Smartlab x ray diffractometerwith

Manufactured by Rigaku

Sourced in United States

The Smartlab X-ray diffractometer is a versatile laboratory instrument designed for advanced materials analysis. It utilizes X-ray diffraction technology to provide detailed structural information about a wide range of materials, including crystals, powders, and thin films. The Smartlab's core function is to accurately measure and analyze the diffraction patterns produced when a sample is exposed to X-rays, allowing users to determine the atomic and molecular structure of their materials.

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Hplc system, by Agilent Technologies (1 mentions) Digital ph meter, by Mettler Toledo (1 mentions) Ftir 8700 spectrophotometer, by Shimadzu (1 mentions)

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2 protocols using smartlab x ray diffractometerwith

Quantitative Analysis of Cyclophosphamide

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The
liquid chromatography
analysis was performed by an Agilent HPLC system equipped with an
ultraviolet–visible detector (infinity two variable), a C₁₈ reverse phase column (100 × 4.6 mm, 5.0 μm, 100
Å; NUCLEOSIL 100-5) at ambient temperature, a binary pump, and
a dual pump to separate and analyze cyclophosphamide. An Agilent 1260.0
UV–Vis diode array detector was set at 195 nm. Also, the volume
injection of the sample was 20.0 μL. A mixture solution of acetonitrile:sodium
phosphate buffer (70:30) (pH 4.0) was applied as an isocratic mobile
phase at a flow rate of 1.0 mL min^–1.
MIL-53(Al)-NH₂ was characterized by a Mira instrument (TESCAN, Czech Republic)
field emission scanning electron microscope, Perkin Elmer series spectrum
65 Fourier transform infrared (4000–400 cm^–1) spectrometer (PerkinElmer, USA), and Rigaku Smartlab X-ray diffractometer
with Cu K radiation (Rigaku, Japan) to investigate the surface morphology
and physicochemical properties of synthesized MIL-53(Al)-NH₂.
The sample and solutions were sonicated with a Tecno-Gaz
ultrasonic
bath (Parma, Italy) and homogenized with a ROTOFIX 32A centrifuge
(Westphalia, Germany) and a vortex mixer SA8 purchased from Stuart
Company (Padova, Italy). A digital pH meter (Mettler Toledo, Greifensee,
Switzerland) was supplied to adjust the acidity of urine samples.

Rahimpoor R., Firoozichahak A., Alizadeh S., Serkan H, & Nematollahi D. (2022). Application of MIL-53(Al)-NH2 as a Dispersive Microsolid-Phase Extraction Material for Determination of Cyclophosphamide in Urine by High-Performance Liquid Chromatography. ACS Omega, 7(41), 36643-36652.

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Electroanalysis of Bacterial Aptamers

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The aptamer-based electroanalysis of bacteria
was carried out at different stages by recording CV and DPV in an
Autolab PGSTAT-204 (Eco Chemie, The Netherlands. model: AUT83785),
and the results were analyzed by NOVA 1.8 software. It consists of
three-electrode systems: Ag/AgCl as a reference electrode, Pt as a
counter electrode, and FTO as a working electrode. All of the electrochemical
experiments were performed at room temperature (RT, 25 °C). UV–vis
spectroscopy (Shimadzu 2600) and scanning electron microscopy (SEM)
(Zeiss EVO 18 448) were performed to see the morphology of the nanostructures.
The analysis of Fourier transform infrared (FTIR) spectra by a Shimadzu
8700 FTIR spectrophotometer was done to identify organic, polymeric,
and, in some cases, inorganic materials. Phase identification was
carried out by X-ray diffraction using a Rigaku Smart Lab X-ray diffractometer
with Cu Kα radiation at 1.540 Å with 2θ in the range
of 10–80°.

Mishra A., Narang J., Pundir C.S., Pilloton R, & Khanuja M. (2018). Morphology-Preferable MoSe2 Nanobrooms as a Sensing Platform for Highly Selective Apta-Capturing of Salmonella Bacteria. ACS Omega, 3(10), 13020-13027.

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