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5 protocols using potassium hydroxide

1

Tung Oil-based Epoxy Composites

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Tung oil was obtained from the Institute of Chemical Industry of Forestry Products. Diglycidyl ether of bisphenol A (epoxide value: 0.48–0.54 equiv. (100 g)−1), Baling Petrochemical Branch Company, PetroChina Co., Ltd, polyetherimide (D230, amine value: 8.1–8.7 mequiv. g−1, Huntsman Chemical Co., Ltd), triphenylphosphine (99.5%, Shanghai Lingfeng Chemical Reagent Co., Ltd), acrylonitrile (98%, Sinopec Shanghai Petrochemical Co., Ltd), potassium oleate (98%, Shanghai Macklin Biochemical Co., Ltd), ammonium persulphate (98%, Shanghai Lingfeng Chemical Reagent Co., Ltd), sodium chloride (Xilong Scientific Co., Ltd), sodium hydroxide (Xilong Scientific Co., Ltd), potassium hydroxide (Xilong Scientific Co., Ltd), methanol (99.5%, Nanjing Chemical Reagent Co., Ltd), hydrochloric acid (36.0–38.0%, Nanjing Chemical Reagent Co., Ltd) and epoxidized soybean oil (epoxide value: 0.38 equiv. (100 g)−1, Shanghai Aladdin Chemical Reagent Co., Ltd) were used as received.
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2

Comprehensive LC-MS and GC-MS Analysis

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MS spectra were acquired using a Synapt G2‐SI Accurate‐Mass Q‐TOF instrument (Waters Corp., Milford, MA) and a 7890A‐5975C system (Agilent Technologies, Inc., Santa Clara, CA). An ACQUITY UPLC HSS T3 column (1.8 μm, 2.1 × 100 mm, Waters Corp.) was used to perform LC–MS analysis; a DB‐1701 GC–MS column (30 m × 250 μm × 0.25 μm, Agilent Technologies, Inc.) was utilized to carry out GC–MS analysis. LC–MS grade acetonitrile and formic acid were purchased from Thermo Fisher Scientific (Waltham, MA, USA). N‐hexane, potassium hydroxide, methanol (LC grade), and anhydrous sodium sulfate were all purchased from Xilong Scientific Co., Ltd. (Silong, China). Water required for UPLC was purified by a Milli‐Q water purification system (Darmstadt, Germany); DPPH was purchased from Shanghai Yuan Ye Bio‐Technology Co., Ltd. (Shanghai, China).
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Momordica grosvenori Extraction and Analysis

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Momordica grosvenori used in this work was purchased from Guilin, Guangxi, China. Potassium hydroxide (KOH, 99.9%) and hydrochloric acid (HCl, 37%) were provided by Xilong Chemical Co., Ltd. (Shantou, China). Nickel foam (99.5%) with a thickness of 2 mm was provided by Lizhiyuan (LZY) Battery Material Co., Ltd. (Taiyuan, China).
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4

Extraction and Characterization of Osmanthus fragrans

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Osmanthus fragrans was acquired at a farmers’ market. Chemicals purchased from Xilong Chemical Co. included potassium hydroxide (KOH), sodium hydroxide (NaOH, 95%), hydrochloric acid (HCl, 37%), and anhydrous ethanol (95%, AR). Methyl orange (MO, AR), methylene blue (MB, AR), rhodamine B (RhB, AR), and Congo red (CR, AR) were bought from Aladdin (Shanghai, China). Malachite green (MG, AR), and crystalline violet (CV, AR) were bought from Xilong Chemical Co., Ltd. (Shantou, China).
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5

Synthesis and Characterization of Pyrrole-Styrene Copolymer

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Pyrrole (C4H5N, CP), styrene (C8H8, >99.5%), amino-1H-tetrazole (CH3N5, >99.0%), sodium dodecyl sulfate (SDS, >99.0%), were purchased from Aladdin Chemistry Co., Ltd. Pyrrole and styrene monomer were distilled under reduced pressure before use. Pt/C (40%, JM) powders (HiSPEC 3000) were obtained from Alfa Aesar. Thiourea (CH4N2S, >99.0%), sodium carbonate (Na2CO3, >98.0%), potassium persulfate (K2S2O8, >99.0%), sodium persulfate ((NH4)2S2O8, >98.0%), polyvinyl alcohol (PVA) were purchased from Sinopharm Chemicals Co., Ltd. Potassium hydroxide (KOH, >95.0%), sulfuric acid (H2SO4, >98.0%), methanol (CH3OH, >99.5%), ethanol (C2H5OH, >99.0%) were provided by Xilong Chemical Reagent Co., Ltd. Distilled deionized water (>18.2 MΩ) was produced by reverse osmosis followed by ion-exchange and filtration (HBI, Shenzhen Honbo Water Treatment Equipment Co., Ltd., China). All chemicals and regents were used without further purification apart from pyrrole and styrene.
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