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48 protocols using sodium chloride (nacl)

1

Quantitative Analysis of Pyrethrins

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Standard Pyrethrin II (w/w, 30%, technical Grade, contains Pyrethrin I) was obtained from Toronto Research Chemicals Inc. (Toronto, ON, Canada). Sodium chloride and anhydrous sodium sulfate were analytical reagent grade and purchased from Beijing Chemical Reagent Company (Beijing, China). Acetonitrile, acetone and n-hexane were both HPLC-grade and purchased from Fisher Scientific (Pittsburgh, PA, USA). Aquapro Ultrapure Water System supply ultrapure water. Florisil SPE cartridges (0.5 g/3 mL) were purchased from ANPEL (Shanghai, China). Stock standard solution of pyrethrins (1000 mg/L) was prepared in acetone and stored at −20 °C. Working standard solutions were prepared by dilution with acetone and stored at −20 °C.
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2

Fluoride Adsorption Optimization Protocol

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The chemicals used in this study were of analytical grade and did not require further purification. Nitric acid (HNO3), sodium hydroxide (NaOH), sodium fluoride (NaF), sodium nitrate (NaNO3), sodium chloride (NaCl), disodium hydrogen phosphate (Na2HPO4·12H2O), sodium sulfate (Na2SO4) and sodium carbonate (Na2CO3) were purchased from Beijing Chemical Factory. Zirconium oxychloride octahydrate (ZrOCl2·8H2O) was purchased from Tianjin Guangfu Fine Chemical Research Institute. The fluoride concentrations and pH values of the aqueous solutions were measured using a PF-1-C type fluoride ion selective electrode and a pH meter, respectively, which were purchased from Shanghai Yue-Ci Electronic Technology Co., Ltd. The morphologies and elemental compositions of the adsorbents were observed using a scanning electron microscope and energy dispersive spectrometer (ZEISS), and the composition of the functional group of the adsorbent was observed using a Fourier transform infrared spectrometer (IRTracer-100). The fluoride stock solution was prepared by dissolving 2.21 g of NaF in 1000 mL deionized water. In addition, other solutions of fluoride ions with different concentrations were prepared by diluting the stock solution.
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3

Goji Berry Wine Production Protocol

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Fully ripe goji berries (Lycium barbarum L.) were harvested in the Ningxia growing region (Yinchuan City, 106.27°E, 28.47°N) by Senmiao Corporation (Yinchuan, China) in the middle of July of 2015. The fresh goji berries were processed by Senmiao Corporation into dry goji berries through a hot-air drying process as well. Both fresh and the dry goji berries were used for the goji berry wine-making. A commercial Saccharomyces cerevisiae strain Red Fruit®, pectinase, and potassium metabisulfite were purchased from Enartis (San Martino, Trecate, Italy). Glycosidase AR 2000 was a product from DSM Food Specialties (Delft, The Netherlands). Deionized water was purified by a Milli-Q purification system (Millipore, Bedford, MA, USA). Sodium hydroxide, diammonium phosphate, sodium chloride, ammonium sulfate, sodium sulfate, tartaric acid, ethanol, and sucrose were purchased from Beijing Chemical Works (Beijing, China). The standards of volatiles were purchased from Sigma-Aldrich (St. Louis, MO, USA).
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4

Comprehensive Analysis of Volatile Compounds

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The standards of volatile compounds were purchased from Sigma-Aldrich (St. Louis, MO, USA), including isobutanol, 3-methyl-1-butanol, cis-3-hexen-1-ol, 1-hexanol, heptanol, octanol, phenethyl alcohol, 2,6-nonadien-1-ol, dodecanol, ethyl acetate, isoamyl acetate, ethyl lactate, ethyl hexanoate, ethyl octanoate, diethyl succinate, phenethyl acetate, ethyl decanoate, butanoic acid, hexanoic acid, octanoic acid, dodecanoic acid, octanal, (2e,6z)-2,6-nonadienal, benzaldehyde, furfural, citronellol, linalool, rose oxide, geraniol, nerol, β-damascenone, β-ionone, nerolidol, hexanal, guaiacol, 4-Ethylphenol, and 2-octanol which were used as the internal standard.
Folin–Ciocalteu reagent and sodium chloride were purchased from Beijing Chemical Works (Beijing, China). Potassium hydrogen tartrate were purchased at Kemiou Chemical Reagent Co. (Tianjin, China). Bovine serum albumin was obtained from Asahi Kasei Corporation (Tokyo, Japan). Deionized water (<18 MW resistance) was purified by using a Milli-Q purification system (Molecular, Chongqing, China). Bentonite, soybean protein and potassium metabisulfite were purchased from Lallemand Company (Lallemand, Toulouse, France).
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5

Halloysite-Supported Metal Nanoparticle Synthesis

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Halloysite mineral (HNT) was purchased from Zhengzhou Jinyangguang Ceramics Co. Ltd. Pristine HNT was cleaned with fresh water, dried in a freeze-drier, and then ground into fine powder in a mortar before use. Analytical grade chloroauric acid (HAuCl4), chloroplatinic acid hexahydrate (H2PtCl6·6H2O), silver nitrate (AgNO3), 4-nitrophenol (4-NP) and ascorbic acid (AA) were purchased from Sinopharm Chemical Reagent Co. Ltd. Sodium borohydride (NaBH4, AR) was purchased from Tianjin Fuchen Chemical Reagent Technologies Co. Ltd. Glucose (AR) was purchased from Tianjin Fengchuan Chemical Reagent Technologies Co. Ltd. Ammonium hydroxide (NH3·H2O, 25%), ethanol (AR), ethylene glycol (EG, AR), hydrogen peroxide (H2O2, 30%) and sodium chloride (AR) were purchased from Beijing Chemical Works. Polyvinylpyrrolidone (PVP, MW 58 000, AR) was purchased from Alfa Aesar. o-Phenylenediamine (OPD, 99.9%) was purchased from Sigma. All chemicals were used as received without further purification.
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6

Synthesis and Characterization of Photocatalysts

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Iron(II) chloride tetrhydrate (98%, Energy Chemical Ltd., Shanghai, China), 1,10-Phenanthroline (99%, J&K Scientific Ltd., Beijing, China), [Ru(bpy)3]Cl2·6H2O, 2-Phenylbenzimidazole (98%, J&K Scientific Ltd., Beijing, China), Iodomethane (97%, Ouhechem, Beijing, China), Sodium borohydride (99%, HuaDa, Guangdong, China). Sodium chloride, Sodium thiosulfate, Ethanol, Dichloromethane, Dithyl ether, N,N-Dimethylformamide, TriEthanolamine come from Beijing Chemical Works (Beijing, China), and were used as purchased, without further purification.
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7

Synthesis and Characterization of Cellulose-Based Composites

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All chemicals used here were of analytical grade and used as received without further purification. All experiments were operated under an ambient atmosphere. Microcrystalline cellulose (MCC, molecular weight of 34 843–38 894 degree of polymerization (DP, DP = 215–240)) of a commercial reagent was purchased from Sinopharm Group Chemical Reagent Co., Ltd. Poly(vinyl alcohol) (PVA, ∼88% hydrolyzed, DP = 1750 ± 50) was purchased from Sinopharm Chemical Reagent Co., Ltd. and poly(vinyl pyrrolidone) (PVP, K-30) was purchased from Xilong Chemical. Potassium dichromate (K2Cr2O7), sulfuric acid (98%), sodium hydroxide (NaOH), and sodium chloride (NaCl) were purchased from Beijing Chemical Works.
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8

Analysis of Goji Berry Pulp Compounds

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This study investigated a set of seven goji berry pulp products that are sold in the Chinese market. Table S1 shows the details of the experimental samples. Ethanol and dichloromethane of HPLC grade were purchased from Honeywell (Marris Township, NJ, USA). All analytical reagents, which included tartaric acid, sodium chloride (NaCl), sodium hydroxide (NaOH), and glucose, were purchased from Beijing Chemical Works (Beijing, China). An n-alkanes solution (C6–C24) was purchased from Supelco (Bellefonte, PA, USA). Table S2 lists the authentic flavor standards purchased commercially and used for qualitative and quantitative analysis of aroma-active compounds.
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9

Analytical and Chromatographic Purity Protocols

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Analytical purity: sulfuric acid, sodium chloride, potassium chloride, sodium bicarbonate (Beijing Chemical Factory, Beijing, China); tannic acid (Tianjin Guangfu Fine Chemical Research Institute, Tianjin, China); Folin-Denis reagent (US sigma, St. Louis, MO, USA); anhydrous sodium carbonate (Tianjin Hengxing Chemical Reagent Manufacturing Co., Ltd., Tianjin, China); glacial acetic acid, hydrochloric acid, anhydrous ethanol, sodium hydroxide, phosphoric acid (Beijing Chemical Factory); potassium hydrogen phthalate, anthrone (Sinopharm Chemical Reagent Co., Ltd., Shanghai, China); anhydrous sodium acetate (Shanghai Hutian Chemical Co., Ltd., Shanghai, China); glucose (Guangzhou Jinhuada Chemical Reagent Co., Ltd., Guangzhou, China).
Chromatographic purity: methanol (TEDIA Reagents, Fairfield, OH, USA); succinic acid, fumaric acid, malic acid, citric acid anhydrous (Shanghai Yuanye Biotechnology Co., Ltd., Shanghai, China); 4-methyl-2-pentanol (Shanghai Lianshuo Biotechnology Co., Ltd., Shanghai, China); glacial acetic acid, tartaric acid, lactic acid (Tianjin Fine Chemical Research Institute, Tianjin, China)
Fermentation auxiliaries: CEC01 active dry yeast (Angel Yeast Co., Ltd., Hubei, China); potassium metabisulphite (Yantai Dibs Homebrewer Co., Ltd., Yantai, China).
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10

Synthesis of Poly(p-methylstyrene) via CTAB-Mediated Anionic Polymerization

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Cumyl alcohol (CumOH, 97%), tris(pentafluorophenyl)boron (B(C6F5)3, 97%), lithium chloride (LiCl, 99%), cetyltrimethylammonium bromide (CTAB, 99%), sodium dodecyl benzene sulfonate (SDBS, 95%), polyoxyethylene mono-4-octylphenyl ether (NP-40) and tetrahydrofuran (THF, 99.8%) were purchased from J&K Scientific Ltd., Beijing, China, and used as received. Sodium chloride (NaCl, 99.5%) and diethyl ether (Et2O, 99.7%) were purchased from Beijing Chemical Works. Methanol (MeOH, 99.5%) and ethanol (EtOH, 99.5%) were purchased from Tianjin Guangfu Technology Development Co., Ltd, Tianjin, China, and used as received. Calcium hydride (CaH2, 97%) was from Shanghai Yien Chemical Technology Co., Ltd. p-Methylstyrene (p-MSt, J&K Scientific Ltd., Beijing, China, 98%) was vacuum distillation at 75 °C with CaH2 before use.
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