Chemical compounds were purchased from Sigma–Aldrich and Merck companies with a commercial grade and used as received without further purification. Melting points were determined in open capillaries using an electrothermal digital melting point apparatus and were uncorrected. Fourier transform infrared (FT-IR) spectra were recorded on a JASCO 4200-A spectrometer with KBr pellets. 1HNMR and 13CNMR spectra were recorded on a Bruker spectrometer (300–500 MHz) using DMSO-d6 as a solvent and Me4Si as an interior standard. The morphology of the functionalized SBA-15 was investigated using a Leica Cambridge S 360 scanning electron microscope (scanning electron microscopy (SEM) and field emission scanning electron microscopy (FE-SEM)). Transmission electron microscopy (TEM) images were recorded on a Philips CM10 microscope with an acceleration voltage of 100 kV. N2 adsorption–desorption isotherms of SBA-15 nanocomposites were measured at the temperature of liquid nitrogen using a Micromeritics system (made in the United States). The Brunauer–Emmett–Teller surface area of the nanoparticles was calculated using the BET method.
Cambridge s 360 scanning electron microscope
Manufactured by Leica camera
Sourced in United Kingdom
The Cambridge S 360 is a scanning electron microscope (SEM) designed for high-resolution imaging and analysis of microscopic samples. It provides a magnification range from 10x to 300,000x, allowing users to observe fine details and structures at the nanoscale level. The SEM utilizes a focused electron beam to scan the surface of a sample, generating detailed information about its topography, composition, and other characteristics. This instrument is a versatile tool for applications in materials science, nanotechnology, and other fields that require advanced microscopic analysis.
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Lab products found in correlation
2 protocols using cambridge s 360 scanning electron microscope
1
Characterization of Functionalized SBA-15 Nanocomposites
2
SEM Scaffold Morphology Evaluation
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Scanning electron
microscopy (SEM) was used to evaluate the scaffold morphology and
infiltration of the cells. At timed intervals, constructs were removed
from the plates, washed in PBS, and fixed with 2.5% glutaraldehyde
for 30 min. The samples were then washed with PBS, dehydrated in a
graded series of ethanol, dried by hexamethyldisilazane, mounted on
aluminum stages, sputter coated with gold (Fisons Instruments, Sputter
Coater SC502, U.K.), and examined with an a Leica Cambridge S360 Scanning
electron microscope.
microscopy (SEM) was used to evaluate the scaffold morphology and
infiltration of the cells. At timed intervals, constructs were removed
from the plates, washed in PBS, and fixed with 2.5% glutaraldehyde
for 30 min. The samples were then washed with PBS, dehydrated in a
graded series of ethanol, dried by hexamethyldisilazane, mounted on
aluminum stages, sputter coated with gold (Fisons Instruments, Sputter
Coater SC502, U.K.), and examined with an a Leica Cambridge S360 Scanning
electron microscope.
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