Tributylphosphine

Manufactured by Merck Group

Sourced in United States

Tributylphosphine is a clear, colorless liquid chemical compound. It is a phosphorus-containing compound with the chemical formula (C4H9)3P. Tributylphosphine is primarily used as a reagent in organic synthesis and as a ligand in coordination chemistry.

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Lab products found in correlation

Oleic acid, by Merck Group (6 mentions) Oleylamine, by Merck Group (4 mentions) Cadmium oxide, by Merck Group (4 mentions) Selenium, by Merck Group (4 mentions) Toluene, by Merck Group (3 mentions) Trioctylphosphine, by Merck Group (3 mentions) 1 octadecene, by Merck Group (3 mentions) Isopropanol, by Thermo Fisher Scientific (2 mentions) Trioctylphosphine oxide, by Merck Group (2 mentions) Octadecene, by Merck Group (2 mentions) Acetonitrile, by Merck Group (2 mentions) Acetone, by Merck Group (2 mentions) Dithiothreitol (dtt), by Merck Group (2 mentions) Tri n octylphosphine, by Merck Group (2 mentions) Dodecylamine, by Merck Group (1 mentions) Anhydrous hexane, by Merck Group (1 mentions) Anhydrous methanol, by Merck Group (1 mentions) Anhydrous toluene, by Merck Group (1 mentions) Zinc chloride, by Merck Group (1 mentions) Tellurium powder, by Thermo Fisher Scientific (1 mentions)

18 protocols using tributylphosphine

Synthesis of Tellurium Nanostructures

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Zinc chloride (99.999% trace metals basis), oleylamine (technical grade, 70%), dodecylamine (99%), tributylphosphine (mixture of isomers, 97%), Super-hydride® solution (1.0 M lithium triethylborohydride in THF), anhydrous hexane (95%), anhydrous toluene (99.8%), and anhydrous methanol (99.8%) were purchased from Sigma-Aldrich. Tellurium powder (∼325 mesh, 99.99% metals basis) was obtained from Alfa Aesar. CDCl₃ (D, 99.8%) was purchased from Cambridge Isotope Laboratories, Inc. All the materials were used as received without further purification.

Wang F., Zhang M., Chen W., Javaid S., Yang H., Wang S., Yang X., Zhang L.C., Buntine M.A., Li C, & Jia G. (2020). Atomically thin heavy-metal-free ZnTe nanoplatelets formed from magic-size nanoclusters. Nanoscale Advances, 2(8), 3316-3322.

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Colloidal Nanoparticle Synthesis

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Oleylamine (technical grade, 70%), tin chloride SnCl₂ (99.99%), iron chloride FeCl₂ (99.99%), nickel chloride NiCl₂ (98%), tri-butylphosphine (TBP, 93,5%), lithium-bis(trimethylsilyl)amide LiN(SiMe₃)₂ (97%), toluene (99.8%), diisobutylaluminium hydride in tetrahydrofuran (1 M DIBAH in THF), oleic acid (90%), and chloroform (99.8%) were used as purchased from Sigma Aldrich. Cobalt chloride CoCl₂ (97%) was used as purchased from Acros Organics.

Düttmann A., Bottke P., Plaggenborg T., Gutsche C., Parisi J., Knipper M, & Kolny-Olesiak J. (2019). Converting bimetallic M (M = Ni, Co, or Fe)–Sn nanoparticles into phosphides: a general strategy for the synthesis of ternary metal phosphide nanocrystals. Nanoscale Advances, 1(7), 2663-2673.

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Colloidal Synthesis of Metal Nanoparticles

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Nickel acetylacetonate (Ni(acac)₂, 95%), oleylamine (OAm, 70%), tributylphosphine (TBP, 97%), and ammonia molybdate ((NH₄)₆Mo₇O₂₄·4H₂O) were purchased from Sigma-Aldrich and used without any further purification. Benzyl ether (BE, 99%) was bought from Acros Organics and used without any further purification. Isopropanol and hexane were purchased from Fisher (ACS Certified), distilled before use and kept with molecular sieve. All experiment was conducted under standard Schlenk line condition.

Lin L., Liu J., Liu X., Gao Z., Rui N., Yao S., Zhang F., Wang M., Liu C., Han L., Yang F., Zhang S., Wen X.D., Senanayake S.D., Wu Y., Li X., Rodriguez J.A, & Ma D. (2021). Reversing sintering effect of Ni particles on γ-Mo2N via strong metal support interaction. Nature Communications, 12, 6978.

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GSK-3β Enzyme Kinetics Assay

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The chemical structure of all of the compounds used in this study is
given in Fig. 1. COB-187 was prepared as
described previously¹⁵.
Tideglusib, alsterpaullone, AR-A014418, hypothemycin, ethanethiol,
tributylphosphine, and THF were purchased from Sigma-Aldrich (St. Louis, MO).
Insect-expressed human recombinant full length histidine-tagged GSK-3β
(catalog number PR5074A) was from Life Technologies/Thermo Fisher (Waltham, MA).
The mutant version of the abovementioned GSK-3β, where the cysteine at
position 199 was replaced with an alanine (C199A), was generated by ThermoFisher
via a contract agreement. The phospho substrate (catalog number AQT0157) and ATP
(catalog number AQT 100XATP) were obtained from AssayQuant Tech (Marlboro, MA).
L-Glutathione reduced (GSH) (catalog number: G4251) and
Tris(2-carboxyethyl)phosphine hydrochlo (TCEP) (catalog number: C4706) were
purchased from Sigma-Aldrich. Dithiotheritol (DTT) (catalog number: AQT1000X
DTT) was purchased from AssayQuant Tech. The kinase reaction buffer (AssayQuant
Tech; catalog number: AQT10XRB) contained 500 mM HEPES, pH 7.5, 0.1% Brij-35,
and 100 mM MgCl₂. The enzyme dilution buffer (AssayQuant Tech;
catalog number: AQT1XEDB) contained 20 mM HEPES, pH 7.5, 0.01% Brij-35, 5%
glycerol, and 1 mg/mL bovine serum albumin.

Ghazanfari D., Noori M.S., Bergmeier S.C., Hines J.V., McCall K.D, & Goetz D.J. (2021). A novel GSK-3 inhibitor binds to GSK-3β via a reversible, time and Cys-199-dependent mechanism. Bioorganic & medicinal chemistry, 40, 116179.

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Synthesis of Colloidal Semiconductor Nanocrystals

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Cadmium oxide (CdO, >99.99%), zinc acetate dihydrate (Zn(AC)₂· 2H₂O, 99.99%), sulfur powder (S, >99.5%), selenium powder (Se, >99.99%), oleylamine (OLA, 80–90%), octadecene (ODE, 90%), oleic acid (OA, 90%), tri-octylphosphine (TOP, 90%), tri-butyl phosphine (TBP, 97%), tri-octylphosphine oxide (TOPO), octadecylphosphonic acid (ODPA, 97%), 1-octanethiol (>98.5%) and thionyl chloride (SOCl₂) were purchased from Sigma Aldrich without further purification.

Adachi M.M., Fan F., Sellan D.P., Hoogland S., Voznyy O., Houtepen A.J., Parrish K.D., Kanjanaboos P., Malen J.A, & Sargent E.H. (2015). Microsecond-sustained lasing from colloidal quantum dot solids. Nature Communications, 6, 8694.

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Thiophene-2-Boronic Acid Bromination

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N-Bromosuccinimide
(NBS,
99%), thiophene-2-boronic acid pinacol ester (98%), Pd(PPh₃)₄ (99%), K₂CO₃ (99%), NH₄SCN (97%), bromodimethylsulfonium bromide (95%), tributylphosphine
(97%), acetonitrile (99%), butyl acetate (99%), N,N-dimethylformamide (99%), and benzene-d₆ (100%, 99.6 atom % D) were supplied by Sigma-Aldrich.

Kowalik P., Bujak P., Wróbel Z., Penkala M., Kotwica K., Maroń A, & Pron A. (2020). From Red to Green Luminescence via Surface Functionalization. Effect of 2-(5-Mercaptothien-2-yl)-8-(thien-2-yl)-5-hexylthieno[3,4-c]pyrrole-4,6-dione Ligands on the Photoluminescence of Alloyed Ag–In–Zn–S Nanocrystals. Inorganic Chemistry, 59(19), 14594-14604.

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Amino Acid Substrate Preparation

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Aminomethylcoumarin (AMC)-coupled amino acid substrates were purchased from both Bachem (UK) and Peptide Institute, Inc. (Japan). Amastatin, bestatin, ethylenediaminetetraacetic acid (EDTA), tributylphosphine (TBP), insulin, heparin, substance P, bovine serum albumin (BSA), streptavidin-peroxidase and 3, 3-diaminobenzidine were purchased from Sigma (Australia). MS grade trypsin was purchased from Promega (USA). Acrylamide was purchased from Bio-Rad (USA). Pre-cast gels, buffers, molecular weight markers and all standard molecular biology reagents were purchased from Life Technologies (Australia), unless otherwise noted.

Jarocki V.M., Santos J., Tacchi J.L., Raymond B.B., Deutscher A.T., Jenkins C., Padula M.P, & Djordjevic S.P. (2015). MHJ_0461 is a multifunctional leucine aminopeptidase on the surface of Mycoplasma hyopneumoniae. Open Biology, 5(1), 140175.

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Synthesis of SnO2 NPs, ZnO NPs, and QDs

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The SnO₂ NPs dispersed in water (>99.5%) was purchased from MKnano and used as received. The synthetic procedure for ZnO nanoparticles and CdSe/CdS/CdZnS red QDs followed a reported method by Kawk et al.^{9 (link)} Precursors for synthesizing QDs and ZnO nanoparticles (zinc acetate dehydrate > 99%, tributylphosphine > 99%, 1-octadecene > 95%, trioctylphosphine > 97%, oleic acid > 99%) were purchased from Sigma-Aldrich, and potassium hydroxide (>85%) was purchased from Duksan Pharmaceutical Co. Ltd.

Park M., Song J., An M., Lim J., Lee C., Roh J, & Lee D. (2020). Colloidal quantum dot light-emitting diodes employing solution-processable tin dioxide nanoparticles in an electron transport layer. RSC Advances, 10(14), 8261-8265.

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Synthesis of Semiconductor Nanocrystals

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Zinc stearate (Zn(St)₂, purum, 10–12% Zn-based), zinc oxide (ZnO, ≥99.0%), caprylic acid (CA, ≥99.0%), 1-dodecanethiol (98%), tributylphosphine (TBP, 97%), selenium (Se, ≥99.5%), sulfur (S, purum), acetone (≥99.0%), n-hexane (≥95.0%), 1-octadecene (ODE, 90%), toluene (≥99.0%), MPA (≥99%), and MUA (95%) were acquired from Sigma Aldrich (St. Louis, MO, USA). Indium acetate (In(Ac)₃, 99.99%) and trioctylphosphine (TOP, 90%) were acquired from Alfa Aesar. Tris(trimethylsilyl)phosphine (P(TMSi)₃, 97.5%) was obtained from Vezerf Laborsynthesen GmbH (Haverhill, MA, USA). Glacial acetic acid (HOAc, ≥99.7%) was acquired from Fisher Scientific (Hampton, VA, USA). Sodium hydroxide solution (NaOH, 1 M) was purchased from Th. Geyer GmbH & Co. KG (Renningen, Germany). Ultrapure water type II (conductivity at 25 °C is 0.055 µS/cm) was obtained from a Sartorius Arium Comfort 2 (Göttingen, Germany). All the chemicals were used without further purification unless stated otherwise.

Heyne B., Arlt K., Geßner A., Richter A.F., Döblinger M., Feldmann J., Taubert A, & Wedel A. (2020). Mixed Mercaptocarboxylic Acid Shells Provide Stable Dispersions of InPZnS/ZnSe/ZnS Multishell Quantum Dots in Aqueous Media. Nanomaterials, 10(9), 1858.

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Comprehensive Proteomic Sample Preparation

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All reagents used were HPLC grade or higher. Trizma base, glycerol, Triton X-100, CHAPS, tributyl phosphine, sodium deoxycholate, α-cyano-4-hydroxy-cinnamic acid, EDTA, sodium chloride (NaCl), urea, thiourea, trifluoracetic acid (TFA), ammonium persulfate (APS) and iodoacetamide (IAA) were purchased from Sigma-Aldrich (United States). Dithiothreitol (DTT), Coomassie Blue and acrylamide/bis-acrylamide was purchased from Serva (Germany). Trypsin sequence-grade was purchased from Promega (United States). Sodium dodecyl sulfate (SDS), N,N,N',N'-tetramethylethylene-diamine (TEMED) and a molecular scale marker for gel electrophoresis were purchased from Bio-Rad (United States). Formic acid (HCOOH), ammonium bicarbonate (Ambic), methanol (MeOH), ethanol (EtOH), acetonitrile (ACN), isobutanol, hydrochloric acid (HCl), glacial acetic acid and xylene were purchased from Scharlau (Spain).

García-Vence M., Chantada-Vazquez M.D., Sosa-Fajardo A., Agra R., Barcia de la Iglesia A., Otero-Glez A., García-González M., Cameselle-Teijeiro J.M., Nuñez C., Bravo J.J, & Bravo S.B. (2021). Protein Extraction From FFPE Kidney Tissue Samples: A Review of the Literature and Characterization of Techniques. Frontiers in Medicine, 8, 657313.

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