2,2'-diselenyldibenzoicacid (DSBA) was synthesized as reported in [3 (link)]. Purity >98.5%. Ebselen (E3520) and diphenyl-diselenide [(PhSe)2] (180629; purity 98%) were purchased from Sigma-Aldrich and all compounds were dissolved in DMSO as described in detail later (see section 2.3 and 2.4).
Diphenyl diselenide phse 2
Manufactured by Merck Group
Sourced in India
Diphenyl-diselenide [(PhSe)2] is a chemical compound used in various laboratory applications. It serves as a source of selenium and can be utilized in a range of experimental setups. The core function of this compound is to provide a reliable and controlled supply of selenium for research purposes.
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Lab products found in correlation
2 protocols using diphenyl diselenide phse 2
1
Synthesis and Purity of DSBA
2
Structural and Thermal Characterization of Pyrrole-Based Nanocomposites
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Pyrrole (Himedia,
India) was distilled and stored at −5 °C
prior to use. Diphenyl diselenide [(PhSe)2, Sigma Aldrich,
India], anhydrous ferric chloride (FeCl3, Fisher Scientific,
India), and chloroform (CHCl3, Fisher Scientific, India)
used were of analytical reagent grade. The structural characterization
of samples was performed by X-ray diffraction (XRD) using a PW 3050
diffractometer (Cu Kα radiation, λ = 1.5418 Å). Fourier
transform infrared spectroscopy (FTIR) was performed on a PerkinElmer
RX-1 FTIR spectrophotometer in the range of 4000–500 cm–1. The thermal properties were measured by thermogravimetric
analysis (TGA) performed on a SEIKO TG/DTA 6200 machine at a heating
rate of 10 °C/min under N2. Dielectric studies of
synthesized samples were performed using a computer-controlled LCR
meter analyzer (Model Agilent 4285). Particle size and morphology
of synthesized nanocomposites have been characterized by scanning
transmission electron microscopy (STEM, Hitachi H-9500).
India) was distilled and stored at −5 °C
prior to use. Diphenyl diselenide [(PhSe)2, Sigma Aldrich,
India], anhydrous ferric chloride (FeCl3, Fisher Scientific,
India), and chloroform (CHCl3, Fisher Scientific, India)
used were of analytical reagent grade. The structural characterization
of samples was performed by X-ray diffraction (XRD) using a PW 3050
diffractometer (Cu Kα radiation, λ = 1.5418 Å). Fourier
transform infrared spectroscopy (FTIR) was performed on a PerkinElmer
RX-1 FTIR spectrophotometer in the range of 4000–500 cm–1. The thermal properties were measured by thermogravimetric
analysis (TGA) performed on a SEIKO TG/DTA 6200 machine at a heating
rate of 10 °C/min under N2. Dielectric studies of
synthesized samples were performed using a computer-controlled LCR
meter analyzer (Model Agilent 4285). Particle size and morphology
of synthesized nanocomposites have been characterized by scanning
transmission electron microscopy (STEM, Hitachi H-9500).
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