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Phenanthridine

Manufactured by Merck Group
Sourced in United States

Phenanthridine is a heterocyclic aromatic compound with the chemical formula C13H9N. It is a colorless crystalline solid that is used as a starting material or intermediate in the synthesis of various pharmaceutical and agrochemical products.

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3 protocols using phenanthridine

1

Polycyclic Aromatic Hydrocarbon Analysis

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Anhydrous sodium sulfate, monobasic and dibasic sodium phosphates, and high-performance liquid chromatography (HPLC)-grade solvents, including dichloromethane (DCM), acetone, and methanol, were purchased from Fisher Scientific (Pittsburgh, PA, U.S.A.). Acridine, phenanthridine, benzo[h]quinoline, benzo[c]Acridine, and the PAH standard solution (EPA 610 PAH mixture) were obtained from Sigma-Aldrich (St. Louis, MO, U.S.A.). Benzo[a]Acridine was purchased from LGC standards (Teddington, Middlesex, UK). Acridine-d9 and dibenzo[a,j]Acridine were from Cambridge Isotope Laboratories (Tewksbury, MA, U.S.A).
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2

Polycyclic Aromatic Hydrocarbons Characterization

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Anhydrous sodium sulfate and high-performance liquid chromatography (HPLC)-grade solvents, including dichloromethane (DCM), acetone, and methanol, were purchased from Fisher Scientific (Pittsburgh, PA, U.S.A.).
Acridine, phenanthridine, benzo[h]quinoline, benzo[c]Acridine, and the PAH standard solution (EPA 610 PAH mixture) were obtained from Sigma-Aldrich (St. Louis, MO, U.S.A.). Benzo[a]Acridine was purchased from LGC standards (Teddington, Middlesex, UK). Acridine-d9 and dibenzo[a,j]Acridine were from Cambridge Isotope Laboratories (Tewksbury, MA, U.S.A).
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3

Synthesis of Phenanthridine Derivatives

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Phenanthridine, 1-isoquinolinyl phenyl ketone, 6-methoxyquinoline, trans-stilbene, diphenyl methanol, deoxyguanosine mononucleotide were obtained from Sigma Aldrich. 8-methoxyquinoline was synthesized according to a literature procedure (49 ). 2-(4′-methoxystyryl) pyridine was a gift from the Eastman Kodak Company. Compounds 1/1E, 2/2E, 3/3E, 4/4E and 6/6E were available from previous studies (41 (link)). The N-methoxy structures 18 were all prepared as tetrafluoroborate salts, the corresponding N-ethyl structures (1E8E) were prepared as either tetrafluoroborate or hexafluorophosphate salts.
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