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Boron trifluoride diethyl etherate

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Boron trifluoride diethyl etherate is a chemical compound with the formula BF3(OEt2). It is a Lewis acid used as a catalyst in organic synthesis reactions.

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Lab products found in correlation

Class gc2010 plus workstation, by Shimadzu (2 mentions) Gc 2010 plus, by Shimadzu (2 mentions) Aniline, by Thermo Fisher Scientific (1 mentions) Paraformaldehyde (pfa), by ITW Reagents (1 mentions) Acetone, by Thermo Fisher Scientific (1 mentions) Tripropylamine, by Merck Group (1 mentions) Sulfuric acid, by Thermo Fisher Scientific (1 mentions) Hydrobromic acid, by Merck Group (1 mentions) Grubbs catalyst 1st generation, by Merck Group (1 mentions) P toluenesulfonyl hydrazide, by Merck Group (1 mentions) Cdcl3, by Merck Group (1 mentions) Silica gel 60, by Macherey-Nagel (1 mentions)

Close spelling variants of this product

Boron trifluoride etherate (6 citations) Boron trifluoride (2 citations)

4 protocols using boron trifluoride diethyl etherate

1

Lipid Extraction and Fatty Acid Profiling

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Total lipids were extracted from diets and muscle of common carp with a mixture of chloroform/methanol (v/v, 2:1), followed by fatty acid methyl esters (FAME) using boron trifluoride diethyl etherate (ca. 48%, Acros Organics, Waltham, MA, USA). FAME were analysed and separated using a gas chromatograph (GC2010-plus, Shimadzu, Japan) as previously described [50 (link)]. Briefly, FAME samples were applied using on-column injection, and the oven temperature was programmed from 80 to 250 °C at a rate of 40 °C min−1 and held at 210 °C for 30 min. Individual FAME were identified through comparison with commercial standards (Sigma, St. Louis, MO,) and quantified with CLASS-GC2010-plus workstation (Shimadzu, Kyoto, Japan).
Xie D., He Z., Dong Y., Gong Z., Nie G, & Li Y. (2020). Molecular Cloning, Characterization, and Expression Regulation of Acyl-CoA Synthetase 6 Gene and Promoter in Common Carp Cyprinus carpio. International Journal of Molecular Sciences, 21(13), 4736.
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2

Benzaldehyde Condensation Synthesis

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4-Hydroxybenzaldehyde
(from
Acros), acetone (from Acros), boron trifluoride diethyl etherate (from
Alfa), aniline (from Acros), paraformaldehyde (from PanReac), and
all solvents (high-performance liquid chromatography grade) were purchased
from various commercial sources and were used without further purification.
Lin C.H., Chen Z.J., Chen C.H., Wang M.W, & Juang T.Y. (2017). Synthesis of a Bisbenzylideneacetone-Containing Benzoxazine and Its Photo- and Thermally Cured Thermoset. ACS Omega, 2(7), 3432-3440.
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3

Fatty Acid Composition Analysis

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The detection of dietary and muscle fatty acid compositions were performed according to the method described previously [17 (link)]. Briefly, total dietary and muscle lipids were extracted using a mixture of chloroform/methanol (v/v, 2:1) containing 0.01% butylated hydroxytoluene [43 (link)]. The fatty acid methyl esters (FAME) of total lipid were performed using boron trifluoride diethyl etherate (ca. 48%, Acros Organics, Waltham, MA, USA). The FAME were analyzed using gas chromatography (GC-2010 plus; Shimadzu, Kyoto, Japan), and individual FAME were identified through comparison with commercial standards (Sigma, St. Louis, MO, USA), and quantified by CLASS-GC2010-plus workstation (Shimadzu).
Yang Z., Zhu H., Huang X., Wang A, & Xie D. (2022). Molecular Characterization, Tissue Distribution Profile, and Nutritional Regulation of acsl Gene Family in Golden Pompano (Trachinotus ovatus). International Journal of Molecular Sciences, 23(12), 6437.
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4

Synthesis of Functionalized Adamantane Derivatives

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2,2′-(Adamantane-1,3-diyl)diacetic
acid (Sigma, 97%), boron trifluoride diethyl etherate (Acros, 48%
in Et2O), 4-chloro-1-butene (Acros, 98%), 9-chloro-1-nonene
(flourochem, >95%), 8-chloro-1-octene (flourochem, >95%), CDCl3 (Sigma, 99.8%), copper(II) chloride (CuCl2, Acros,
anhydrous 99%), Grubbs Catalyst 1st Generation (Sigma, 97%), HDPE
(Alfa Aesar, Mw = 125 kDa), hydrobromic
acid (Sigma, 47% in H2O), lithium aluminium hydride (Acros,
2.4 M in THF), magnesium purum, for Grignard reactions (Sigma, >99.5%),
1-phenyl-1-propyne (Acros, 99%), sulfuric acid (Fischer scientific,
>95%), THF anhydrous (Sigma, >99.9% inhibitor free), p-toluenesulfonyl hydrazide (Sigma, 97%), tripropylamine
(TCI, >98%), o-xylol anhydrous (Sigma, 97%) were
used and flash column
chromatography was performed on silica gel 60 (Macherey-Nagel GmbH,
40–63 μm, 230–400 mesh).
Friebel J., Ender C.P., Mezger M., Michels J., Wagner M., Wagener K.B, & Weil T. (2019). Synthesis of Precision Poly(1,3-adamantylene alkylene)s via Acyclic Diene Metathesis Polycondensation. Macromolecules, 52(12), 4483-4491.
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