Solutions of LiTFSI with RTILs and poly(ethylene glycol) methyl ether (PEG), Mn = 550 g·mol−1 from Sigma-Aldrich (Sigma-Aldrich, St. Louis, MO, USA) were prepared by magnetic stirring for 30–120 min, as model liquid phases for the solid polymer electrolytes.
Peo mw
PEO Mw is a laboratory equipment product from Merck Group. It is a polyethylene oxide material with a specified molecular weight. The core function of this product is to provide a well-defined macromolecular material for research and analytical applications.
Lab products found in correlation
2 protocols using peo mw
Preparation of Solid Polymer Electrolytes
Solutions of LiTFSI with RTILs and poly(ethylene glycol) methyl ether (PEG), Mn = 550 g·mol−1 from Sigma-Aldrich (Sigma-Aldrich, St. Louis, MO, USA) were prepared by magnetic stirring for 30–120 min, as model liquid phases for the solid polymer electrolytes.
Preparation and Characterization of PEO-based Polymer Gel Electrolytes
Preparation procedure U150 was placed in a glass beaker on top of a heating plate inside a glovebox under an argon atmosphere ([O2] < 1 ppm, [H2O] < 1 ppm), and PEO powder was added stepwise while stirring with a glass rod and rising the temperature up to 70 o C. As soon as the temperature got close to 60 o C, the change in the viscosity revealed the melting and mixing of the polymer and the PGE formed.
The PEO:urea 1:1 inclusion compound (IC), used as a reference for the interpretation of the FT-IR spectrum of PEO50-1/U150, has been prepared as reported in the literature [9] by adding the desired quantity of urea to 100 mL of MilliQ water. Under vigorous stirring at 70 o C, 0.5 g of PEO were added stepwise. Once the polymer was dissolved, the mixture was let to cool down at ambient temperature. Then, 10 mL aliquots were frozen for 12 hours at -20 o C and freeze-dried to eliminate the water. The IC obtained were white solids.
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