Barium oxide (BaO, 90%, ACROS), calcium hydride (CaH2, Sigma-Aldrich), triethylamine (TEA, Sigma-Aldrich), potassium phthalimide (Sigma-Aldrich), hydrazine monohydrate (N2H2, 64 to 66% N2H4, Sigma-Aldrich), sodium trifluoroacetate (NaTFA, 98%, Sigma-Aldrich), 2,5-dihydroxybenzoic acid (DHB, 98%, Sigma-Aldrich) were used as purchased. Prior to use, 2-ethyl-2-oxazoline (EtOx, Sigma-Aldrich) and 2-methyl-2-oxazoline (MeOx, Sigma-Aldrich) were stirred over BaO overnight, distilled and stored under argon atmosphere. Methyl p-tosylate (MeTos, Sigma-Aldrich) was pre-dried over CaH2, distilled under reduced pressure and stored under argon atmosphere. Acetonitrile was obtained from a solvent purification system (SPS; Pure solv EN, InnovativeTechnology). HPLC and MS grade acetonitrile and water for HPLC measurements were obtained from VWR. All other chemicals and solvents were received from common commercial sources and used without further purification unless otherwise stated.
2 methyl 2 oxazoline meox
Manufactured by Merck Group
2-methyl-2-oxazoline (MeOx) is a heterocyclic organic compound that serves as a versatile building block in various chemical reactions and processes. It is a colorless liquid with a characteristic odor. MeOx is commonly used as a precursor in the synthesis of various polymers and other organic compounds.
Automatically generated - may contain errors
Lab products found in correlation
2 5 dihydroxybenzoic acid dhb, by Merck Group (1 mentions)
Triethylamine tea, by Merck Group (1 mentions)
Barium oxide, by Thermo Fisher Scientific (1 mentions)
Calcium hydride cah2, by Merck Group (1 mentions)
2 ethyl 2 oxazoline etox, by Merck Group (1 mentions)
Potassium phthalimide, by Merck Group (1 mentions)
Sodium trifluoroacetate natfa, by Merck Group (1 mentions)
Ethanol, by Merck Group (1 mentions)
Acrylic acid, by Merck Group (1 mentions)
Bacmam 2, by Thermo Fisher Scientific (1 mentions)
1 4 dioxane, by Merck Group (1 mentions)
Celllight golgi gfp, by Thermo Fisher Scientific (1 mentions)
L ascorbic acid, by Merck Group (1 mentions)
Diethyl ether dee, by Merck Group (1 mentions)
Poly ethylene glycol methyl ether acrylate, by Merck Group (1 mentions)
Celllight er gfp, by Thermo Fisher Scientific (1 mentions)
Cyanine5 amine, by Lumiprobe (1 mentions)
2 protocols using 2 methyl 2 oxazoline meox
1
Synthesis of Functionalized Polymers
2
Synthesis and Characterization of Functional Polymers
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Acrylic acid (AA, 99%, anhydrous, Sigma-Aldrich), acetonitrile (ACN, 99.8%, Sigma-Aldrich), 4-methoxyphenol (MEHQ, 99%, Sigma-Aldrich), diethyl ether (DEE, >98%, Sigma-Aldrich), ethanol (>99.8%, Sigma-Aldrich), 1,4-dioxane (>99%, Sigma-Aldrich), Luperox® TBH70X tertbutyl hydroperoxide solution (tBuOOH, 70% wt.% in H2O, Sigma-Aldrich), L-ascorbic acid (AsAc, Sigma Aldrich), 2-methoxyethylamine (MeOEtNH2, 99%, Sigmal-Aldrich), poly(ethylene glycol) methyl ether acrylate (Sigma-Aldrich), 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4methylmorpholinium chloride (DMTMM-HCl, >96%, Sigma-Aldrich) and 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium tetrafluoroborate (DMTMM-BF4, 97%, Sigma Aldrich) were used as purchased without further purification. 2-Methyl-2-oxazoline (MeOx, 98%, Sigma-Aldrich) was distilled to dryness over barium oxide (BaO) and stored in a nitrogen atmosphere.
The chain transfer agent (CTA), 2-(((butylthio)-carbonothioyl)thio)-propanoic acid was prepared according to a literature procedure. 35 Amine-terminated poly(2-ethyl-2-oxazoline) (PEtOxNH2) was synthesized following a literature procedure. 36 2-(pyridyldithio)-ethylamine hydrochloride (PDS) was obtained from Speed Chemical, China. Cyanine5 amine was purchased from Lumiprobe. CellLight™ ER-GFP, BacMam 2.0 and CellLight™ Golgi-GFP, BacMam 2.0 were purchased from Thermo Fisher Scientific.
The chain transfer agent (CTA), 2-(((butylthio)-carbonothioyl)thio)-propanoic acid was prepared according to a literature procedure. 35 Amine-terminated poly(2-ethyl-2-oxazoline) (PEtOxNH2) was synthesized following a literature procedure. 36 2-(pyridyldithio)-ethylamine hydrochloride (PDS) was obtained from Speed Chemical, China. Cyanine5 amine was purchased from Lumiprobe. CellLight™ ER-GFP, BacMam 2.0 and CellLight™ Golgi-GFP, BacMam 2.0 were purchased from Thermo Fisher Scientific.
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