Samples (3–7 mg) were accurately weighed using ENTRIS224-1S Balance, Sartorius Lab Instrument GmbH & Co. K.G. (Gottingen, Germany), into sealed aluminum pans with a capacity of 40 μL. The weighing pans were hermetically sealed with three vent holes. The samples were scanned at a heating rate of 10 °C/min under nitrogen purge from 25–400 °C [17 ] using Shimadzu DSC-60 (Kyoto, Japan) calorimeter. Shimadzu DSC-60 data analysis software was used for the analysis of thermodynamic events.
Dsc 60
Manufactured by Shimadzu
Sourced in Japan, Germany, United States
The DSC-60 is a Differential Scanning Calorimeter (DSC) manufactured by Shimadzu. It is a thermal analysis instrument that measures the difference in the amount of heat required to increase the temperature of a sample and a reference material as a function of temperature. The DSC-60 can be used to study a variety of thermal events, such as melting, crystallization, and glass transitions, in a wide range of materials.
Automatically generated - may contain errors
Lab products found in correlation
Dtg 60, by Shimadzu (8 mentions)
Tga 50, by Shimadzu (6 mentions)
Ta 60ws software, by Shimadzu (6 mentions)
Dtg 60h, by Shimadzu (5 mentions)
Ta 50i pc system, by Shimadzu (5 mentions)
Ifs 55, by Bruker (5 mentions)
Tga 51, by Shimadzu (4 mentions)
Jsm 7001f, by JEOL (4 mentions)
Tecnai g2 f30, by Thermo Fisher Scientific (4 mentions)
Ta 60w, by Shimadzu (4 mentions)
Ta 60, by Shimadzu (4 mentions)
Geigerflex xrd, by Philips (3 mentions)
Jem 2100, by JEOL (2 mentions)
Jem 1200ex, by JEOL (2 mentions)
Sa3100, by Beckman Coulter (2 mentions)
Ultima 4, by Rigaku (2 mentions)
Zetasizer nano z, by Malvern Panalytical (2 mentions)
Tg 60, by Shimadzu (2 mentions)
Tga 60, by Shimadzu (2 mentions)
Geigerflex xrd, by Rigaku (2 mentions)
349 protocols using dsc 60
1
Thermodynamic Analysis of Solid Samples
2
Synthesis and Characterization of Phenothiazine Derivatives
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Melting points were measured in glass plates
on a Yanagimoto melting point apparatus. UV/vis/near-IR absorption
spectra in solution state and KBr pellets were obtained on a JASCO
V-650 spectrophotometer and a Shimadzu UV/vis/near-IR scanning spectrometer
UV-3100 PC, respectively. UV/vis/near-IR spectra of neat samples were
recorded using an Ocean Optics HR4000 spectrometer. Differential scanning
calorimetry (DSC) was performed with a SHIMADZU DSC-60. TGA and differential
thermal analysis were measured using a SHIMADZU DTG-60. ESR spectra
were recorded with a JEOL JES-FE1XG. The magnetic susceptibility measurements
were performed using a Quantum Design SQUID magnetometer, MPMS-XL.
Single-crystal X-ray data were collected by a Rigaku XtaLAB P200 diffractometer
with graphite monochromated Mo Kα radiation (λ = 0.71075
Å). Powder XRD was performed on a Philips X’Pert Pro MPD
diffractometer using Cu Kα radiation (λ = 1.5418 Å).
Silver bis(trifluoromethanesulfonyl)imide, dehydrated dichloromethane,
and cyclohexane were commercially available and used without further
purification. N-n-Pentyl-10H-phenothiazine (1 ) and N-n-octyl-10H-phenothiazine (N-octyl analogue) were prepared according to the literature.19 (link) Compounds 1 •+ ·BF 4 – , 1 •+ ·PF 6 – , and 1 •+ ·SbF 6 – were prepared
using corresponding silver salts by the similar method of1 •+ ·NTf 2–.
on a Yanagimoto melting point apparatus. UV/vis/near-IR absorption
spectra in solution state and KBr pellets were obtained on a JASCO
V-650 spectrophotometer and a Shimadzu UV/vis/near-IR scanning spectrometer
UV-3100 PC, respectively. UV/vis/near-IR spectra of neat samples were
recorded using an Ocean Optics HR4000 spectrometer. Differential scanning
calorimetry (DSC) was performed with a SHIMADZU DSC-60. TGA and differential
thermal analysis were measured using a SHIMADZU DTG-60. ESR spectra
were recorded with a JEOL JES-FE1XG. The magnetic susceptibility measurements
were performed using a Quantum Design SQUID magnetometer, MPMS-XL.
Single-crystal X-ray data were collected by a Rigaku XtaLAB P200 diffractometer
with graphite monochromated Mo Kα radiation (λ = 0.71075
Å). Powder XRD was performed on a Philips X’Pert Pro MPD
diffractometer using Cu Kα radiation (λ = 1.5418 Å).
Silver bis(trifluoromethanesulfonyl)imide, dehydrated dichloromethane,
and cyclohexane were commercially available and used without further
purification. N-n-Pentyl-10H-phenothiazine (
using corresponding silver salts by the similar method of
3
Thermal Analysis of PEGylated Nanoparticles
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Lyophilized PEGylated nanoparticles were analyzed by means of the DSC method to ascertain the enthalpy changes that occurred because of changes in the physical and chemical properties of the samples. The Shimadzu DSC 60 (Japan) was utilized to carry out the DSC analysis on the PEGylated chitosan nanoparticles. In an un hermetically sealed aluminium pan, nanoparticle powder was placed, and the temperature was increased from 30 to 250 °C at a rate of 10 °C per minute while maintaining a 10 mL/min airflow min−1 (Madkhali et al., 2021 (link)).
4
Thermal Analysis of Polymeric Nanoparticles
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DSC analysis of the samples was performed on a previously calibrated DSC 60 (Shimadzu, Tokyo, Japan) for temperature and heat flow precisely using Indium. SB, PCL/Pluronic F68, and SB loaded PCL/Pluronic F68 Nanoparticles DSC spectra were collected. Accurately weighted samples (3 mg) were put in hermetically sealed aluminium pans and heated at a scanning speed of 50 °C/min while purging with nitrogen at a rate of 10 mL/min through the melting temperature range. Endotherms were measured from 40 to 300°C against a reference of a sealed aluminium empty crucible.
5
Thermal Analysis of Drug Formulation
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The Differential scanning calorimeter (Shimadzu DSC-60, Tokyo, Japan) were used for DSC scan of pure drug and selected SD4 formulation. The study was held out at a heating rate of 10 °C/min from 10 to 200 °C in the nitrogen atmosphere.
6
Thermal Analysis of Phenol-Formaldehyde Powder
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The DSC analysis was carried out as per ASTM D3418 (ASTM D3418-21, 2021 ) standards using the Shimadzu DSC 60 plus machine with temperatures ranging from -100 °C to 500 °C. Here, 10 mg of phenol-formaldehyde powder was placed in the Standard cooling bath with liquid nitrogen and used to analyze the DSC. The powder was analyzed with the range of temperature from 0 to 200 °C and rate of heat at 25 °C/min.
7
Thermal Characterization of EPI Mixture
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The curing temperature of the EPI mixture was measured using a differential scanning calorimeter (DSC, DSC-60, Shimadzu, Kyoto, Japan). A total of 13 mg of the mixture was placed into an aluminum pan and heated to 30–300 °C (5 °C/min) in a nitrogen atmosphere at a feeding rate of 50 cc/min. In addition, the glass transition temperature (Tg) and curing degree of the postcured EPI was analyzed by placing a specimen of about 4.37 mg in an aluminum pan and heated to 30–300 °C (5 °C/min) in a nitrogen atmosphere at a feeding rate of 50 cc/min.
Thermogravimetric analysis (TGA, TGA-50, Shimadzu, Kyoto, Japan) can measure the initiating decomposition temperature, decomposition propagation behaviors, and total thermal stability in various atmospheres such as nitrogen, helium, and argon. The heat resistance of the EPI was measured by TGA. Thirteen milligrams of crushed blend samples (after curing) were placed into an alumina pan and heated to 900 °C (5 °C/min) in a nitrogen atmosphere at a feeding rate of 50 cc/min. The initial pyrolysis temperature (IDT), maximum weight loss temperature (Tmax), thermal stability index (A*·K*), and integral pyrolysis temperature (IPDT) were calculated based on the results of the TGA.
Thermogravimetric analysis (TGA, TGA-50, Shimadzu, Kyoto, Japan) can measure the initiating decomposition temperature, decomposition propagation behaviors, and total thermal stability in various atmospheres such as nitrogen, helium, and argon. The heat resistance of the EPI was measured by TGA. Thirteen milligrams of crushed blend samples (after curing) were placed into an alumina pan and heated to 900 °C (5 °C/min) in a nitrogen atmosphere at a feeding rate of 50 cc/min. The initial pyrolysis temperature (IDT), maximum weight loss temperature (Tmax), thermal stability index (A*·K*), and integral pyrolysis temperature (IPDT) were calculated based on the results of the TGA.
8
DSC Analysis of Thermal Properties
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DSC measurements were performed using a Shimadzu DSC-60 (Shimadzu, Tokyo, Japan) calorimeter. Samples of 3–10 mg were placed into aluminum pans and the pans were sealed. The reference was an empty aluminum pan of the same type. The samples were subjected to heating in the temperature range of 25 to 200 °C with a heating rate of 2 °C/min.
9
Thermal Analysis of Glibenclamide Formulations
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Thermograms of glibenclamide powder and formulations were recorded on a DSC-60 (Shimadzu, Konstanz, Japan) with a scanning rate of 10°C/min. About 5 mg of the samples were put in aluminum pans. Their thermal behavior ranged from 30 to 300°C.
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Thermograms of glibenclamide powder and formulations were recorded on a DSC-60 (Shimadzu, Konstanz, Japan) with a scanning rate of 10°C/min. About 5 mg of the samples were put in aluminum pans. Their thermal behavior ranged from 30 to 300°C.
10
Thermal Analysis of Electrospray Products
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Melting point, glass transition temperature, and presence of solvents or water in the products of electrospray were investigated by means of a DSC 60 (Shimadzu, Kyoto, Japan). To this end, accurately weighed samples (3–5 mg) were loaded on the sealed aluminum pans. Then, they were examined in the instrument operating at 20°C/min heating rate and 25–250°C temperature range. The reference and calibration substances were aluminum oxide and indium, respectively. TA60 software was administered to analyze the resultant thermograms.
+ Expand
Melting point, glass transition temperature, and presence of solvents or water in the products of electrospray were investigated by means of a DSC 60 (Shimadzu, Kyoto, Japan). To this end, accurately weighed samples (3–5 mg) were loaded on the sealed aluminum pans. Then, they were examined in the instrument operating at 20°C/min heating rate and 25–250°C temperature range. The reference and calibration substances were aluminum oxide and indium, respectively. TA60 software was administered to analyze the resultant thermograms.
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