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Tetrachloroethylene

Manufactured by Merck Group
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Tetrachloroethylene is a colorless, dense liquid that is commonly used as a solvent in industrial and laboratory applications. Its primary function is to act as a cleaning and degreasing agent for various materials and equipment.

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Lab products found in correlation

Oleic acid, by Merck Group (12 mentions) Oleylamine, by Merck Group (8 mentions) 1 octadecene, by Merck Group (8 mentions) Toluene, by Merck Group (7 mentions) Methanol, by Merck Group (6 mentions) Chloroform, by Merck Group (6 mentions) Copper 2 acetylacetonate, by Merck Group (3 mentions) 1 dodecanethiol, by Merck Group (3 mentions) Acetonitrile, by Merck Group (3 mentions) Ethanol, by Thermo Fisher Scientific (3 mentions) Acetone, by Merck Group (3 mentions) Dichloromethane, by Merck Group (3 mentions) Hexadecylamine, by Merck Group (2 mentions) Selenium powder, by Strem Chemicals (2 mentions) Trioctylphosphine, by Merck Group (2 mentions) Trifluoroacetic acid, by Merck Group (2 mentions) Ethylene glycol, by Merck Group (2 mentions) Cadmium acetate dihydrate, by Merck Group (2 mentions) 1 butanol, by Merck Group (2 mentions) Trichloroethylene, by Merck Group (2 mentions)

23 protocols using tetrachloroethylene

1

Synthesis and Characterization of Bi-MMOF Adsorbent

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High purity trichloroethylene (99%), tetrachloroethylene (99.5%), chloroform (99.3%), and tetrachloroethylene (99.2%) as targeted analytes were purchased from Sigma Aldrich company. Moreover, Zn(ii) nitrate hexahydrate (Zn(NO3)2·6H2O; 99%), nickel(ii) nitrate hexahydrate (Ni(NO3)2·6H2O; 99%), and benzene-1,3,5-tricarboxylic acid (H3BTC; 95%) as reagent-grade materials for the preparation of the bi-MMOF absorbent were purchased from the Merck company (Darmstadt, Germany). The chemicals were used as received without any purification. Ethanol (C2H5OH; 99%) as the solvent was purchased from Merck company (Darmstadt, Germany). Pure nitrogen gas (99.9%) was obtained from Roham gas Co (Tehran, Iran).
Rahimpoor R., Firoozichahak A., Nematollahi D., Alizadeh S., Alizadeh P.M, & Alinaghi Langari A.A. (2021). Determination of halogenated hydrocarbons in urine samples using a needle trap device packed with Ni/Zn–BTC bi-MMOF via the dynamic headspace method. RSC Advances, 11(35), 21537-21547.
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2

Synthesis and Characterization of Metal Nanoparticles

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Copper (II) acetylacetonate (Cu(acac)2, 97%), iron (III) acetylacetonate (Fe(acac)3, ≥99.9%), 1-dodecanethiol (DDT, ≥ 98%), oleic acid (OA, technical grade, 90%), oleylamine (Olam, technical grade, 70%), toluene (anhydrous), nitric acid (70%, TraceMetal grade), and tetrachloroethylene (TCE, ≥ 99.9%) were purchased from Sigma-Aldrich. Hexanes (Optima for HPLC, ≥ 99.9%), isopropyl alcohol (99.5%), ethanol (anhydrous, histological), and cobaltocene (98%) were purchased from Fisher Scientific, while sulfur (refined, 99.5%) was procured from ACROS Organics. Quartz glass cuvettes were sourced from Starna Cells Inc. Gold nanorods (10 nm × 67 nm), citrate-coated, were purchased from Nanopartz, and 1,2-distearoyl-sn-glycero-3-phosphoethanolamine-N-[methoxy-(polyethylene glycol)-2000] (ammonium salt) was purchased from Avanti Lipids. All air-sensitive materials were stored and handled in a glovebox under an argon atmosphere.
Kays J.C., Conti CR I.I.I., Margaronis A., Kuszynski J.E., Strouse G.F, & Dennis A.M. (2021). Controlled Synthesis and Exploration of CuxFeS4 Bornite Nanocrystals. Chemistry of materials : a publication of the American Chemical Society, 33(18), 7408-7416.
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3

Synthesis of Lead Halide Perovskites

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Lead bromide (PbBr2, ≥98%),
lead thiocyanate (Pb(SCN)2, 99.5%), cesium carbonate (Cs2CO3, 99%), oleylamine (OLAM, 70%), oleic acid (OA,
90%), 1-octadecene (ODE, 90%), tetrachloroethylene, toluene (anhydrous,
99.8%), lead(II) acetate trihydrate (≥99.5%), benzoyl bromide
(97%), and dodecane were purchased from Sigma-Aldrich. Cesium acetate
(99%) and ethyl acetate (≥99.5%) were purchased from Fisher
Scientific. All chemicals were used without further purification;
lead compounds were stored inside a nitrogen-filled glovebox.
Toso S., Baranov D., Altamura D., Scattarella F., Dahl J., Wang X., Marras S., Alivisatos A.P., Singer A., Giannini C, & Manna L. (2021). Multilayer Diffraction Reveals That Colloidal Superlattices Approach the Structural Perfection of Single Crystals. ACS Nano, 15(4), 6243-6256.
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4

Synthesis of Semiconductor Nanocrystals

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Cadmium oxide (CdO, 99.5%), trioctylphosphine
oxide (99%), trioctylphosphine (TOP, 97%), selenium powder (Se, 99.99%),
and lead(II) acetate trihydrate (Pb(CH3CO2)2·3H2O, 99.999%) were purchased from Strem
Chemicals. Octadecylphosphonic acid (99%) was purchased from Polycarbon
Industries. Copper(II) acetylacetonate (Cu(acac)2, 97%),
hexadecylamine (98%), tetrakis(acetonitrile)copper(I) hexafluorophosphate
(99.99%), octadecene (technical grade, 90%), 1-dodecanethiol (≥98%),
oleylamine (70%), tetrachloroethylene (≥99%), anhydrous chloroform,
methanol, toluene, and tetrahydrofuran were purchased from Sigma-Aldrich.
All chemicals were used without any further purification.
Gariano G., Lesnyak V., Brescia R., Bertoni G., Dang Z., Gaspari R., De Trizio L, & Manna L. (2017). Role of the Crystal Structure in Cation Exchange Reactions Involving Colloidal Cu2Se Nanocrystals. Journal of the American Chemical Society, 139(28), 9583-9590.
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5

Refractive Index Matched PMMA Colloids

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We suspend Nile Red–dyed PMMA colloids and polyhydroxystearic acid polymer–grafted PMMA colloids in a mixture of cis-decahydronaphthalene and tetrachloroethylene (Sigma-Aldrich), whose refractive index and density are closely matched with those of particles, inside a glass capillary. The PMMA particles have diameter σ = 1.8 μm, with the polydispersity of less than 2.5%. The colloidal particle volume fraction ϕ is around 54%. We find that adding 50 mM/liter dioctyl sulfosuccinate sodium salt (Sigma-Aldrich) to the system largely screens surface charges on particles, which allows us to regard the system as hard-sphere like. The other experimental procedures are the same as the charged colloidal systems.
Li M., Chen Y., Tanaka H, & Tan P. (2020). Revealing roles of competing local structural orderings in crystallization of polymorphic systems. Science Advances, 6(27), eaaw8938.
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6

Synthesis of Colloidal Nanocrystal Superlattices

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Benzene (99.8%, anhydrous), n-butanol (99.8%,
anhydrous), 1-chloropentane (99%), cyclohexyl isocyanide
(98%), diphenylphosphine (98%), hexane (mixture of isomers, ≥99%,
anhydrous), isopropanol (99.5%, anhydrous), lead acetate trihydrate
(≥99.99%), methanol (99.8%, anhydrous), 1-octadecene (90%),
octane (≥99%, anhydrous), oleic acid (90%), pyrrolidine (≥99%),
selenium powder (99.99%, −100 mesh), tetrachloroethylene (≥99%,
anhydrous), toluene (99.8%, anhydrous), triethylamine (≥99%),
trifluoroacetic acid (99%), trifluoroacetic anhydride (≥99%),
trimethylbenzene (98%), and trioctylphosphine (90%) were purchased
from Sigma-Aldrich and used without further purification. Lead (II)
oxide (99.999+%) was purchased from Strem Chemicals. 1,4-Butanediol
(BD, 99%, ReagentPlus), diethylene glycol (DEG, 99%), diphenyl ether
(≥99%), ethylene glycol (EG, 99.8%, anhydrous), and hexadecane
(≥99%) were purchased from Sigma-Aldrich and degassed under
vacuum for ∼14 h at 60 °C prior use. For superlattice
formation, a distillation of the EG did not result in a significant
difference in the quality of the formed superlattice (see Figure S1).
van der Sluijs M.M., Sanders D., Jansen K.J., Soligno G., Vanmaekelbergh D, & Peters J.L. (2022). On the Formation of Honeycomb Superlattices from PbSe Quantum Dots: The Role of Solvent-Mediated Repulsion and Facet-to-Facet Attraction in NC Self-Assembly and Alignment. The Journal of Physical Chemistry. C, Nanomaterials and Interfaces, 126(2), 986-996.
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7

Synthesis of Colloidal Nanoparticles

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Acetonitrile (ACN, anhydrous, 99.8%), 1-butanol
(BuOH, 99.8%), cadmium acetate dihydrate (Cd(Ac)2·3H2O), lead(II) thiocyanate (Pb(SCN)2 99.5%), methanol
(MeOH, 99.8%), 1-octadecene (ODE, 90%), oleic acid (OA, 90%), oleylamine
(OLAM, 99%), selenium powder (Se mesh, 99.99%), and tetrachloroethylene
(TCE) were purchased from Sigma-Aldrich. Hexane (anhydrous, 99%) and
toluene (anhydrous, 99.8%) was purchased from Alfa Aesar.
van der Sluijs M.M., Vliem J.F., de Wit J.W., Rietveld J.J., Meeldijk J.D, & Vanmaekelbergh D.A. (2023). Cation Exchange and Spontaneous Crystal Repair Resulting in Ultrathin, Planar CdS Nanosheets. Chemistry of Materials, 35(19), 8301-8308.
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8

Synthesis of Lead Oxide Nanostructures

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Lead(II)
oxide (PbO, yellow powder 99.99%),
hexamethyldisilathiane (synthesis grade), trioctylphosphine (90% technical
grade), toluene (laboratory reagent, ≥99.3%), tetrachloroethylene
(>99%), chloroform (≥99.8%), 1-octadecene (ODE, 90% technical
grade), oleic acid (technical grade 90%), and n-octane
(anhydrous, 99.8%) were purchased by Sigma-Aldrich and used as received.
Ermakov V.A., Silva Filho J.M., Bonato L.G., Mogili N.V., Montoro F.E., Iikawa F., Nogueira A.F., Cesar C.L., Jiménez-Villar E, & Marques F.C. (2018). Three-Dimensional Superlattice of PbS Quantum Dots in Flakes. ACS Omega, 3(2), 2027-2032.
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9

Synthesis and Characterization of Advanced Materials

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The following chemicals were used as received: sodium hydroxide (1 M), sulfuric acid (0.5 M), hexanes (> 99%), anhydrous sodium sulfate and ferrous sulfate were obtained from Fisher Scientific. Sodium borohydride (99.99%), sodium carboxymethyl cellulose (Mw~90k), potassium tetrachloropalladate (II) (98%), biphenyl_d10 (99 atom % D), trichloroethylene (99.5%) and tetrachloroethylene (> 99%) were purchased from Sigma-Aldrich. PVDF powder was purchased from Polysciences, Inc. Potassium persulfate (98%), N,N′-methylenebisacrylamide (NNMA, 99%) and methacrylic acid (99.5%, stabilized) were received from Acros Organics. Nitric Acid (AR select ACS) was ordered from Macron Fine Chemicals. 2-chlorobiphenyl (> 97%) and its analytical solution (100 ppm in hexane) as well as the analytical standards of chloroform (100 ppm in methanol), carbon tetrachloride (100 ppm in methanol) and hexachlorobutadiene (100 ppm in methanol) were obtained from Ultra Scientific. Ethanol (200 proof) was bought from EMD Millipore Corporation. Full scale PVDF 700 microfiltration membranes were obtained from Solecta, Inc. DVPP04700 membranes were purchased from Millipore. Deoxygenated water was obtained by purging N2 into deionized ultra-filtered (DIUF) water for 30 min.
Wan H., Islam M.S., Briot N.J., Schnobrich M., Pacholik L., Ormsbee L, & Bhattacharyya D. (2019). Pd/Fe nanoparticle integrated PMAA-PVDF membranes for chloro-organic remediation from synthetic and site groundwater. Journal of membrane science, 594, 117454.
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10

Colloidal Nanocrystal Synthesis

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Antimony(III) chloride (99.999%, STREM),
copper(I) chloride (99.99%, Sigma-Aldrich), 1-dodecanethiol (DDT,
98%, Sigma-Aldrich), oleylamine (OLA, techn. 80–90%, Acros),
selenium (shots, 99.99%, STREM), chloroform (anhydrous, >99%, Sigma-Aldrich),
ethanol (anhydrous, 99.9%, Acros), tetrachloroethylene (anhydrous,
99%, Sigma-Aldrich), tetrabutylammonium iodide (TBAI, 99%, Sigma-Aldrich),
and methanol (anhydrous, 99.8%, Sigma-Aldrich) were used.
Moser A., Yarema O., Garcia G., Luisier M., Longo F., Billeter E., Borgschulte A., Yarema M, & Wood V. (2023). Synthesis and Electronic Structure of Mid-Infrared Absorbing Cu3SbSe4 and CuxSbSe4 Nanocrystals. Chemistry of Materials, 35(16), 6323-6331.
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