Wurtzite CdSe/CdZnS core/shell quantum dots and MA-PIL ligands were synthesized as described previously [20 ], PEG side-chains were incorporated using poly(ethylene glycol) methyl ether methacrylate 500 from Sigma–Aldrich. Bio-Beads S-X1 GPC medium was obtained from Bio-Rad Laboratories. Toluene-d8 (D, 99.5%) was obtained from Cambridge Isotope Laboratories. Decylamine (95%) was purchased from Sigma Aldrich. Oleylamine (80–90%) and Bis(trimethylsilyl) sulfide ((TMS)2S; 95%) were purchased from Acros Organics. Rhodamine 590 chloride (R590, MW 464.98) was obtained from Exciton. Toluene (99.5%) and Tetrahydrofuran (THF, 99%) were purchased from Mallinckrodt Chemicals. Ethanol (200 proof) was obtained from Decon Laboratories. Acetone (99.9%) was purchased from VWR. Methanol (99.9%) was purchased from Fisher Scientific. Toluene was dried with activated 4A molecular sieves. THF was dried using the Puresolv system from Innovative Technologies. Synthetic or analytical procedures under inert conditions were carried out using Schlenk line techniques or in a glovebox under N2 atmosphere. All media components were from Sigma Aldrich. 96 well plates with clear plastic bottoms and black walls were obtained from VWR. Calcein AM was obtained from Invitrogen.
Bio beads s x1 gpc medium
Manufactured by Bio-Rad
Bio-Beads S-X1 GPC medium is a styrene-divinylbenzene copolymer used for size exclusion chromatography applications. It is designed for the separation and purification of macromolecules based on their molecular size or hydrodynamic volume.
Automatically generated - may contain errors
Lab products found in correlation
Hexane, by Merck Group (2 mentions)
Toluene, by Merck Group (2 mentions)
Calcein am, by Thermo Fisher Scientific (1 mentions)
Methanol, by Thermo Fisher Scientific (1 mentions)
Acetone, by Avantor (1 mentions)
Oleylamine, by Thermo Fisher Scientific (1 mentions)
Decylamine, by Merck Group (1 mentions)
Toluene d8, by Cambridge Isotopes (1 mentions)
Tetrahydrofuran thf, by Mallinckrodt (1 mentions)
Toluene, by Mallinckrodt (1 mentions)
Zinc stearate, by Merck Group (1 mentions)
Zinc oxide, by Merck Group (1 mentions)
Oleic acid, by Merck Group (1 mentions)
Myristic acid, by Merck Group (1 mentions)
Deuterium oxide, by Merck Group (1 mentions)
1 octadecene, by Merck Group (1 mentions)
Chlorotrimethylsilane, by Merck Group (1 mentions)
Indium acetate, by Merck Group (1 mentions)
Squalane, by Merck Group (1 mentions)
Butanol, by Merck Group (1 mentions)
3 protocols using bio beads s x1 gpc medium
1
Synthesis of Quantum Dot Nanoparticles
2
Synthesis of Colloidal Nanocrystals
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Indium acetate (In(Ac)3, 99.99%), indium chloride (InCl3, 98%), myristic acid (HMA) (≥99%), oleic acid (OA) (≥99%), octadecylphosphonic acid (ODPA) (97%), chlorotrimethylsilane (TMS-Cl) (≥98%), zinc stearate (Zn(SA)2) (technical grade), zinc oxide (99.99%), toluene (99.5%), hexanes (98.5%), 1-octadecene (ODE, 90%), squalane (≥95%), toluene-d8 (99 atom % D), deuterium oxide (99.9 atom % D), hydrochloric acid aqueous solution (35.0%), and phosphoric acid aqueous solution (85.0%) were purchased from Aldrich. Tris(trimethylsilyl)phosphine ((TMS)3P) (95%) was purchased from SK chemicals. Bio-Beads S-X1 GPC medium was purchased from Bio-Rad Laboratories, Inc. All chemicals were used without further purification.
3
Synthesis of Indium-based Nanostructures
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Indium(III) acetate (InOAc,
UNIAM, 99.99%), oleic acid (OA, UNIAM, 99%), 1-octadecene (ODE, UNIAM,
99.99%), dioctylamine (DOA, Aldrich, 97%), tris(trimethylsilyl)arsine
((TMS)3As, JSI silicon, 99%), trioctylphosphine (TOP, UNIAM),
and n-hexadecane (Alfa Aesar, 99%) were used as purchased
without any further purification. All solvents, including anhydrous
methanol, butanol, ethanol, hexane, toluene, and tetrachlorethylene
(TCE), were purchased from Sigma-Aldrich Chemical Co. Bio Beads S-X1
GPC medium was purchased from Bio-Rad Laboratories, Inc. Deuterated
toluene was purchased from DEUTERO.
UNIAM, 99.99%), oleic acid (OA, UNIAM, 99%), 1-octadecene (ODE, UNIAM,
99.99%), dioctylamine (DOA, Aldrich, 97%), tris(trimethylsilyl)arsine
((TMS)3As, JSI silicon, 99%), trioctylphosphine (TOP, UNIAM),
and n-hexadecane (Alfa Aesar, 99%) were used as purchased
without any further purification. All solvents, including anhydrous
methanol, butanol, ethanol, hexane, toluene, and tetrachlorethylene
(TCE), were purchased from Sigma-Aldrich Chemical Co. Bio Beads S-X1
GPC medium was purchased from Bio-Rad Laboratories, Inc. Deuterated
toluene was purchased from DEUTERO.
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