Dpx 300 ft nmr spectrometer

Manufactured by Bruker

Sourced in United States

The DPX 300 FT-NMR spectrometer is a compact and affordable nuclear magnetic resonance (NMR) instrument designed for routine analysis. It provides high-resolution 1H and 13C NMR spectra for the identification and characterization of organic compounds.

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Lab products found in correlation

Toledo mp90 melting point system, by Mettler Toledo (2 mentions) Lcms it tof, by Shimadzu (2 mentions) Dpx 75 mhz spectrometer, by Bruker (2 mentions)

Close spelling variants of this product

Avance DPX-300 FT-NMR spectrometer DPX FT-NMR spectrometer DPX-300 NMR spectrometer DPX-300 spectrometer FT-NMR spectrometer DPX-300 DPX spectrometers NMR spectrometer Bruker spectrometers

2 protocols using dpx 300 ft nmr spectrometer

Synthesis and Characterization of Novel Organic Compounds

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All reagents were purchased from commercial suppliers and were used without further purification. Melting points (M. p.) were determined on the Mettler Toledo-MP90 Melting Point System and were uncorrected. ¹H-NMR (nuclear magnetic resonance) Bruker DPX 300 FT-NMR spectrometer; ¹³C-NMR, Bruker DPX 75 MHz spectrometer (Bruker Bioscience, Billerica, MA, USA). In the ¹H NMR spectra, the splitting patterns were designated as follows: s: singlet; brs: broad singlet; d: doublet; dd: doublet of doublets; t: triplet; m: multiplet; q: quartet. The coupling constants (J) were expressed in Hertz (Hz). Mass spectra were recorded on a LCMS-IT-TOF (Shimadzu, Kyoto, Japan) using ESI.

Karaca Ş., Osmaniye D., Sağlık B.N., Levent S., Ilgın S., Özkay Y., Karaburun A.Ç., Kaplancıklı Z.A, & Gundogdu-Karaburun N. (2022). Synthesis of novel benzothiazole derivatives and investigation of their enzyme inhibitory effects against Alzheimer's disease. RSC Advances, 12(36), 23626-23636.

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Characterization of Organic Compounds

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All reagents were purchased from commercial suppliers and were used without further purification. Melting points (M.p.) were determined using the Mettler Toledo-MP90 Melting Point System and were uncorrected. A ¹H-NMR (nuclear magnetic resonance) Bruker DPX 300 FT-NMR spectrometer and a ¹³C-NMR, Bruker DPX 75 MHz spectrometer (Bruker Bioscience, Billerica, MA, USA) were used. A total of 10 mg of compound was weighed and dissolved in 600 µL of DMSO-d₆. In this way, the NMR procedure was carried out. Mass spectra were recorded on an LCMS-IT-TOF (Shimadzu, Kyoto, Japan) using ESI. In total, 10 mg of compound was weighed and dissolved in 1500 µL of MeOH. In this way, the HRMS procedure was carried out.

Haji Ali S., Osmaniye D., Sağlık B.N., Levent S., Özkay Y, & Kaplancıklı Z.A. (2022). Design, Synthesis, and Evaluation of Novel 2H-Benzo[b][1,4]thiazin-3(4H)-one Derivatives as New Acetylcholinesterase Inhibitors. Molecules, 27(7), 2121.

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