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2 protocols using hexamine

1

Synthesis of Phloroglucinol-based Composites

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Phloroglucinol (M = 126.11
g/mol), 4,4′-methylenedianiline (M = 198.27
g/mol), and hexamine (M = 140.18 g/mol) were obtained
from Sigma-Adrich, India. Trifluoroacetic acid (99.5%) was purchased
from Alfa Aesar. Anhydrous N,N-dimethylformamide
(DMF) was obtained from Spectrochem, India, and was used without further
purification. All other organic substrates and hydrochloric acid (analytical
grade) were procured from E-Merck, India.
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2

Polyphenol Quantification and Antioxidant Assays

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Procyanidin B1, procyanidin B2 and procyanidin C1 were acquired from Chromadex (Irvine, California, USA). (+)-catechin, (−)-epicatechin, quercetin glucoside, phloridzin, chlorogenic acid, horseradish peroxidase type I, hydrogen peroxide (H2O2), ABTS (2,2′-azinobis-(3-ethylbenzthiazoline-6-sulfonic acid), potassium persulfate, potassium chloride (KCl), cupric sulfate pentahydrate (CuSO4.5H2O), hexamine, murexide, phloroglucinol, sodium carbonate, ascorbic acid, acetic acid, formic acid, ethanol, acetone, and methanol were purchased from Sigma-Aldrich (St. Louis MO, USA). Acetonitrile and hydrochloric acid were acquired from J.T. Baker (Edo. de Méx., México). Deionized water (18 MΩ•cm−1) was prepared with a Milli-Q system (Millipore, Bedford, MA, USA).
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