Diethyl ether dee

Manufactured by Merck Group

Sourced in Germany

Diethyl ether (DEE) is a volatile, colorless, and highly flammable liquid chemical compound. It is commonly used as a laboratory solvent and as a starting material in the synthesis of various organic compounds. DEE has a characteristic sweet, ethereal odor and is primarily employed in chemical research and analysis applications.

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Diethyl ether (590 citations)

3 protocols using diethyl ether dee

Biodegradable Polymer Synthesis and Characterization

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ε-Caprolactone (CL, Acros, 99% purity), 2-ethylhexanoic acid tin(II) salt (Sn(Oct)₂; Sigma-Aldrich, St. Louis, MO, USA, purity ≥95%), 4,4′-Azobis(4-cyanovaleric acid) (ACVA; Sigma-Aldrich, purity ≥ 98%), 4-Cyano-4-(phenylcarbonothioylthio)pentanoic acid (CPA; Sigma-Aldrich, purity ≥ 97%), poly(ethylene glycol) methyl ether methacrylate (PEGMA; Sigma-Aldrich, M_n 950 Da), Tween80 (Sigma-Aldrich), Diethyl ether (DEE, Sigma-Aldrich, ≥99%), Deuterated chloroform (CDCl₃, Sigma-Aldrich, 99.8%), Ethanol (EtOH, Sigma-Aldrich, 99.8%), acetonitrile (ACN, Sigma-Aldrich, 99.9%), 6-hydroxycaproic acid (HCA, ABCR, Karlsruhe, Germany, 95%) were used as received without further treatments. The cell medium is composed by high glucose DMEM/F12 (Biowest, Nuaillé, France) supplemented with 10% fetal bovine serum (Lonza, Basel, Switzerland). Phosphate-buffered saline solution (PBS) was purchased from Sigma-Aldrich. For gel permeation chromatography (SEC) analysis Tetrahydrofuran (THF, Sigma-Aldrich, purity ≥ 99.7%) was used as eluent.

Gatti S., Agostini A., Ferrari R, & Moscatelli D. (2017). Synthesis and Nanoprecipitation of HEMA-CLn Based Polymers for the Production of Biodegradable Nanoparticles. Polymers, 9(9), 389.

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Perovskite Solar Cell Fabrication

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Lead
iodide (PbI₂, TCI), lead
bromide (PbBr₂, TCI), formamidinium iodide (FAI, Greatcell
Solar Materials), methylammonium bromide (MABr, Greatcell Solar Materials), n-hexyl trimethylammonium bromide (HTABr, Greatcell Solar
Materials), polyethylenoxide (PEO, Sigma-Aldrich), methylammonium
chloride (MACl, Sigma-Aldrich), spiro-OMeTAD (Luminescence Technology
corp.), FK209 (Luminescence Technology corp.), creatine (Sigma-Aldrich),
hydriodic acid (Alfa Aesar), SnO₂ colloidal solution (Alfa
Aesar), dimethylformamide (DMF, Sigma-Aldrich), dimethyl sulfoxide
(DMSO, Sigma-Aldrich), isopropyl alcohol (IPA, Sigma-Aldrich), chlorobenzene
(CB, Sigma-Aldrich), diethyl ether (DEE, Sigma-Aldrich), acetone (Sigma-Aldrich),
and ethanol (Sigma-Aldrich)

Kim G.W., Min J., Park T, & Petrozza A. (2022). Defect Passivation through (α-Methylguanido)acetic Acid in Perovskite Solar Cell for High Operational Stability. ACS Applied Materials & Interfaces, 14(18), 20848-20855.

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Synthesis and Characterization of Functional Polymers

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Acrylic acid (AA, 99%, anhydrous, Sigma-Aldrich), acetonitrile (ACN, 99.8%, Sigma-Aldrich), 4-methoxyphenol (MEHQ, 99%, Sigma-Aldrich), diethyl ether (DEE, >98%, Sigma-Aldrich), ethanol (>99.8%, Sigma-Aldrich), 1,4-dioxane (>99%, Sigma-Aldrich), Luperox® TBH70X tertbutyl hydroperoxide solution (tBuOOH, 70% wt.% in H2O, Sigma-Aldrich), L-ascorbic acid (AsAc, Sigma Aldrich), 2-methoxyethylamine (MeOEtNH2, 99%, Sigmal-Aldrich), poly(ethylene glycol) methyl ether acrylate (Sigma-Aldrich), 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4methylmorpholinium chloride (DMTMM-HCl, >96%, Sigma-Aldrich) and 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium tetrafluoroborate (DMTMM-BF4, 97%, Sigma Aldrich) were used as purchased without further purification. 2-Methyl-2-oxazoline (MeOx, 98%, Sigma-Aldrich) was distilled to dryness over barium oxide (BaO) and stored in a nitrogen atmosphere.
The chain transfer agent (CTA), 2-(((butylthio)-carbonothioyl)thio)-propanoic acid was prepared according to a literature procedure. 35 Amine-terminated poly(2-ethyl-2-oxazoline) (PEtOxNH2) was synthesized following a literature procedure. 36 2-(pyridyldithio)-ethylamine hydrochloride (PDS) was obtained from Speed Chemical, China. Cyanine5 amine was purchased from Lumiprobe. CellLight™ ER-GFP, BacMam 2.0 and CellLight™ Golgi-GFP, BacMam 2.0 were purchased from Thermo Fisher Scientific.

Mahmoud A.M., de Jongh P.A.J.M., Briere S., Chen M., Nowell C.J., Johnston A.P.R., Davis T.P., Haddleton D.M, & Kempe K. (2019). Carboxylated Cy5-Labeled Comb Polymers Passively Diffuse the Cell Membrane and Target Mitochondria. ACS applied materials & interfaces, 11(34).

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