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2 protocols using sodium bicarbonate

1

Synthesis of Polyurethane-Based Composites

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Guanidine carbonate, ethyl acetoacetate, alpha-acetyl-gamma-butyrolactone, triethylamine, ethylene glycol monoallyl ether, 1-thioglycerol, 2,2-dimethoxy-2-phenylacetophenone, hexamethylene diisocyanate, polytetramethylene ether glycol (PTMEG, Mn = ∼1000 g mol−1), ditinbutyl dilaurate (DBTDL) were purchased from Aladdin Chemistry Regent Co., Ltd (China). Triethylene glycol bis(3-tert-butyl-4-hydroxy-5-methylphenyl)propionate (AO-70) was obtained from Beijing Additive Research Institute (China). Hydroxyl groups modified multi-walled carbon nanotubes (MWCNTs-OH) with hydroxyl content of 1.85 wt% was purchased from Chengdu Organic Chemicals Co. Ltd (China). 4,4′-Dicyclohexylmethane diisocyanate (HMDI) was kindly provided by Wanhua Chemical Group Co., Ltd (China). Absolute alcohol, sodium hydroxide, dichloromethane, hydrochloric acid, p-toluene sulfonic acid, cyclohexane, sodium bicarbonate, tetrahydrofuran, anhydrous sodium sulfate, acetone, petroleum ether and dimethyl formamide (DMF) were purchased from Chengdu Kelong Chemical Reagent Co. Ltd (China). DMF was dehydrated with activated 4A molecular sieves for at least one week before use, the other reagents were used as received.
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2

Polyphenol-Aroma Compound Analysis Protocol

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The polyphenol additive, primary aroma component standard, C7–C40 normal paraffin standard and phenolic acid standard utilized in this investigation were procured from PtSrTi (Chongqing, China).
The high-activity dry yeast utilized for fruit wine production was procured from Angel Yeast (Angel Yeast, Yichang, China). Chemical reagents such as Pectinase 500 U/mg, potassium metabisulfite, 3,5-dinitrosalicylic acid, phenol, methanol (HPLC), acetonitrile (HPLC), and formic acid (HPLC) were obtained from Shanghai Yuanye Biotechnology Co., Ltd. (Shanghai, China). Additionally, sodium bicarbonate, sodium potassium tartrate, DPPH (2,20-azinobis (3-ethylbenzothiazoline-6-sulfonic acid)) and glucose were acquired from Chengdu Kelong Chemical Reagent Factory (Chengdu., China).
The ABTS Assay Kit was procured from Suzhou Keming Biotechnology Co., Ltd. (Suzhou, China). The FRAP Assay Kit was procured from Suzhou Greis Biotechnology Co., Ltd. (Suzhou, China).
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