Zirconium oxychloride octahydrate

Manufactured by Merck Group

Zirconium oxychloride octahydrate is a chemical compound with the formula ZrOCl2·8H2O. It is a white, crystalline solid that is soluble in water and various organic solvents. Zirconium oxychloride octahydrate is commonly used as a precursor in the production of zirconium-based materials and as a reagent in various chemical processes.

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Zirconium(IV) oxychloride octahydrate Zirconium oxychloride

8 protocols using zirconium oxychloride octahydrate

Tunable Superhydrophobic Polymer Coatings

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Hexamethylene diisocyanate
(HDI), polycaprolactone diol (PCL-OH, Mn ∼ 2000 g mol^–1), pyromellitic dianhydride (PMD), dibutyltin dilaurate (DBTDL),
ethanolamine, zirconium oxychloride octahydrate (ZrCl₂·8H₂O), 2-aminoterepthalic acid (ATPA), octanoic acid, sodium
hydroxide, acetic acid, trichloro(octadecyl)silane (OTS), dimethyl
formamide (DMF), chloroform, acetone, toluene, isopropanol, hexane,
and silicone oil (20, 100, 500, and 1000 cSt) were purchased from
Sigma-Aldrich. 1,5-Diisocyanatonaphthalene (NDI) was purchased from
Tokyo Chemical Industry UK Ltd. All the chemicals were used without
further purification. Commercial NeverWet coating components, used
as a control for comparison, were obtained from the Rust-Oleum.

Zhang J., Singh V., Huang W., Mandal P, & Tiwari M.K. (2023). Self-Healing, Robust, Liquid-Repellent Coatings Exploiting the Donor–Acceptor Self-Assembly. ACS Applied Materials & Interfaces, 15(6), 8699-8708.

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Synthesis of Bismuth Zirconate Nanoparticles

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Zirconium
oxychloride octahydrate [ZrOCl₂.8H₂O] and bismuth
acetate [(CH₃CO₂)₃Bi], oleic acid,
1-octadecane, selenourea, and ethanol were used directly as purchased
from Sigma Aldrich.

Aher R., Punde A., Shinde P., Shah S., Doiphode V., Waghmare A., Hase Y., Bade B.R., Jadhav Y., Prasad M., Pathan H.M., Patole S.P, & Jadkar S.R. (2022). Synthesis, Structural and Optical Properties of ZrBi2Se6 Nanoflowers: A Next-Generation Semiconductor Alloy Material for Optoelectronic Applications. ACS Omega, 7(36), 31877-31887.

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Chemical Characterization and Purification

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All the chemicals used in the experiments
were of analytical grade and used without further purification. Citric
acid (Merck), ethylenediamine (Merck), zirconium oxychloride octahydrate
(Sigma-Aldrich), barium chloride dihydrate (Merck), potassium hydroxide
pellets (Merck), sodium sulfide (Sigma-Aldrich), sodium sulfite (Sigma-Aldrich),
glacial acetic acid (Merck), and MB (Merck) were used as received.
Milli-Q water (18.2 MΩ cm) was used in all the experiments.

Patra A.S., Gogoi G, & Qureshi M. (2018). Ordered–Disordered BaZrO3−δ Hollow Nanosphere/Carbon Dot Hybrid Nanocomposite: A New Visible-Light-Driven Efficient Composite Photocatalyst for Hydrogen Production and Dye Degradation. ACS Omega, 3(9), 10980-10991.

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Synthesis and Characterization of Neem-Based Nanomaterials

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Ceric-ammonium nitrate, zirconium oxychloride
octahydrate (ZrOCl₂·8H₂O, ≥99.5%),
methylene blue (C₁₆H₁₈ClN₃S.XH₂O), β-cyclodextrin, dopamine hydrochloride, and TMB
were purchased from Sigma-Aldrich. H₂O₂ (30
wt %), 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyl tetrazolium bromide
(MTT), and 2′,7′-dichlorofluorescin diacetate (DCFH-DA)
were purchased from Alfa-Asser. Fresh neem leaves were collected from
the University of North Bengal Campus. All the chemicals are used
in this work were analytical graded and used without further purification.

Ali S., Sikdar S., Basak S., Rajbanshi B., Mondal M., Roy D., Dutta A., Kumar A., Dakua V.K., Chakrabarty R., Roy A., Barman A., Datta A., Roy P.K., Chakraborty B, & Roy M.N. (2022). β-Cyclodextrin-Stabilized Biosynthesis Nanozyme for Dual Enzyme Mimicking and Fenton Reaction with a High Potential Anticancer Agent. ACS Omega, 7(5), 4457-4470.

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Zirconium Oxychloride-based Synthesis

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Zirconium oxychloride octahydrate (ZrOCl₂·8H₂O, purity ≥99.5%), fumaric acid,
and Sigmacote siliconizing reagent were obtained from Sigma-Aldrich
Co. N,N-Dimethylformamide (DMF),
formic acid (purity ≥99.0%), and anhydrous methanol were obtained
from EMD Millipore Chemicals. Anhydrous acetone was obtained from
Acros Organics.

Fuchs A., Knechtel F., Wang H., Ji Z., Wuttke S., Yaghi O.M, & Ploetz E. (2023). Water Harvesting at the Single-Crystal Level. Journal of the American Chemical Society, 145(26), 14324-14334.

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Synthesis of Zirconium Oxide Nanocomposites

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Zirconium oxychloride octahydrate
(ZrOCl₂·8H₂O, 98%) and trans-1,2 diaminocyclohexane-N,N,N,N-tetraacetic acid monohydrate (CDTA
monohydrate, 98%) were purchased from Sigma-Aldrich. Polyvinyl alcohol
(molecular weight = 1,45,000; degree of hydrolysis = 98–99%),
sodium fluoride (NaF, 99.99%), sodium hydroxide (NaOH, 99%), hydrochloric
acid (HCl, 37–38%), acetic acid (CH₃COOH, 96%),
copper sulfate pentahydrate (CuSO₄·5H₂O,
99%), ferric nitrate nonahydrate [Fe(NO₃)₃·9H₂O, 98%], glutaraldehyde [OHC(CH₂)₃CHO,
50 wt % solution in H₂O], and potassium chromate (K₂CrO₄, 98.5%) were procured from Merck, India. Sodium
arsenate heptahydrate (Na₂HAsO₄·7H₂O, 98%) was obtained from Loba Chemie Pvt. Ltd., India. All
chemicals were of analytical grade and used without further processing.
The solutions were prepared in Milli-Q water (Direct Q UV-8, 18 MΩ
cm^–1).

Mani S.K, & Bhandari R. (2022). Efficient Fluoride Removal by a Fixed-Bed Column of Self-Assembled Zr(IV)-, Fe(III)-, Cu(II)-Complexed Polyvinyl Alcohol Hydrogel Beads. ACS Omega, 7(17), 15048-15063.

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Synthesis and Characterization of Zr-based MOFs

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All the reagents were commercially available and used as such without further purification. Zirconium tetrachloride (ZrCl₄·8H₂O, purity ≥ 98%), Zirconium oxychloride octahydrate (ZrOCl₂·8H₂O, purity ≥ 99.5%) 1,3,5-Benzenetricarboxylic acid (BTC), 1-Pyrenebutyric acid (PBA), and Methyl viologen (MV) were purchased from Sigma-Aldrich Chemical Co. Ltd. Dimethylformamide (DMF), formic acid (purity > 98%), anhydrous acetone and anhydrous methanol were purchased from Spectrochem Pvt. Ltd. All the photophysical studies were carried out using HPLC grade solvents. ¹³CO₂ cylinder was purchased from Sigma-Aldrich Chemical Co. Ltd.

Karmakar S., Barman S., Rahimi F.A., Rambabu D., Nath S, & Maji T.K. (2023). Confining charge-transfer complex in a metal-organic framework for photocatalytic CO2 reduction in water. Nature Communications, 14, 4508.

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Synthesis of Doped Zirconia Nanopowders

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Zirconium oxychloride octahydrate (ZrOCl∙8H₂O), yttrium oxide (Y₂O₃), gadolinium nitrate hexahydrate and neodymium oxide were purchased from Sigma Aldrich and used as received for nanopowders synthesis of 3 mol % yttria-stabilized zirconia (YSZ), YSZ doped with Nd and YSZ doped with Gd. Chemicals such as HCl, NH₄OH, NaOH used in synthesis and adsorption tests were of analytical grade.
One g/L stock solution of humic acids (Sigma Aldrich, Steinheim, Germany) was prepared by dissolution of HA in the proper volume of double distilled water.

Suchanek M., Niewiara E., Wilkosz K, & Kubiak W.W. (2019). Nanopowders of Yttria-Stabilized Zirconia Doped with Rare Earth Elements as Adsorbents of Humic Acids. Materials, 12(23), 3915.

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