PdCl2 (Silversalt, St. Petersburg, Russia, 98%), LiCl (TTX, Sergiev Posad, Russia, 98+), isopropanol (IPA, 99.5+%, Acros, Fair Lawn, NJ, USA), tetramethylorthosilicate (TMOS, Acros, 99%), (3-aminopropyl)trimethoxysilane (APTMS, Acros, 95%), N-(2-aminoethyl)-3-(trimethoxysilyl)propylamine (AEAPTMS, Sigma-Aldrich, St. Louis, MO, USA, 97%), (S)-(+)-2-phenylglycine methyl ester hydrochloride (Acros, 97%), L-phenylalanine methyl ester hydrochloride (Acros, 98%), methanol (Acros, 99.9%), hexene-1 (Acros, 97%), benzene (Sigma-Aldrich, 99.8%), acetophenone (Acros, 98%), benzaldehyde (Acros, 98+%), benzophenone (Acros, 99%), hexyne-1 (Acros, 98%), dicyclopentadiene (Merck, Darmstadt, Germany, 98%), cyclohexanone (Acros, 99.8%) and 1,4–dioxane (Acros, 99+%) were used without further purification. Lithium tetrachloropalladate (II) was prepared by mixing 1 mol of PdCl2 and 2 mol of LiCl in methanol and stirring for 24 h at room temperature.
Tetramethylorthosilicate
Manufactured by Thermo Fisher Scientific
Sourced in United States
Tetramethylorthosilicate is a chemical compound with the formula Si(OCH3)4. It is a colorless, volatile liquid that is commonly used as a precursor in the synthesis of silicon-containing materials, such as silicon dioxide and silicon nitride, for various applications in the electronics and semiconductor industries.
Automatically generated - may contain errors
Lab products found in correlation
Acetophenone, by Thermo Fisher Scientific (1 mentions)
Benzophenone, by Thermo Fisher Scientific (1 mentions)
1 4 dioxane, by Thermo Fisher Scientific (1 mentions)
Aptms, by Thermo Fisher Scientific (1 mentions)
3 aminopropyl trimethoxysilane, by Thermo Fisher Scientific (1 mentions)
Methanol, by Thermo Fisher Scientific (1 mentions)
Benzaldehyde, by Thermo Fisher Scientific (1 mentions)
Cyclohexanone, by Thermo Fisher Scientific (1 mentions)
3 aminopropyltrimethoxysilane, by Merck Group (1 mentions)
Benzaldehyde, by Merck Group (1 mentions)
Ethanol, by Thermo Fisher Scientific (1 mentions)
Urea, by Merck Group (1 mentions)
Ethyl cyanoacetate, by Merck Group (1 mentions)
Dry toluene, by Thermo Fisher Scientific (1 mentions)
Acetic acid, by Carl Roth (1 mentions)
Acetylacetone, by Merck Group (1 mentions)
Yttrium nitrate hexahydrate, by Merck Group (1 mentions)
Zirconium propoxide, by Merck Group (1 mentions)
3 protocols using tetramethylorthosilicate
1
Synthesis and Characterization of Silica-based Materials
2
Synthesis of Functionalized Silica Materials
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Tetramethyl orthosilicate
(TMOS, 99%), dry Ethanol (99.5%, extradry, absolute), and dry toluene
(99.85%, extradry over a molecular sieve) were purchased from Acros
Organics. Poly(ethylene glycol) (PEG, Mn = 10 000) was purchased from Fluka. Ethanol (99.8%) was purchased
from Fisher Chemicals. Urea (≥99.5%) and (3-aminopropyl)trimethoxysilane
(APTMS, 97%) were purchased from Sigma-Aldrich. Acetic acid (100%)
was purchased from Carl Roth. MEthanol (≥99.85%) was purchased
from Chemsolute. Benzaldehyde (purified by redistillation, ≥99.5%),
ethyl cyanoacetate (≥98%), p-chloroBenzaldehyde
(97%), p-tolualdehyde (97%), and biphenyl-4-carboxaldehyde
(99%) were purchased from Aldrich. p-Anisaldehyde
was purchased from TCI. PEEK tubes (1/4 in. outer diameter ×
3.17 mm inner diameter, 50 cm length) were purchased from BGB Analytik.
PTFE shrink tubes (shrink rate 4:1) were purchased from AUTEC GmbH.
All chemicals were used without further purification.
(TMOS, 99%), dry Ethanol (99.5%, extradry, absolute), and dry toluene
(99.85%, extradry over a molecular sieve) were purchased from Acros
Organics. Poly(ethylene glycol) (PEG, Mn = 10 000) was purchased from Fluka. Ethanol (99.8%) was purchased
from Fisher Chemicals. Urea (≥99.5%) and (3-aminopropyl)trimethoxysilane
(APTMS, 97%) were purchased from Sigma-Aldrich. Acetic acid (100%)
was purchased from Carl Roth. MEthanol (≥99.85%) was purchased
from Chemsolute. Benzaldehyde (purified by redistillation, ≥99.5%),
ethyl cyanoacetate (≥98%), p-chloroBenzaldehyde
(97%), p-tolualdehyde (97%), and biphenyl-4-carboxaldehyde
(99%) were purchased from Aldrich. p-Anisaldehyde
was purchased from TCI. PEEK tubes (1/4 in. outer diameter ×
3.17 mm inner diameter, 50 cm length) were purchased from BGB Analytik.
PTFE shrink tubes (shrink rate 4:1) were purchased from AUTEC GmbH.
All chemicals were used without further purification.
3
Synthesis of Yttrium-Zirconium-Silicate Compounds
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Yttrium nitrate hexahydrate (99%) and acetylacetone (AcAc, 99.5%) were purchased from Sigma-Aldrich Inc. (St. Louis, MO, USA); zirconium propoxide (ZIP, 70% sol. in 1-propanol), lithium methoxide (LiOMe, 2.2M sol. in methanol), and tetramethyl orthosilicate (TMOS 99%) were purchased from Acros Organics (Acros Organics™, Thermo Fisher Scientific, Waltham, MA, USA). All reagents were used as received. Methanol, ethanol, and isopropanol were kept on 3A molecular sieves for 48 h and further distilled under dry nitrogen.
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