Somers A., Forsyth M, & Mecerreyes D. (2021). Design of Polymeric Corrosion Inhibitors Based on Ionic Coumarate Groups. ACS Applied Polymer Materials, 3(4), 1739-1746.

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