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5 protocols using polyurethane pu

1

Biosynthesis of Silver Nanoparticles from Nerium oleander

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Hydroxypropyl starch (HPS; Formula weight 666.57768, CAS No. 9049-76-7) was purchased from Shanghai Time Chemicals CO., Ltd. Changhai (China). Polyurethane (PU; Mw = 80 kg mol−1) was bought from Sigma-Aldrich Co. Saint Louis MO 63,103 (USA). Silver nitrate (AgNO3) was purchased from Sigma Aldrich Co, Berlin, Germany. N,N-Dimethylforamide (DMF) was supplied by Sigma Aldrich Co., Czech republic, Prague. Dimethyl sulfoxide (DMSO) was provided by Merck KGaA, Berlin, Germany. Glutaraldehyde solution was purchased from WINLAB Co., Kolkata-711102, West Bengal, India. Green leaves of the street ornamental plant Nerium oleander (Family: Apocynaceae) and commonly named “Dafla” were collected during September 2021 from Dekernis city, Dakahlia governorate, Egypt.
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2

Fabrication of Bioinspired Spider Silk Composite

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The chimera spidroin gene consists of NT (gene bank accession number AM259067), CT (gene bank accession number JX513956), and two repeat regions (gene bank accession number AJ973155), which were synthesized by Genewiz (Suzhou, China). Silicone rubber liquids (Ecoflex) and polyurethane (PU) were obtained from Sigma–Aldrich. Lithium bromide (LiBr) and sodium carbonate (Na2CO3) were purchased from Aladdin Co., Ltd. (Shanghai, China). Ti3C2Tx MXene and PTFE films were purchased from 11 Technology Co. Copper foil tape was obtained from Sigma‒Aldrich Co. Rhodamine B, PTFE film, and gelatin hydrogel obtained from bovine skin were purchased from Sigma‒Aldrich Co.
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3

Perovskite Solar Cell Fabrication

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All the chemical materials and reagents are purchased and used directly without further optimization or purification, including bathocuproine (BCP, Sigma-Aldrich), poly(ethylene-co-vinyl acetate) (EVA, vinyl acetate 40 wt%), anhydrous N, N-dimethylformamide (DMF, Sigma-Aldrich), anhydrous dimethyl sulfoxide (DMSO, Sigma-Aldrich), anhydrous ethyl alcohol (99.5%, Sigma-Aldrich), lead (II) iodide (PbI2, 99.999% purity, Afar Aesar), polyurethane (PU, Sigma-Aldrich), lead(II) bromide (PbBr2, Sigma-Aldrich), formamidinium iodide (HC(NH2)2I, Xi’an p-OLED Corp), aqueous PEDOT:PSS solution (CLEVIOSTM Al 4083, Heraeus), methylamine iodide (MAI) (>98% purity, Dyesol) and [6,6]-phenyl-C61-butyric acid methyl ester (PC61BM, American Dye Source Inc), anhydrous isopropanol (99.5%, Sigma-Aldrich), rigid and flexible indium tin oxide (ITO) substrates.
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4

Peppermint Extract Polymer Nanoformulation

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Dried Mentha piperita L. (peppermint) was purchased from a local herbal drug market (Tehran, Iran) and was identified and deposited at the Herbarium of Pharmacy Faculty, Tehran University of Medical Sciences, Iran (PMP-1301). Gelatin, dimethylformamide (DMF), ethanol, and tannic acid were obtained from Merck. Pluronic F127 and polyurethane PU (Mw = 110,000) were purchased from Sigma-Aldrich and Cardio Tech., Japan, respectively.
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5

Electrochemical Glucose Sensor Development

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Aspergillus Niger GOx (270 U/mg) was purchased from BBI solutions Ltd, UK. TTF, 0.01 M sterile phosphate buffer solution (PBS used as the supporting electrolyte for the electrochemical studies), D glucose anhydrous, paraffin wax, Tetrahydrofuran (THF), Methyl Ethyl Ketone (MEK) and extra pure deionised water were purchased from Fisher Scientific, UK. Glutaraldehyde (25%), diacetone alcohol and polyurethane (PU) were purchased from Sigma Aldrich, UK. Graphene based carbon ink (HDPlas ® IGSC02002) was purchased from Haydale, UK. SU8-2075 was purchased from A-Gas Electronic Materials. 126-49 -Silicone Medical Electrode Ag/AgCl Ink was purchased from Creative Materials Ltd. Details on the solutions preparation are provided in Supporting Information, section 1.
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