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2 protocols using potassium permanganate

1

Peracetic Acid-based Decontamination Protocols

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Peracetic acid (15%, w/w) was purchased from Sinopharm Chemical Reagent Co. Ltd. (China). Diclofenac sodium (>99%) and fulvic acid (FA) were obtained from Aladdin (China). Methanol and acetic acid were HPLC grade. Sodium chloride (NaCl), sodium sulfate (Na2SO4), potassium nitrate (KNO3), sodium carbonate (Na2CO3), ferric chloride hexahydrate (FeCl3·6H2O), cupric sulfate pentahydrate (CuSO4·5H2O), monosodium phosphate dihydrate (NaH2PO4·2H2O), disodium hydrogen phosphate heptahydrate (Na2HPO4·7H2O), sodium hydroxide (NaOH), sulphuric acid (H2SO4), potassium iodide (KI), manganese sulfate monohydrate (MnSO4·H2O), ammonium molybdate tetrahydrate ((NH4)6Mo7O24·4H2O), soluble starch, potassium permanganate (KMnO4) and sodium hyposulfite pentahydrate (Na2S2O3·5H2O) were all analytical reagent grade and purchased from Chengdu Kelong Chemical Reagent Co. Ltd. (China). All the chemicals were used as received without further purification. Ultrapure water (18 MΩ cm) was used to prepare aqueous solutions.
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2

Graphite-based Epoxy Composite Synthesis

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Natural
flake graphite
powder (purity 99.9%) with an average particle size of 500 mesh was
supplied by Qingdao Xingyuan Graphite Co., Ltd. (Shandong, China).
Concentrated sulfuric acid (98%), sodium nitrate, potassium permanganate,
hydrogen peroxide (30%), hydrochloric acid, anhydrous ethanol, acetic
acid, and acetone all were of analytical reagent grade and purchased
from Chengdu Kelong Chemical Co., Ltd. (Chengdu, China). DOPO was
supplied by Guangdong Wengjiang Chemical Reagent Co., Ltd. (Guangdong,
China). Vinyltriethoxysilane (VTES) was kindly supplied by Qufu Chenguang
Chemical Co., Ltd. (Shandong, China). Epoxy resin (E-51, epoxy value:
0.48–0.54 mol/100 g) was purchased from Hangzhou Wuhuigang
Adhesive Co., Ltd. (Hangzhou, China). 4,4-Diamino-diphenyl methane
(DDM) was obtained from Aladdin Industrial Corporation (Shanghai,
China).
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