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1 octadecene ode

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1-octadecene (ODE) is a linear alpha-olefin with the chemical formula CH₂=CH(CH₂)₁₆CH₃. It is a clear, colorless liquid at room temperature. ODE is commonly used as a raw material in various industrial applications, such as the production of lubricants, surfactants, and other specialty chemicals.

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Lab products found in correlation

Oleic acid, by Merck Group (25 mentions) Oleylamine, by Merck Group (12 mentions) Oleic acid oa, by Merck Group (7 mentions) Toluene, by Merck Group (5 mentions) Ethanol, by Merck Group (4 mentions) Cyclohexane, by Merck Group (4 mentions) Cesium carbonate cs2co3, by Merck Group (3 mentions) Sodium hydroxide (naoh), by Merck Group (3 mentions) Methanol, by Sinopharm (3 mentions) Cadmium oxide, by Merck Group (3 mentions) Sulfur powder, by Merck Group (3 mentions) Oleic acid oac, by Merck Group (3 mentions) Oleylamine oam, by Merck Group (3 mentions) Methanol, by Merck Group (3 mentions) Hydrochloric acid (hcl), by Merck Group (3 mentions) Oleylamine ola, by Merck Group (3 mentions) Trioctylphosphine top, by Merck Group (3 mentions) Hexane, by Merck Group (3 mentions) Cs2co3, by Merck Group (2 mentions) Myristic acid, by Merck Group (2 mentions)

Close spelling variants of this product

1-octadecene (1-ODE, (3 citations) 1-octadecene (ODE; C18H36, (2 citations) Octadecene (ODE) (9 citations) 1-ODE (5 citations) 1-octadecene (431 citations) Octadecene (101 citations)

54 protocols using 1 octadecene ode

1

Synthesis of CsPbBr3 Perovskite Nanocrystals

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Cesium carbonate (Cs2CO3, Sigma-Aldrich, St. Louis, MO, USA, 99%), lead bromide (PbBr2, Alfa Aesar, Haverhill, MA, USA, 99.9%), oleic acid (OA, Sigma-Aldrich, 90%), 1- octadecene (ODE, Sigma-Aldrich, 90%), oleylamine (OAM, Acros Organics, Waltham, MA, USA, 80–90%), parylene type C (Specialty Coating Systems, Indianapolis, IN, USA) and silane A174 (Sigma-Aldrich) were used as received from commercial sources.
Colloidal solutions of perovskite CsPbBr3 NCs were prepared following the hot-injection method reported by Kovalenko et al., with minor modifications [15 (link)].
Pinheiro A., Ruivo A., Rocha J., Ferro M., Pinto J.V., Deuermeier J., Mateus T., Santa A., Mendes M.J., Martins R., Gago S., Laia C.A, & Águas H. (2023). Parylene-Sealed Perovskite Nanocrystals Down-Shifting Layer for Luminescent Spectral Matching in Thin Film Photovoltaics. Nanomaterials, 13(1), 210.
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2

Synthesis of Cesium Lead Bromide Nanocrystals

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All chemicals were used as received without further purification. Cesium carbonate (Cs2CO3, 99.9%, Sigma-Aldrich), oleic acid (OA, 90%, Sigma-Aldrich), 1-octadecene (ODE, 90%, Sigma-Aldrich), PbBr2 (99.9%, Maclin), MnBr2 (99.9%, Maclin), and oleylamine (OAm, 70%, Sigma-Aldrich).
Jiang M.C, & Pan C.Y. (2022). Research on the stability of luminescence of CsPbBr3 and Mn:CsPbBr3 PQDs in polar solution. RSC Advances, 12(24), 15420-15426.
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3

Synthesis of Cs-oleate Precursor

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A 1.3-g Cs2CO3 (Thermo Fisher Scientific, United States) was loaded into a 50-ml three-neck round-bottom flask with 4 ml of oleic acid (OA; Thermo Fisher Scientific, USA) and 16 ml of 1-octadecene (ODE; Sigma-Aldrich, USA). The system was then degassed for 10 min and dried under vigorous stirring and vacuum conditions for 1 hour at 120°C. Afterward, the mixture was heated to 150°C under nitrogen atmosphere until all Cs2CO3 reacted and the solution became clear. Cs-oleate precursor must be heated to 120°C before use because it precipitates at room temperature.
Chen C., Wang Z., Wu J., Deng Z., Zhang T., Zhu Z., Jin Y., Lew B., Srivastava I., Liang Z., Nie S, & Gruev V. (2023). Bioinspired, vertically stacked, and perovskite nanocrystal–enhanced CMOS imaging sensors for resolving UV spectral signatures. Science Advances, 9(44), eadk3860.
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4

Synthesis and Characterization of Quantum Dots

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Copper (I) acetate (97 %), zinc acetate (99 %), oleic acid (90 %), oleylamine (70 %), 1-octadecene (ODE, 90 %), poly(maleic anhydride-alt-1-octadecene) (PMAO) (average Mn 30,000–50,000 as a powder), 3-(dimethylamino)-1-propylamine (DMAPA) (99 %), methyl iodide (99 %), poly-D-lysine, and gelatin were purchased from Sigma-Aldrich. Indium (III) acetate (99.99 %) and 1-dodecanethiol (DDT, 98 %) were purchased from Alfa Aesar. RPMI-1640 and MEM media were from Corning Cellgro. Heat-inactivated fetal bovine serum(FBS) was from Gibco. Fluorescein diacetate/propidium iodide (FDA/PI) was from Invitrogen. Dulbecco’s phosphate-buffered saline (DPBS) was from Fisher Scientific. U-87 MG and HEK-293 cells were ordered from ATCC. Chemicals were used as received without further purification.
The ultraviolet and visible (UV–Vis) spectra of QDs in organic solvents and aqueous solutions were obtained with a UV–Vis spectrometer (UV-2450 from Shimadzu) using cuvettes with a path length of 1 cm. Photoluminescence spectra were acquired using a spectrophotometer (RF-5301PC from Shimadzu). Infrared (IR) spectra of polymers and QDs were collected using a FT-IR spectrometer (Perkin-Elmer Frontier) equipped with attenuated total reflectance and measurement software (Spectrum 10). Particle size measurements of QDs were made using a ZetaPALS dynamic light scattering detector (Brookhaven Instruments Corp.).
Huang L., Liao M., Chen S., Demillo V.G., Dupre S.A., Zhu X., Publicover N.G, & Hunter KW J.r. (2014). A polymer encapsulation approach to prepare zwitterion-like, biocompatible quantum dots with wide pH and ionic stability. Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 16(8), 2555.
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5

Synthesis and Characterization of Copper-based Nanoparticles

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Copper chloride (CuCl, 98%, Sigma-Aldrich),
oleylamine (OLAM, 80%, Sigma-Aldrich), 1-octadecene (ODE, 90%, Sigma-Aldrich),
sulfur powder (S, 99.99%, Alfa Aesar), octanedithiol (ODT, 98%, Sigma-Aldrich),
Indium-doped Tin Oxide substrates (ITO, ∼25 nm film thickness, Rsq ≤ 120 Ω/cm2, PGO
Germany), lithium perchlorate (LiClO4, 99.99%, Sigma-Aldrich),
tetraoctylammonium tetrafluoroborate ((TOA)BF4, >98%,
Sigma-Aldrich),
tetrabutylammonium perchlorate ((TBA)ClO4, >98%, Sigma-Aldrich),
tetramethylammonium hexafluorophosphate ((TMA)PF6, >98%,
Sigma-Aldrich), cesium perchlorate (CsClO4, 99.995%, Sigma-Aldrich),
copper(I) tetrafluoroborate (CuBF4, >98%, Sigma-Aldrich),
ferrocene (Fc, 98%, Sigma-Aldrich). Anhydrous solvents (methanol,
99.8%, butanol, 99.8%, toluene, 99.8%, tetrachloroethylene (TCE, >99%)
and acetonitrile, 99.99%) were all purchased from Sigma-Aldrich. acetonitrile
was dried before use in an Innovative Technology PureSolv Micro column.
All other chemicals were used as received.
van der Stam W., Gudjonsdottir S., Evers W.H, & Houtepen A.J. (2017). Switching between Plasmonic and Fluorescent Copper Sulfide Nanocrystals. Journal of the American Chemical Society, 139(37), 13208-13217.
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6

Synthesis of Luminescent Lanthanide Nanoparticles

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Lu(Ac)3·xH2O (99.9%), Gd(Ac)3·xH2O (99.9%), Tb(Ac)3·xH2O (99.9%), Dy(Ac)3·xH2O (99.9%), Sm(Ac)3·xH2O (99.9%), Pr(Ac)3·xH2O (99.9%), Ce(Ac)3·xH2O (99.9%), Yb(Ac)3·xH2O (99.9%), Tm(Ac)3·xH2O (99.9%), Ho(Ac)3·xH2O (99.9%), Er(NO3)3·5H2O (99.9%), Yb(NO3)3·5H2O (99.9%), NH4F (98%), NaOH (≥96%), 1-Octadecene (ODE, 90%), Oleic acid (OA, 90%) and Hafnium (IV) acetylacetonate (97%) were supplied by Sigma Aldrich Company. Cyclohexane, methanol, and absolute ethanol were purchased from Sinopharm Chemical Reagent Company. Toluene was provided by the Hangzhou Gaojing Fine Chemical Industry Co., Ltd. Polymethyl methacrylate (PMMA) was purchased from Cool Chemical Technology (Beijing) Co., Ltd. All chemicals were of analytical grade and used as received without further purification.
Lei L., Wang Y., Xu W., Ye R., Hua Y., Deng D., Chen L., Prasad P.N, & Xu S. (2022). Manipulation of time-dependent multicolour evolution of X-ray excited afterglow in lanthanide-doped fluoride nanoparticles. Nature Communications, 13, 5739.
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7

Synthesis of Rare-Earth Nanocrystals

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RE(CH3COO)3·xH2O (RE: Y, Yb, Er, Nd) (99.9% metals basis), RECl3·6H2O (99.9%), oleic acid (90%), 1-octadecene (ODE, 90%), NaOH, NH4F, sodium oleate (NaOA), acetic acid, acetic anhydride, methanol, ethanol, acetone, and cyclohexane were purchased from Sigma-Aldrich. All the chemicals were of analytical grade and were used without further purification.
Feng Y., Li Z., Li Q., Yuan J., Tu L., Ning L, & Zhang H. (2021). Internal OH− induced cascade quenching of upconversion luminescence in NaYF4:Yb/Er nanocrystals. Light, Science & Applications, 10, 105.
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8

Synthesis of Nanocrystalline Materials

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Cadmium acetate dihydrate (Sigma-Aldrich,
98%), myristic acid (Sigma-Aldrich, 98%), selenium (Se, Sigma-Aldrich,
99.99%), tellurium (Te, SigmaAldrich, 99.99%), copper chloride dihydrate
(ACS reagent, 99.8%), zinc acetate trihydrate (Zn(CH3COO)2·2H2O, Sigma-Aldrich, 98%), sodium borohydride
(NaBH4, Sigma-Aldrich, 96%), trioctylphosphine (TOP, Sigma-Aldrich,
technical grade, 90%), 1-octadecene (ODE, Sigma-Aldrich, technical
grade, 90%), oleylamine (technical grade, 70%), sulfur (S, Sigma-Aldrich,
<99.5%), oleic acid (technical grade, Sigma-Aldrich, 90%), cadmium
oxide (Sigma-Aldrich, 99.9%), and lead oxide (Alfa Aesar, 99.9%).
Hexane (AR grade, 99%), 1,4-butanediol (90%, AR), dextrose (95% anhydrous,
AR), HCl (99%), and HNO3 (98%) were purchased from SD Fine
Chemicals. All chemicals were used without further purification.
Mahadevu R, & Pandey A. (2018). Thermodynamic Model for Quantum Dot Assemblies Formed Because of Charge Transfer. ACS Omega, 3(1), 266-272.
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9

Synthesis and Characterization of DNA-Encapsulated Quantum Dots

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The unlabeled and modified, labeled oligonucleotides (HPLC-purified and lyophilized) were obtained from IBA GmbH. N-cyano imidazole (NCI) was synthesized in-house according to previous protocols30 (link). 1-octadecene (ODE, Sigma), oleylamine (Sigma), oleic acid (Sigma), trioctylphosphine (TOP, Cytec), cadmium oxide (Sigma), selenium pellets (Sigma), sulfur powder (Sigma) and tetradecylphosphonic acid (TDPA, PCI synthesis) were purchased from the indicated suppliers. Methods for DNA icosahedron construction and characterization have been previously described30 (link). CdSe/CdS/ZnS QDs were synthesized according to previously published protocols21 (link). The detailed procedures for synthesis, characterization and encapsulation of QDs within DNA icosahedron are provided in the supplementary information. The experiments on cells were carried out using QDs provided by Nexdot (www.nexdot.fr).
Bhatia D., Arumugam S., Nasilowski M., Joshi H., Wunder C., Chambon V., Prakash V., Grazon C., Nadal B., Maiti P.K., Johannes L., Dubertret B, & Krishnan Y. (2016). Quantum dot-loaded monofunctionalized DNA Icosahedra for single particle tracking of endocytic pathways. Nature nanotechnology, 11(12), 1112-1119.
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10

Synthesis of Colloidal Semiconductor Nanocrystals

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The following materials were purchased from
Merck Sigma and used as received: indium acetate (99.99%), palmitic
acid (PAH, 99%), trioctylphosphine (TOP, 97%), anhydrous acetone (99.8%),
octylamine (99%), anhydrous hexadecane (99%), zinc chloride (ZnCl2, 99.999%), tributylphosphine (TBP, 97%), and triethylamine
(99.5%). Tris(trimethylsilyl)phosphine (TMSP, 98%, Strem; caution: TMSP is a highly pyrophoric substance that can release toxic
phosphine gas upon reaction with air), anhydrous toluene
(99.8%, Alfa Aesar), benzoyl fluoride (98%, TCI), didodecylamine (97%,
TCI), and indium fluoride (InF3, 99.95%, Alfa Aesar) were
used as received. 1-Octadecene (ODE, 90%, Merck Sigma) and mesitylene
(98%, Merck Sigma) were degassed in vacuo at 100 °C and room
temperature respectively before being stored in a nitrogen-filled
glovebox.
Ubbink R.F., Almeida G., Iziyi H., du Fossé I., Verkleij R., Ganapathy S., van Eck E.R, & Houtepen A.J. (2022). A Water-Free In Situ HF Treatment for Ultrabright InP Quantum Dots. Chemistry of Materials, 34(22), 10093-10103.
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