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2 protocols using lead ii acetate trihydrate

1

Hybrid Adsorbent for Heavy Metal Removal

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Phytic acid (PA, 45 wt%) was purchased from J&K Chemical Company Ltd. (Beijing, China). Chitosan (CS) was purchased from Sigma-Aldrich (USA). Calcium chloride (CaCl2), magnesium sulfate heptahydrate (MgSO4·7H2O), lead(ii) acetate trihydrate (Pb(CH3COO)2·3H2O), barium chloride dihydrate (BaCl2·2H2O), copper(ii) chloride dihydrate (CuCl2·2H2O), ethylenediaminetetraacetic acid (EDTA), sodium hydroxide (NaOH) and cadmium acetate dehydrate (Cd(CH3COO)2·2H2O) and xylenol orange (XO) were all purchased from Sinopharm Chemical Reagent Co. Ltd. (Shanghai, China) and were of p.a. quality. Ultrapure water used in the experiment was prepared by a UPH-IV ultrapure water purifier (Chengdu Ultrapure Technology Co. Ltd., China) with a resistivity of 18.25 MΩ cm.
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2

Electrochemical Synthesis Protocols

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Acetaldehyde (40% water solution), sodium hydroxide, potassium hydroxide, hydrochloric acid, lead (II) acetate trihydrate (≥99.5%), glucose and anhydrous ethanol were supplied by Sinopharm Chemical Reagent Co., China. 2-Mercaptopropionic acid (98%) and titanium (IV) oxysulfate-sulfuric acid hydrate (93%) were purchased from Macklin Co., China. Nafion solution (5 wt.%) was provided by Sigma-Aldrich Co., USA. Carbon black (Vulcan XC-72) was bought from The Cabot Co., USA. All chemicals and reagents were directly used as received without further purification.
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