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Ascend lh 600 mhz nmr spectrometer

Manufactured by Bruker
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Sourced in Switzerland

The Ascend LH 600 MHz NMR spectrometer is a high-resolution nuclear magnetic resonance instrument designed for analytical applications. It features a superconducting magnet that operates at 600 MHz for proton observation. The spectrometer is capable of performing various NMR experiments to analyze the chemical structure and properties of samples.

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2 protocols using ascend lh 600 mhz nmr spectrometer

1

NMR Spectroscopy of Methanol Solutions

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1H NMR (600 MHz) and 13C NMR (150 MHz) spectra were acquired with a Bruker Ascend LH 600 MHz NMR spectrometer (Bruker, Switzerland) equipped with a 5 mm CryoProbe (CP DCH 600S3 C/H-D-05 Z) in deuterated methanol solution at 298°K. Chemical shifts are given in δ (ppm), and coupling constants (J) are expressed in Hertz (Hz) (Kerkoub et al., 2018 (link)).
Kouakou K., Panda S.K., Yang M.R., Lu J.G., Jiang Z.H., Van Puyvelde L, & Luyten W. (2019). Isolation of Antimicrobial Compounds From Cnestis ferruginea Vahl ex. DC (Connaraceae) Leaves Through Bioassay-Guided Fractionation. Frontiers in Microbiology, 10, 705.
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2

NMR Spectroscopy Analysis of Metabolites

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All experiments were performed on a Bruker Ascend LH 600 MHz NMR spectrometer (Bruker, Switzerland) operating at NMR frequency of 600 MHz for 1H and 150 MHz for 13C NMR. It was equipped with a 5 mm CryoProbe (CP DCH 600S3 C/H-D-05 Z) in deuterated methanol solution at 298°K. All 1H (600 MHz) and 13C NMR (150 MHz) spectra were recorded with chemical shifts in δ (ppm) and coupling constants (J) in hertz (Hz).
Kerkoub N., Panda S.K., Yang M.R., Lu J.G., Jiang Z.H., Nasri H, & Luyten W. (2018). Bioassay-Guided Isolation of Anti-Candida Biofilm Compounds From Methanol Extracts of the Aerial Parts of Salvia officinalis (Annaba, Algeria). Frontiers in Pharmacology, 9, 1418.
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