2,4,6–Trihydroxybenzene–1,3,5–tricarbaldehyde was ordered from Jilin Yanshen Technology Co., Ltd., Jilin, China. 2,2’–Bipyridine–5,5’–diamine, acetic acid (99%) was obtained from Bide Pharmatech Co., Ltd., Shanghai, China. 1,3,5-Trimethylbenzene (97%), 1,4–dioxane (97%), potassium tetrachloroplatinate(II) (K2PtCl4, 98%), deuterium oxide (99.9%), sodium metavanadate (99.0%), sodium phosphate dibasic dodecahydrate (99%), and sodium molybdate dihydrate (99.0%) were prepared from Aladdin Co., Ltd., Shanghai, China. A total of 30 wt % H2O2 aqueous water, dimethylformamide (DMF, ≥99.5%), isopropyl alcohol (≥99.7%), and methanol (≥99.5%) were bought from Xilong Scientific Co., Ltd., Shantou, China. Iron(III) chloride hexahydrate and cobalt(II) chloride were obtained from Shanghai Macklin Biochemical Co., Ltd., Shanghai, China. The preparation of COF–TB [37 (link)] and 11–molybdo–1–vanadophosphoric acid (polyoxometalates, POM) [49 (link),50 (link)] was based on the supplementary materials . The preparation of COF–TB needs to be carried out at 120 °C without water and oxygen, while the preparation of POM needs to be carried out under normal conditions. The prepared products were dried under vacuum overnight without special instructions.
Iron 3 chloride hexahydrate
Manufactured by Maclin Biochemical Technology
Sourced in China
Iron(III) chloride hexahydrate is a chemical compound with the formula FeCl3·6H2O. It is a crystalline solid that is soluble in water and alcohol. The compound serves as a source of ferric ions (Fe3+) and is commonly used in various industrial and laboratory applications.
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Lab products found in correlation
Methanol, by Xilong (1 mentions)
Isopropyl alcohol, by Xilong (1 mentions)
Dimethylformamide, by Xilong (1 mentions)
Cobalt 2 chloride, by Maclin Biochemical Technology (1 mentions)
Acetonitrile, by Maclin Biochemical Technology (1 mentions)
Acetic acid, by Maclin Biochemical Technology (1 mentions)
Ultra high performance liquid chromatography, by Shimadzu (1 mentions)
Mk 801, by Merck Group (1 mentions)
Uric acid, by Merck Group (1 mentions)
4 6 diamidino 2 phenylindole (dapi), by Beyotime (1 mentions)
Dopamine, by Merck Group (1 mentions)
Norepinephrine, by Merck Group (1 mentions)
L glutamate, by Merck Group (1 mentions)
5 hydroxytryptamine, by Merck Group (1 mentions)
3 4 dihydroxyphenylacetic acid, by Merck Group (1 mentions)
N dimethylformamide, by Maclin Biochemical Technology (1 mentions)
4 protocols using iron 3 chloride hexahydrate
1
COF-TB and Polyoxometalates Synthesis
2
Polycyclic Aromatic Hydrocarbons Analysis
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PAHs standards of benzo[b]fluoranthene (99.4%), ben-zo[a]anthracene (99.0%), fluorene, anthracene (99.9%), and pyrene (98.5%), as shown in Table 1 , were acquired from Manhage Bio-technology (Beijing, China). Analytical grade sodium hydroxide (NaOH), Iron (Ⅱ) chloride tetrahydrate, and Iron (III) chloride hexahydrate were obtained from Macklin. Tetraethyl orthosilicate (TEOS), isopropyl alcohol, ammonia, anhydrous toluene, triethylamine, chloro(diethyl)octadecylsilane (ODS, 95% v/v), hydrochloric acid (HCl, 37% v/v), and potassium bromide (KBr) came from Sigma Macau. Methanol (CH4O, polarity:6.6), 95% ethanol (C2H6O, polarity:4.3), acetonitrile (CH3CN, polarity:6.2), and acetic acid (CH3COOH, polarity:6.2) came from Macklin (Shanghai, China). Acidified acetonitrile (3% acetic acid, v/v) was prepared personally. Ultra-high performance liquid chromatography was from Shimadzu. HPLC-grade acetonitrile and methanol were provided by Anaqua (Cleveland, OH, USA).
3
N-MWCNT-Based Electrochemical Biosensor
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N-MWCNTs was purchased from XFNANO Materials Tech Co. Ltd. (Jiangsu, China). 3HT was bought from TCI (Shanghai, China). Iron(III) chloride hexahydrate was obtained from Shanghai Macklin Biochemical Co. Ltd. (Shanghai, China). Chloroform, methyl alcohol, ethanol, acetone, nitric acid, and potassium hydroxide were purchased from Chongqing Chuandong Chemical Group Co. Ltd. (Chongqing, China). AA, adrenaline, norepinephrine, 3,4-dihydroxyphenylacetic acid, dopamine, 5-hydroxytryptamine, uric acid, AAox, l -glutamate, MK-801, and DIDS were obtained from Sigma-Aldrich (St. Louis, MO, USA), and were prepared in ultrapure water (18.2 MΩ). Artificial CSF (aCSF) was prepared by dissolving NaCl (126 mM), KCl (2.4 mM), KH2PO4 (0.5 mM), MgCl2 (0.85 mM), NaHCO3 (27.5 mM), Na2SO4 (0.5 mM), and CaCl2 (1.1 mM) in ultrapure water, and the solution was adjusted to pH 7.4. CD68 and 4′,6-diamidino-2-phenylindole were bought from Beyotime (Shanghai, China). CD206 (i.e. MRC1) was bought from Proteintech (Hubei, China).
4
Synthesis and Characterization of Transition Metal Complexes
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Rhodium (III) 2,4-pentanedionate (Rh(acac)3, 98%) was purchased from Shanghai Xinbo Chemical Technology Co., Ltd. (China). Zinc nitrate hexahydrate (Zn(NO3)2·6H2O, 99%), hydrogen peroxide (30 wt % in H2O), Dimethyl sulfoxide (DMSO, >99.8%), and isopropanol (99.8%) were purchased from Shanghai Aladdin Biochemical Co., Ltd. (China). Vanadium (III)-2,4-pentanedionate (V(acac)3, 97%), 2-methylimidazole (99%), and 3,3′,5,5′-tetramethylbenzidine (TMB, 99%) were purchased from Meryer (Shanghai) Chemical Technology Co., Ltd. (China). Iron (III) chloride hexahydrate (FeCl3·6H2O, 99%), Cupric chloride (CuCl2, 98%), N, N-dimethylformamide (DMF, 99.5%), and HRP ( >300 U/mg), were obtained by Shanghai Macklin Biochemical Co., Ltd. (China). GPx (740 U/mg), CAT (4323 U/mg) were purchased from Sigma-Aldrich Company Ltd. NADPH tetracyclohexanamina (90%), GR (1164.8 U/mL) were purchased from Shanghai Yuanye Bio-Technology Co., Ltd. (China). GSH (97%) was purchased from Tianjin Xiensaopude Technology Co., Ltd. (China). SOD (5200 U/mg) was purchased from Beijing Solarbio Science & Technology Co., Ltd. (China). Deionized water (>99.5%), methanol (>99.5%), and ethanol absolute (>99.7%) were purified to analytical grade by Tianjin Yuanli Chemical Co., Ltd. (China). Except for special instructions, all experiments were carried out at room temperature.
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