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4 protocols using 1 octadecene

1

Synthesis of Inorganic Nanoparticles

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Sodium diethyldithiocarbamate trihydrate (NaDDTC·3H2O, 99%), sodium molybdate dihydrate (Na2MoO4·2H2O), 1-octadecene (1-ODE, 90%), and 1-dodecanethiol (DDT, C12H25SH, 99.5%) were provided by Sinopharm Chemical Reagent Co., Ltd. Aldrich provided analytical solvents such as methanol, ethanol, acetone, and n-hexane. All solvents and reactants were employed without additional purification.
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2

Synthesis of Niobium Diselenide Nanostructures

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All the reagents were directly used without further purification. Niobium chloride (NbCl5, 99.9%) and selenium powder (Se, ≥ 99.99% metals basis) were purchased from Shanghai Macklin Biochemical Co., Ltd.; 1-octadecene (ODE, 90%) and oleylamine (OA, 98%) were purchased from Adamas-beta; and carbon disulfide (CS2, Aldrich, 99.9%) was from Sinopharm Chemical Reagent Co., Ltd. All chemicals were used without further purification.
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3

Synthesis of Nanomaterials Using Diverse Reagents

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CTAB, polyvinylpyrrolidone (PVP, molecular weight 55,000 g mol−1), sodium citrate monohydrate (99%), sodium citrate dihydrate (99%), and TEOS were purchased from Aladdin (Shanghai, China). 1-Octadecene (ODE), oleylamine (OAm), trioctylphosphine (TOP), palladium acetylacetonate (Pd(acac)2), platinum acetylacetonate (Pt(acac)2), dimethyl formamide (DMF), THF, ethyl acetate (EtOAc), n-pentanol, ammonium hydroxide (NH3·H2O 28 wt%), anhydrous ethanol, iron (III) chloride hexahydrate (99%), iron (II) chloride tetrahydrate (99.95%) were purchased from Sinopharm (Shanghai, China). All chemicals were used as received without further purification. Deionized water was used for all experiments.
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4

Synthesis of Inorganic Nanoparticles

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Dimethyl sulfoxide and 1-octadecene (90%) were purchased from Sinopharm Group (Sinopharm, Hongkong, China). Oleic acid and cyclohexane (C6H12) were obtained from Adamas-beta Company (Adamas-beta, Shanghai, China). Sodium tungstate dehydrate (Na2WO4·2H2O) was purchased from Sigma-Aldrich (St Louis, MO, USA). All chemical reagents were used as bought without any purification. All aqueous solution used in the experiment was deionized water (18.2 MΩ.cm) obtained from Milli-Q water purification system.
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