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2 protocols using na2co3

1

Montmorillonite-Sewage Sludge Composite Preparation

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Mt used in this study was obtained from Nanhai, Guangdong province, China. Its cation exchange capacity (CEC) and specific surface area is 0.78 meq·g−1 and 71 m2·g−1, respectively. The chemical composition of Mt is 50.8%, 32.4%, 6.75%, 1.86%, 1.7%, 0.09%, 0.72% and 2.07% for O, Si, Al, Mg, Ca, K, Na and Fe, respectively, which was determinated by X-ray fluorescence. Sewage sludge sample was supplied by the Lijiao wastewater treatment, located in Guangzhou, China. Fe(NO3)3, Na2CO3, HF (40 wt%) and HCl (37 wt%) were purchased from Guangzhou Chemical Reagent Factory (Guangzhou, P. R. China). All the chemicals were of analytical grade and were used without further purification.
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2

Fabrication of Hydrogel Composites

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PVA (PVA-1799), acrylic acid (AA), 2-hydroxy-2-methylpropiophenone (I1173), ZrOCl2·8H2O, chitosan (deacetylation degree ≥ 95%, viscosity is 100–200 mPa·s), and ZnCl2 were purchased from Shanghai Macklin Biochemical Co., Ltd. Agarose (high gel strength) and gelatin (gel strength ~250 g Bloom) were purchased from Shanghai Aladdin Bio-Chem Technology Co., Ltd. AlCl3 was purchased from Sinopharm Chemical Reagent Co., Ltd. Gly, K2CO3, NaBr, KCl, CaCl2, BaCl2, MgCl2, Na2SO4, NaCl, Na3Cit, NaAc, Na2HPO4, and Na2CO3 were purchased from Guangzhou Chemical Reagent Factory. The deionized water was obtained using a water purification system.
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