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Avaspec hs2048xl

Manufactured by Avantes

The AvaSpec-HS2048XL is a high-sensitivity, high-resolution fiber optic spectrometer designed for laboratory applications. It features a 2048-pixel CCD detector and a wide spectral range. The core function of this product is to provide precise spectral measurements with high sensitivity and resolution.

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2 protocols using avaspec hs2048xl

1

Goniometric Optical Scattering Measurement

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Measurements
were carried out using a lab-made goniometer: A xenon lamp (HPX-2000,
Ocean Optics) was used as the light source, and a spectrometer (AvaSpec-HS2048XL,
Avantes) was used to analyze the scattered optical signal. The sample
was mounted on a rotating stage in the center of the goniometer and
illuminated with a collimated incident beam focused with a 300 mm
focus on the sample surface (light spot size Ø ∼ 1 mm).
A detector was mounted on an arm attached to a motorized rotation
stage and coupled the scattered light into an optic fiber connected
to the spectrometer. The recorded light intensity was normalized with
respect to a white Lambertian diffuser, while the exposure time was
adjusted using an automatized high dynamic range method.53 (link) Measurements were recorded at a fixed angle
γ = 90° between incident and outgoing beams by scanning
the sample tilt ϕ̂, defined from the angular bisector
of the two beams (e.g., ϕ̂
= 0° corresponds to specular conditions).
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2

Photoluminescence Characterization of Phosphors

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The PL excitation spectra were recorded using a spectrometer (Varian Carry 50) in the 600–250 nm range, monitored at 650 nm for Ca1-xS:Eux2+ 614 nm for Sr1-xS:Eux2+ and 514 nm for the SAED phosphors. The phosphors were placed in 1 mm quartz cuvettes during the measurement. The PL emission was recorded using a spectrometer (CCS200, Thorlabs) coupled with an optical fiber of 1 mm diameter (FP100URT, Thorlabs) after 450 nm LED excitation. To calculate the PLQY, an optical setup with a spectrometer (AvaSpec-HS2048XL, Avantes) coupled with an optical fiber (FP100URT, Thorlabs) to an integrating sphere (15 cm diameter, Lab sphere) was used. A 450 nm LED, controlled with a benchtop diode controller (ITC4001, Thorlabs) was used as the excitation source and was directed towards the sample in quartz cuvettes inside the integrating sphere where several measurements as described by de Mello et al. method were taken44 (link). Measurements of the empty sphere, direct and indirect excitation spectra, direct and indirect PL emission spectra, and black background were recorded, from which the PLQY was calculated.
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