XPS (Kratos AXIS 165 electron spectrometer, Japan) was employed to acquire quantitative information on the chemical species of the surface. XPS spectra were recorded with a Kratos AXIS 165 electron spectrometer (Japan) using monochromated Al Kα X-ray irradiation generated at 350 ​W. The standard take-off angle used for analysis was 45°, which produced a maximum analysis depth in the range of 3–5 ​nm. Low-resolution survey spectra were recorded in 0.5 ​eV steps with a 187.85 ​eV analyzer pass energy from 0 to 1400 ​eV. SEM images of the samples were recorded using a scanning electron microscope (Philips XL-30, Holland). The surface topography of each sample was determined using a D3000 AFM microscope with a Nanoscope IV controller (Agilent PicoPlus). The scanning area was 1.5 ​× ​1.5 ​μm to determine roughness on the nanoscale. Root mean square (RMS) roughness values were obtained as Rq using the instrument software NanoScope Analysis.
+ Open protocol