Infrared spectra of MC and its composites with HEC and GO were measured using an FTIR spectrometer (Thermo Nicolet Nexus 870) purged with dry air. The spectrometer was equipped with a liquid nitrogen-cooled MCT (mercury cadmium telluride) detector and a Golden Gate single reflection ATR sampling accessory (Specac, Ltd.) with a diamond internal reflection element. The ATR FTIR spectra were recorded with a resolution of 4 cm−1; 256 scans were averaged per spectrum. After subtraction of the spectrum of atmosphere, the baseline was corrected and an advanced ATR correction was applied using the FTIR control software OMNIC. The final spectra were normalized for better comparison.
Golden gate single reflection atr sampling accessory
Manufactured by Specac
Sourced in United Kingdom
The Golden Gate single reflection ATR sampling accessory is a versatile tool designed for Attenuated Total Reflection (ATR) spectroscopy. It provides a straightforward and efficient method for analyzing solid, liquid, and semi-solid samples without the need for complex sample preparation.
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Lab products found in correlation
2 protocols using golden gate single reflection atr sampling accessory
1
FTIR Analysis of MC Composites
2
FTIR Spectroscopic Imaging of ATR Samples
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Mid-IR spectroscopic images were collected using a Varian 680-IR spectrometer (Agilent Technologies LDA UK Limited, Stockport, UK) coupled to a variable temperature Golden Gate single reflection ATR sampling accessory (Specac, Orpington, UK) held at 37 o C. Images were collected at a spectral resolution of 8 cm -1 with 8 co-additions. It was observed that an S/N advantage can be obtained by using a large number of background scans whilst maintaining the speed advantage of having fewer sample scans. Therefore, blank ATR crystal images at a resolution of 8 cm -1 and 256 co-additions were used as a background reference for image processing.
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