Titanium 3 chloride

Manufactured by Merck Group

Sourced in United States

Titanium (III) chloride is an inorganic compound with the chemical formula TiCl3. It is a gray-black crystalline solid that is widely used in various industrial and research applications. The core function of Titanium (III) chloride is as a reducing agent and a precursor for other titanium compounds.

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Titanium chloride (2 citations)

4 protocols using titanium 3 chloride

Chlordecone and Related Compounds Analysis

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Chlordecone was obtained from Azur Isotopes (purity 98%). Chemical products used for microbiological media, vitamin B₁₂ (>98%), chloro(pyridine)cobaloxime(III), lindane (97%), 1,3-di chlorobenzene (98%), 1,4-di chlorobenzene (99%), chlorobenzene (99.8%), and benzene (99.8%) were obtained from Sigma Aldrich. Titanium (III) citrate was prepared from titanium (III) chloride (>12% in HCl; Sigma Aldrich) and sodium citrate and neutralized with Na₂CO₃ (Chevallier et al., 2019 (link)). Dichloromethane (HPLC grade) was obtained from Fisher Chemical.

Barbance A., Della-Negra O., Chaussonnerie S., Delmas V., Muselet D., Ugarte E., Saaidi P.L., Weissenbach J., Fischer C., Le Paslier D, & Fonknechten N. (2020). Genetic Analysis of Citrobacter sp.86 Reveals Involvement of Corrinoids in Chlordecone and Lindane Biotransformations. Frontiers in Microbiology, 11, 590061.

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Chlordecone Degradation Protocol

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Chlordecone was obtained from Azur Isotopes (purity 98%). Na₂S (≥ 98%), pyridine (99.8%), iodomethane (> 99%) and phosphorus pentasulfide (99%) were purchased from Sigma Aldrich. Titanium (III) citrate was prepared from titanium (III) chloride (> 12% in HCl) (Sigma Aldrich) and sodium citrate and neutralized with Na₂CO₃. Dichloromethane (DCM) and pentane (HPLC grade) were obtained from Fisher Chemical; cyclohexane (99.8%) and NMR solvents from Acros Organics; and acetonitrile (MeCN, LC-HRMS grade) and acetone (> 99.9%) from VWR Chemicals. Chemical products used for microbiological media were obtained from Sigma Aldrich. Chemicals and media used for chlordecone TPs are described elsewhere^{6 (link)}.

Della-Negra O., Chaussonnerie S., Fonknechten N., Barbance A., Muselet D., Martin D.E., Fouteau S., Fischer C., Saaidi P.L, & Le Paslier D. (2020). Transformation of the recalcitrant pesticide chlordecone by Desulfovibrio sp.86 with a switch from ring-opening dechlorination to reductive sulfidation activity. Scientific Reports, 10, 13545.

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Colorimetric Determination of Molybdenum

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The starting materials, including commercially available ammonium molybdate tetrahydrate (AMT: (NH₄)₆Mo₇O₂₄·4H₂O; 99.9%), ammonium oxalate (C₂H₈N₂O₄; 99.5%), ascorbic acid (HC₆H₇O₆; 99%), titanium(iii) chloride (TiCl₃; 99%), sodium lauryl sulfate (SLS: NaC₁₂H₂₅SO₄; 99%), ethanol (C₂H₅OH; 99.9%) and methyl orange (C₁₄H₁₄N₃NaO₃S; 85%), were obtained from Sigma-Aldrich (Missouri, United States). Double distilled water (DIW) was used for sample preparation.

El-Sawaf A.K., Nassar A.A., Tolan D.A., Ismael M., Alhindawy I., M. El-Desouky E., El-Nahas A., Shahien M, & Maize M. (2024). A mesoporous Mo and N Co-doped TiO2 nanocomposite with enhanced photocatalytic efficiency. RSC Advances, 14(5), 3536-3547.

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Synthesis and Detection of TiO2, ZnO, and Amoxicillin

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Titanium (III) chloride (> 15% TiCl₃ basis, 5–10% free acid as HCl, Sigma-Aldrich) was used in the synthesis of TiO₂. For ZnO synthesis, zinc chloride (> 98%, Merck) and NaOH (pellets > 97%, Merck) have been used. For rinsing the samples, isopropyl alcohol (> 99.8%, Merck) and double distilled water were used, the latter been prepared in the Research Laboratory at the chemical engineering Department of Amirkabir University of Technology. The Glutardialdehyde solution (25%, Merck), and GOx is gifted from Bonda Group Development. Glucose monohydrates has been employed as the substrate for GOx. The target water contaminant is Amoxicillin trihydrate, which is received from Afa Chimi. Sodium 1, 2-naphthoquinone-4-sulfonate (> 97%, Merck) acts as the chemical derivative chromogenic reagent, K₂HPO₄ (> 98%, Merck), and KH₂PO₄ (> 99.5%, Merck) for adjusting pH are used in the visible spectroscopic detection of amoxicillin. PDMS (Sylgard 184 Silicon Elastomer Kit, Dow Corning) is used in the microfabrication of the spiral chip.

Sohrabi S., Keshavarz Moraveji M., Iranshahi D, & Karimi A. (2022). Microfluidic assisted low-temperature and speedy synthesis of TiO2/ZnO/GOx with bio/photo active cites for amoxicillin degradation. Scientific Reports, 12, 15488.

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