Standards of anti-DP (catalog number: a-DP), 13C-labeled syn-DP (catalog number: Ms-DP), and syn-DP (catalog number: s-DP) (each at 50 mg·mL−1, >95% pure) were purchased from Wellington Laboratories (Guelph, ON, Canada). All organic solvents were obtained from J.T. Baker (Phillipsburg, NJ, USA) and were pesticide analysis grade. Ultra-pure water was produced using a Milli-Q system (EMD Millipore, Billerica, MA, USA). Analytical grade anhydrous sodium sulfate was baked at 450 °C for 5 h before use. Silica gel (100–200 mesh; Merck, Darmstadt, Germany) was activated at 105 °C for 12 h, cooled, and deactivated by adding 3% of the sorbent weight of deionized water.
Syn dp
Manufactured by Wellington Laboratories
Sourced in Canada
Syn-DP is a laboratory instrument designed for the synthesis and purification of organic compounds. It provides precise control over reaction parameters, ensuring consistent and reliable results.
Automatically generated - may contain errors
2 protocols using syn dp
1
Synthesis and Characterization of DP Standards
2
Comprehensive Analytical Protocol for Persistent Organic Pollutants
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All solvents used in this study were of HPLC grade or higher, obtained from Fisher Scientic (Loughborough, UK). Individual stock standard solutions of natives, internal standards, and recovery determination standards (PBDEs -28, 47, 99, 100, 153, 154, 183, 209, 77, 128, 13 (link) C-BDE-100, 13 (link) C-BDE-209, a-HBCDD, b-HBCDD, g-HBCDD, 13 (link) C-a-HBCDD, 13 (link) C-b-HBCDD, 13 (link) C-g-HBCDD, d 18 -g-HBCDD, DBDPE, anti-DP, syn-DP, HBBz, PBBz, PBEB, and PBT) were purchased from Wellington Laboratories (Guelph, ON, Canada). PCBs -11, 14, 28, 29, 34, 52, 62, 101, 118, 119, 129, 138, 147, 153, 173, and 180 were bought from Greyhound Chromatography (Birkenhead, Merseyside, UK). Pesticide grade orisil (60-100 mesh) and concentrated sulfuric acid, were purchased from Acros Organics (Geel, Belgium) and Sigma-Aldrich (St. Louis, MA, US) respectively.
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