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2 protocols using diphenyl phosphoryl chloride

1

Cardanol-Based Epoxy Resin Synthesis

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Cardanol was supplied by Biochempia (Korea) and was used as received. Diphenyl phosphoryl chloride (DPPC), triethylamine (TEA), bisphenol A diglycidyl ether (BADGE), and 4,4′-diaminodiphenylmethane (DDM) were purchased from Sigma-Aldrich. Dimethylformamide (DMF), methylene dichloride (MC), and magnesium sulfate were purchased from Daejung chemical. All the other reagents and solvents were used without further purification.
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2

Synthesis of Novel Zirconium-based MOFs

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All the chemicals and solvents were obtained commercially and were used as received without any further purification. ZrCl4 was procured from Acros Organics; 2-aminoterephthalic acid, glutaric anhydride, 2-pyridinecarboxaldehyde, diphenylphosphinic chloride and diphenylphosphoryl chloride were received from Sigma-Aldrich. Acetic anhydride was obtained from Reechem Pvt. Ltd. Maleic anhydride, sulfamic acid and 5-sulfosalicylic acid were received from Loba Chemie Pvt. Ltd. Triethylamine, acetonitrile, DMF, toluene and chloroform were obtained from Merck, while methanol and ethanol were purchased from SD Fine-Chem Ltd. and Changshu Hongsheng Fine Chemicals Co. Ltd., respectively.
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