Methacrylate acid

Manufactured by Merck Group

Methacrylate acid is a colorless organic compound used in various industrial applications. It is a key building block for the production of polymers and other chemical compounds. The core function of methacrylate acid is to serve as a raw material in chemical synthesis processes.

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3 protocols using methacrylate acid

Methacrylate-Based Polymer Synthesis and Characterization

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3-(Trimethoxysilyl)-propyl methacrylate (MAPS) (Tokyo Chemical Industry), atenolol (Tokyo Chemical Industry), metoprolol tartrate hydrochloride (Tokyo Chemical Industry), propranolol hydrochloride (Tokyo Chemical Industry), acetic acid, phosphoric acid, hydrochloric acid (HCl), acetone (Merck), benzoyl peroxide (BPO), ethanol proanalysis, sodium hydroxide, pyridine, and propanol were from Merck. Methacrylate acid (MAA), triethylamine, and ethylene glycol dimethacrylate (EGDMA) were provided by Sigma-Aldrich. Aquabidestillata (Ipha Laboratories), methanol (JT Baker and Fisher Scientific), toluene (Mallinckrodt), and acetonitrile were of HPLC gradient grade (Fisher Scientific). All materials other than those mentioned were of proanalysis grade.
A BET surface area analyser (NOVA instrument© 1994–2010), field emission-scanning electron microscope (FE-SEM) (FEI Quanta 650 FEG), Fourier transform infrared (FTIR) apparatus (IR-Prestige-21 Shimadzu), silicosteel column (outer diameter 1/16 mm, inner diameter 1.02 mm, length 10 cm) (Tubing Sulfinert Restek), oven (Memmert), centrifuge (Labnet C2500-R Prism R™), scanning electron microscope (SEM) (Hitachi TM3000), ultra high-performance liquid chromatography unit (Waters Acquity™), ultrasonicator (NEY 19H), water bath (Memmert), and glass tools were commonly used in laboratories.

Hasanah A.N., Maelaningsih F.S., Apriliandi F, & Sabarudin A. (2020). Synthesis and Characterisation of a Monolithic Imprinted Column Using a Methacrylic Acid Monomer with Porogen Propanol for Atenolol Analysis. Journal of Analytical Methods in Chemistry, 2020, 3027618.

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Synthesis of MIP@MOF Sorbent for Diazinon

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To synthesize of MIP@MOF nano-composite as a sorbent, ethylene glycol demethacrylate (EGDMA; 98.0%), 2-azobisisobutyronitrile (AIBN; 98.0%), terephthalic acid (H₂BDC; 97.0%), ferric chloride hexahydrate (FeCl₃·6H₂O), dimethylformamide (DMF; 99.8%), methacrylate acid (MA; 99%), acetonitrile (99.8%), methanol (99.8%) and acetic acid, toluene (99.0%), and acetone (99.0%) were purchased from Sigma Aldrich and used without any purification. Also, diazinon (60.0%) was purchased from Merck Co (Darmstadt, Germany). Nitrogen with high purity (99.99%) was obtained from Roham Co (Tehran, Iran). XAD-2 sorbent tubes (270 : 140 weight ratio) were purchased from SKC.

Rahimpoor R., Firoozichahak A., Alizadeh S., Soleymani-Ghoozhdi D, & Mehregan F. (2022). Application of a needle trap device packed with a MIP@MOF nano-composite for efficient sampling and determination of airborne diazinon pesticide. RSC Advances, 12(25), 16267-16276.

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Synthesis of Functional Latex Polymers

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Diethyl methylene malonate (Chemi-lian M1000, DEMM) and Forza B3100 (DEMM)₆ were provided by Sirrus Inc. (Loveland, OH). Methyl methacrylate (MMA, Fisher), butyl acrylate (BA, Acros Organics), and methacrylate acid (MAA, Sigma-Aldrich) were used as monomers for latex synthesis. 2,2′-Azobis[2-(2-imidazolin-2-yl) propane] dihydrochloride (AIBI, TCI) was used as an initiator, and Triton X-405 (Sigma-Aldrich) was used as a surfactant. Acrylic acid (AA, Sigma-Aldrich), catechol (Acros Organics), 2-vinylbenzoic acid (VBA, Fisher), and benzeneboronic acid (BBA, Alfa Aesar) were used to prepare initiators for DEMM polymerization. Aluminum oxide (Sigma-Aldrich) was used to remove the inhibitor from monomers. N,N-Dimethylformamide (DMF, Fisher) was used as an extractor. Deuterium oxide (D₂O, 99.8% atom D), chloroform-d (CDCl3, 99.8% atom D), and methyl sulfoxide-d₆ (DMSO-d₆, 99.5+% atom D) were obtained from Acros Organics. Doubly deionized (DDI) water was used throughout the work.

Huang M., Liu Y., Yang G., Klier J, & Schiffman J.D. (2019). Anionic Polymerization of Methylene Malonate for High-Performance Coatings. ACS applied polymer materials, 1(4), 657-663.

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