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2 protocols using silver hexafluorophosphate

1

Synthesis and Evaluation of Gold Nanoparticles

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Silver hexafluorophosphate (98%), potassium hexafluorophosphate (99.5%), N, N, N′, 2-hydroxyethyl disulfide, α-bromoisobutyryl bromide (98%), anisole, tetrafluoroboranuide (IR 1061, 80%), hydrogen tetrachloroaurate (III) trihydrate (HAuCl4·3H2O), and sodium borohydride (96%) silver nitrate (99%) were purchased from Sigma Aldrich. Poly (ethylene glycol) methyl ether thiol (SH-PEG, average Mw 5000) was purchased from Ruixi Biological Technology (Xi'an, China). Ultrapure water (18.25 MΩ resistivity, 25°C) was used in all experiments. Propidium iodide (PI) dye and Annexin V-FITC apoptosis detection kit were purchased from Beyotime Biotechnology (Shanghai, China). Cell Counting Kit-8 (CCK-8) was purchased from MedChemExpress (Monmouth Junction, NJ, USA).
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2

Synthesis of Octabutoxy Naphthalocyanine

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5,9,14,18,23,27,32,36-Octabutoxy-2,3-naphthalocyanine (ONc) was from HPPE Co., tin dichloride was from Alfa Aesar, PEG-10K, PEG 20-K and silver hexafluorophosphate were from Sigma Aldrich, TWEEN 20 was from Amresco, Biobeads SX-1 were from Bio-Rad Laboratories, XTT was from Biotium. ICR mice were ordered from Harlan Laboratories.
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