DSC and TGA were performed with a Mettler-Toledo TGA/DSC STARe system (Mettler, Switzerland) under an atmosphere of dry N2 flowing at 50 cm3 min−1. DSC was performed in the range 30–300°C at a rate of 10°C min−1; TGA was performed in the range 30–500°C at a rate of 10°C min−1. The TGA/DSC data were analysed using STARe software.
Tga dsc stare system
Manufactured by Mettler Toledo
Sourced in Switzerland, United States
The TGA/DSC STARe System is a thermal analysis instrument designed for simultaneous thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) measurements. It provides quantitative information about physical and chemical changes in materials as a function of temperature or time under a controlled atmosphere.
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Lab products found in correlation
6 protocols using tga dsc stare system
1
Thermal Analysis of Materials
2
Instrumental Analysis of Organic Compounds
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All reagents were purchased from Aldrich or Alfa Aesar and used as received. IR spectra were measured using PerkinElmer FT-IR spectrum 1000 instrument. Solid-state spectra were obtained by using a universal ATR sampling accessory. Gas-phase spectra were measured by using a purposely designed sample cell as previously described.[14b (link)] TGA and DSC data were obtained using a Mettler Toledo TGA-DSC STARe system. Elemental analyses were conducted by the Elemental Analysis Service in the Department of Chemistry at University of Sheffield.
3
Thermogravimetric Analysis of Suspensions
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The mass fractions of the suspensions were determined with a TGA/DSC STARe System from Mettler-Toledo GmbH. The samples were filled into 40 μL aluminum crucibles, heated in air at a rate of 10 °C min–1 to 120 °C and then kept at 120 °C for 2 h. The masses of initial dispersions and dried particles were measured with a precision of ca. 10–3 mg.
4
Thermogravimetric Analysis of Nanocomposite Residual Water
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TGA was carried out at 30–250 °C at the heating rate of 10 °C/min under nitrogen flow (20 mL/min) using the TGA/DSC STARe system (Mettler-Toledo, Inc, Columbus, OH, USA) for characterizing residual water in the nanocomposites.
5
Thermal Characterization of Materials
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Thermal characterization was carried out on a Mettler-Toledo TGA/DSC STARe System, from 25 to 800 o C at a heating rate of 10 o C min -1 , under constant flow of 60 mL/min of nitrogen. The TGA data were analysed using the Mettler-Toledo Star System SW 9.30.
6
Thermal Analysis of Materials
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Thermal analysis was carried out on a Mettler-Toledo TGA/DSC STARe System, from 25 to 800 °C at a heating rate of 10 °C/min, under a constant flow of 60 mL/min of nitrogen. The obtained TGA data were analysed using the Mettler-Toledo Star System SW 9.30.
Thermal characteristics of the materials studied were also obtained using a TA DSC 2010 apparatus (TA Instruments, New Castle, DE). The first calorimetric trace (I-scan, preliminary heating run) in which the thermal history was suppressed, were acquired from -80 °C to 200 °C at a heating rate of 20 °C/min, under a nitrogen atmosphere (flow rate = 50 mL/min). The instrument was calibrated with indium and gallium standards. The melting temperature (T m ) was taken as the peak maximum of the melting endotherm.
Thermal characteristics of the materials studied were also obtained using a TA DSC 2010 apparatus (TA Instruments, New Castle, DE). The first calorimetric trace (I-scan, preliminary heating run) in which the thermal history was suppressed, were acquired from -80 °C to 200 °C at a heating rate of 20 °C/min, under a nitrogen atmosphere (flow rate = 50 mL/min). The instrument was calibrated with indium and gallium standards. The melting temperature (T m ) was taken as the peak maximum of the melting endotherm.
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