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Microbalance tg 209 f1 libra

Manufactured by Netzsch

The Microbalance TG 209 F1 Libra is a thermogravimetric analyzer (TGA) designed for precise and accurate measurement of weight changes in materials as a function of temperature or time. It features a high-resolution microbalance for sensitive sample mass detection.

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2 protocols using microbalance tg 209 f1 libra

1

Synthesis and Characterization of Pyridyl-Functionalized Isophthalic Acid Ligands

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Organic ligands 5-(3-(pyridin-3-yl)benzamido)isophthalic acid (3-H2PBI) and 5-(3-(pyridin-4-yl)benzamido)isophthalic acid (4-H2PBI) were synthesized according to reported methods.26,27 (link) Infrared spectra were collected with KBr pellets on a Nicolet/Nexus-670 FT-IR spectrometer. Elemental analyses were obtained by a PerkinElmer 240 elemental analyzer. Thermogravimetric analyses (TGA) were conducted on a Netzsch Thermo Microbalance TG 209 F1 Libra from room temperature to 900 °C with a heating rate of 10 °C min−1 under N2 atmosphere. Powder X-ray diffraction patterns (PXRD) were recorded on a Bruker D8 Advance diffractometer with a Cu target tube and a graphite monochromator.
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2

Comprehensive Physicochemical Characterization

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Bruker‐AXS D8 Advance system with a Cu Kα radiation was conducted on measuring the crystal phase with PXRD in the 2θ range from 10° to 90°. Renishaw inVia confocal Raman microscope provision with an argon ion laser beam was implemented to test Raman spectra. Netzsch Thermo Microbalance TG 209 F1 Libra was employed to observe TGA from ambient temperature to 900 °C with a heating rate of 5 °C min−1 under nitrogen flow. Belsorp max gas sorption analyzer was used to analyze the sorption isotherms at 77 K. K‐Alpha+ XPS spectrometer (Thermo fisher Scientific, USA) was operated using Al Kα radiation to evaluate XPS and the elemental compositions. Moreover, FESEM (TESCAN Maia 3, Czech) and TEM (FEI Talos F200X, USA) with high‐angle annular dark‐field (HAADF) STEM and EDS (JEM2010‐HR, 200 kV) were utilized to study the surface morphology and architecture.
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