All chemicals are commercially available and used as received. Tetraoctylammonium bromide (TOAB, 98.0%), 2-Phenylethanethiol (PhC2H4SH, 99.0%) and phenylmethanethiol (PhCH2SH, 99.0%) were purchased from Sigma-Aldrich. Tetrachloroauric(III) acid (HAuCl4·4H2O, 99.7%), sodium borohydride (NaBH4, 98.0%), acetonitrile (99.0%, AR), dichloromethane (CH2Cl2, 99.0%, AR), tetrahydrofuran (THF, 99.0%, AR), toluene (99.5%, AR), methanol (CH3OH, 99.5%, AR), and petroleum ether (AR) were purchased from Sinopharm Chemical Reagent Co., Ltd.
2 phenylethanethiol
Manufactured by Merck Group
Sourced in United Kingdom, United States
2-phenylethanethiol is a chemical compound used as a laboratory reagent. It is a colorless to pale yellow liquid with a characteristic mercaptan odor. 2-phenylethanethiol is commonly used in organic synthesis and as a precursor for other chemical compounds.
Automatically generated - may contain errors
Lab products found in correlation
Tetraoctylammonium bromide, by Merck Group (2 mentions)
Dichloromethane, by Merck Group (2 mentions)
Diethyl ether, by Merck Group (2 mentions)
Phenylmethanethiol, by Merck Group (1 mentions)
Toluene, by Sinopharm (1 mentions)
Methanol, by Sinopharm (1 mentions)
Petroleum ether, by Sinopharm (1 mentions)
Toluene, by Thermo Fisher Scientific (1 mentions)
Acetone, by Thermo Fisher Scientific (1 mentions)
Methanol, by Thermo Fisher Scientific (1 mentions)
Hydrogen tetrachloroaurate, by Thermo Fisher Scientific (1 mentions)
Ethanol, by Merck Group (1 mentions)
Sodium borohydrate, by Merck Group (1 mentions)
Sodium hydride, by Merck Group (1 mentions)
Carbon disulfide, by Merck Group (1 mentions)
Lauryl methacrylate, by Merck Group (1 mentions)
Sodium dodecyl sulfate (sds), by Avantor (1 mentions)
Benzophenone, by Merck Group (1 mentions)
Cd3od, by Merck Group (1 mentions)
N dodecane, by Merck Group (1 mentions)
5 protocols using 2 phenylethanethiol
1
Synthesis of Gold Nanoparticles with Thiol Ligands
2
Synthesis of Gold Nanoparticles with Thiolated Crown Ether
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Hydrogen tetrachloroaurate(iii ) trihydrate (ACS, Alfa Aesar, 99.99%), tetraoctylammonium bromide (Sigma-Aldrich, 98%), 2-phenylethanethiol (Sigma-Aldrich-Fluka, 99+%), sodium borohydrate (Aldrich, ≥96%), KBr (Merck, for spectroscopy), gadolinium(iii ) chloride hydrate (Sigma-Aldrich-Fluka, 99.99%), europium(iii ) chloride hexahydrate (Strem, 99.9%), acetone (Fisher, 99.7%), toluene (Fisher, 99.9%), ethanol (Sigma-Aldrich, >99.8%), methanol (Fisher, 99.9%), dichloromethane (Merck, 99.7+%) were used as received. Milli-Q water was used (18.2 MΩ cm), {N2,N11-bis(3,5-bis(trifluoromethyl)phenyl)-3,12-bis(mercaptomethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane-2,11-dicarboxamide} ligand (thiolated crown ether, abbreviated t-CE).
3
Synthesis and Characterization of Glycerol-Based Polymers
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
glycerol monomethacrylate (GMA, purity 97%) was obtained from GEO speciality chemicals (Hythe, UK) and was used as received. 2,2,2-Trifluoroethylmethacrylate (TFEMA, 99%), lauryl methacrylate (LMA, 96%), n-dodecane (>99%), glycerol (>99%), sucrose (>99.5%), Nile red, CD3OD, tetrahydrofuran (THF), dimethylformamide (DMF) (CD3)2CO, lithium bromide (LiBr), CDCl3, dimethyl sulfoxide (DMSO), triethylamine, 3,5-di-tert-4-butylhydroxytoluene (BHT), toluene, benzyl methacrylate (BzMA, 96%), 4,4′-azobis(4-cyanovaleric acid) (ACVA, >97%), benzophenone (>99%), pyrene (>99%), 2-cyanopropyldithiobenzoate (CPDB, >97%), 2-phenylethanethiol, sodium hydride (60% in mineral oil), diethyl ether, carbon disulfide, iodine, sodium thiosulfate, sodium sulfate, ethyl acetate and n-hexane were purchased from Sigma Aldrich (UK). tert-Butyl peroxy-2-ethylhexanoate (Trigonox 21S or T21s) initiator was supplied by AkzoNobel (The Netherlands) and sodium dodecylsulfate (SDS) was obtained from BDH laboratory supplies (Poole, UK). benzyl methacrylate was passed through basic alumina prior to use; all remaining reagents were used as received unless otherwise stated. Deionized water (pH 6.1 at 20 °C) was used for all experiments described herein. All solvents used were of HPLC grade.
4
Synthesis and Deposition of Metallic Nanostructures
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Silver nitrate (AgNO3) was purchased from RANKEM. Sodium borohydride (NaBH4), 2-phenylethanethiol (PET), 1,4-benzenedithiol (BDT), 2,4-dimethylbenzenethiol (DMBT), sodium citrate (Cit), ethanethiol (ET), 1-octadecanethiol (ODT), and dodecanethiol (DDT) were purchased from Sigma Aldrich Chemicals. Pure ethanol, methanol, dichloromethane, pyridine, carbon tetrachloride, acetone, diethyl ether, chloroform, acetonitrile, and N,N-dimethylformamide were sourced from Merck India and used as solvents for the electrospray deposition experiments.
5
Preparation of functionalized SAM surfaces
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
To prepare a molecularly smooth gold surface, which has a low root-mean-square roughness of <0.2 nm, gold (∼45 nm) was deposited onto freshly cleaved muscovite mica (grade #1, S&J Trading, Floral Park, NY, USA) with a uniform surface via electron beam evaporation. 22 The gold-coated mica was adhered to cylindrical disks (radius of curvature, R = 2 cm), gold side down, using an optical adhesive (NOA 81, Norland Products, NJ, USA), followed by UV curing for ∼50 min using a UV lamp (UVP B-100AP, AnalytikJena, Germany). The mica was then carefully detached to obtain the molecularly smooth and clean gold layer. 23 To deposit OH-, COOH-, C 6 H 5 -, CH 3 -, and NH 2 -functionalized SAMs onto the prepared gold surfaces, the following alkanethiol solutions (1 mM in ethanol) were prepared: 11-hydroxy-1-undecanethiol (97%), 10-carboxy-1-decanethiol (95%), 2-phenylethanethiol (98%), 1-undecanethiol (98%), and 11-amino-1undecanethiol hydrochloride (99%), respectively, purchased from Sigma-Aldrich (St Louis, MO, USA). Specifically, the prepared gold surfaces were separately immersed in each target alkanethiol solution for ∼18 h. Finally, each SAM-coated disk was weakly sonicated to remove unbound and/or loosely bound molecules, followed by drying with N 2 blowing.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!