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2 protocols using cetyltrimethylammonium chloride solution ctac

1

Gold Nanoparticle Synthesis with CTAB

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All chemicals and oligomers were used as received without any modification or further purification. Hexadecyltrimethylammonium bromide (CTAB, 99%), Cetyltrimethylammonium chloride solution (CTAC, 25 wt% in H2O), Potassium Iodide (KI, 99.5%), L-ascorbic acid (AA, 99%) and tetrachloroauric(III) trihydrate (HAuCl4·3H2O, 99.9%) were purchased from Sigma-Aldrich. All single-stranded oligonucleotides were synthesized and purchased from Integrated DNA Technologies, Inc. (IDT). All aqueous solutions were prepared using high-purity deionized water (18.2 MΩ cm−1).
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2

Epoxy Resin Matrix Fabrication

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Two forms of epoxy resins (diglycidyl ether of bisphenol A), EPIKOTE 828 (12 000–14 000 cps at 25 °C) and ARALDITE 506 (500–700 cps at 25 °C), were used as an epoxy matrix and as capsule core material, respectively. Diethylenetriamine (99%, DETA) as the hardener, ethanol (60%), acetone, calcium chloride (99.5%), sodium carbonate (99.5–100.5%), sodium dodecyl sulphate (SDS, 98.5%), sodium chloride (NaCl, 99.5%), and cetyltrimethylammonium chloride solution (CTAC, 25%) were purchased from Sigma Aldrich. All chemicals and reagents were of analytical grade and used without further purification. All solutions were prepared using distilled water.
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