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2 protocols using valeric acid

1

Characterization of Carboxylic Acids

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Formic acid, acetic acid, propionic acid, butyric acid, valeric acid, caproic acid, enanthic acid, caprylic acid, pelargonic acid and capric acid were purchased from FUJIFILM Wako Pure Chemical Corporation (Osaka, Japan) abbreviated as WAKO and Tokyo Chemical Industry Co., Ltd. (Tokyo, Japan) abbreviated as TCI. THAB and PFBB were obtained from WAKO. Sodium dihydrogen phosphate, disodium hydrogen phosphate, sodium hydroxide, perchloric acid (60 wt%, 9.2 mol/L), toluene, n-hexane and methanol were obtained from WAKO. Purified water was processed with Milli-Q water purification system (Millipore. Bedford, MA, USA). Sulfuric acid (97 wt%, 18.2 mol/L) and silver sulfate obtained from WAKO. All reagents and chemicals were of the highest grade available.
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2

Synthesis and Characterization of PVA Films

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(weight-average molecular weights (M w ) = 150,000), trifluoroacetic anhydride (TFAA), acetic acid, propionic acid, butyric acid, valeric acid, hexanoic acid, octanoic acid, decanoic acid, lauric acid, ethanol, and chloroform were purchased from Wako Pure Chemicals (Tokyo, Japan). PVA films were provided by Kuraray. All reagents are used without further purification.
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