were carried out using a lab-made goniometer: A xenon lamp (HPX-2000,
Ocean Optics) was used as the light source, and a spectrometer (AvaSpec-HS2048XL,
Avantes) was used to analyze the scattered optical signal. The sample
was mounted on a rotating stage in the center of the goniometer and
illuminated with a collimated incident beam focused with a 300 mm
focus on the sample surface (light spot size Ø ∼ 1 mm).
A detector was mounted on an arm attached to a motorized rotation
stage and coupled the scattered light into an optic fiber connected
to the spectrometer. The recorded light intensity was normalized with
respect to a white Lambertian diffuser, while the exposure time was
adjusted using an automatized high dynamic range method.53 (link) Measurements were recorded at a fixed angle
γ = 90° between incident and outgoing beams by scanning
the sample tilt ϕ̂, defined from the angular bisector
of the two beams (e.g., ϕ̂
= 0° corresponds to specular conditions).