The alternating aliphatic polyketone (PK30; CO, ethylene, propylene: 50, 30, and 20 mol %, respectively, MW = 2687 g/mol) was synthesized according to a reported procedure [40 ]. 2-thiophenemethylamine (TMA, pure), n-butylamine (nBuA, ≥99%), phenylethylamine (PEA, 99%), and 1-pyrenemethylamine hydrochloride (PMA, 95%) were purchased from Sigma-Aldrich (Darmstadt, Germany) and freshly distilled before use. Multi-walled carbon nanotubes (MWCNTs, Sigma-Aldrich, as-produced cathode deposit, >7.5% MWCNT basis, O.D. × L 7–15 nm × 0.5–10 μm) were used as an electrically conductive filler and used as received. Dimethylsulfoxide (DMSO, Acros, 99.7%), ammonia (Sigma-Aldrich, ca. 25), toluene (anhydrous, 99.8%, Sigma-Aldrich,), tetrahydrofuran (THF ≥ 99.9, Sigma-Aldrich), and methanol (Sigma-Aldrich, anhydrous, 99.8%) were used as received. Dimethyl sulfoxide-d6 (DMSO-d6, anhydrous, 99.9 atom % D, Sigma-Aldrich) was used as a deuterated solvent for 1H-NMR studies.
N butylamine
Manufactured by Merck Group
Sourced in United States, Germany
N-butylamine is a colorless, volatile liquid chemical compound. It is used as a building block in the synthesis of various organic compounds and as a chemical intermediate in the production of other substances. The core function of N-butylamine is to serve as a raw material for further chemical processes.
Automatically generated - may contain errors
Lab products found in correlation
Dimethyl sulfoxide (dmso), by Merck Group (4 mentions)
Sodium hydroxide (naoh), by Merck Group (4 mentions)
N n dimethylformamide (dmf), by Merck Group (4 mentions)
Acetonitrile, by Merck Group (4 mentions)
Hydrochloric acid (hcl), by Merck Group (4 mentions)
Triethylamine, by Merck Group (4 mentions)
Ethyl acetate, by Merck Group (3 mentions)
Pyridine, by Merck Group (3 mentions)
Dmso d6, by Merck Group (2 mentions)
Sodium alginate, by Merck Group (2 mentions)
Oleylamine, by Merck Group (2 mentions)
Ethanol, by Merck Group (2 mentions)
Hydrochloric acid (hcl), by Thermo Fisher Scientific (2 mentions)
Irgacure 369 1 369, by BASF (2 mentions)
Hexane, by Thermo Fisher Scientific (2 mentions)
N octylamine, by Merck Group (2 mentions)
Sodium bicarbonate, by Merck Group (2 mentions)
Cyclohexane, by Merck Group (2 mentions)
Chloroform, by Thermo Fisher Scientific (2 mentions)
2 mercaptoethanol, by Merck Group (2 mentions)
36 protocols using n butylamine
1
Synthesis and Characterization of PK30 Polyketone Composites
2
CCVD Synthesis of Carbon Nanotubes
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For the CCVD synthesis the following materials were used: n‐butylamine (Sigma Aldrich; as the carbon source), Ni(NO3)2×6H2O (Merck) and MgO (Sigma Aldrich) for preparation of CCVD catalyst. The purification of nanotubes was performed with 37 wt % cc. HCl (VWR). Nitric acid, 67 wt % (VWR) and sulfuric acid, 98 wt % (VWR) were used for functionalization of BCNTs. During of application gelled BCNT spheres sodium alginate (Sigma Aldrich) and CaCl2 (Merck) were used. The hydrogenation catalysts were synthetized from the following precursors: PdCl2 (Alfa Aesar), [(CH3CO2)2Rh]2 (Sigma Aldrich), Ni(NO3)2×6H2O (Merck).
3
Silane Coupling Agents and Surfactants in Materials Synthesis
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The following chemicals were used. Silane
coupling agents: (3-methacryloxypropyl)trimethoxysilane (MPTMS, ≥
98%, Sigma-Aldrich), octadecyltrimethoxysilane (OTMS, 90%, technical
grade, Aldrich), and (3-aminopropyl)triethoxysilane (APTES, ≥
98%, Sigma-Aldrich). Surfactants: Pluronic F108 block copolymer surfactant
(average mol. wt.: 14 600 g/mol, BASF), Igepal CO-520 (average
mol. wt.: 441 g/mol, Aldrich), and Triton X-100 (laboratory grade,
Sigma-Aldrich). Water was deionized with a Millipore Direct-Q UV3
reverse osmosis filter apparatus (Millipore Corporation) and had a
resistivity of at least 18.2 MΩ cm. Ethanol (absolute) was obtained
from Merck and 1-pentanol (ReagentPlus, ≥99%) from Sigma-Aldrich.
The catalysts aqueous ammonia (26.6 wt %), n-butylamine
(99.5 wt %), and sodium citrate dihydrate (p.a. ≥ 99.0%, anhydrous)
were purchased from Sigma-Aldrich. 2,2′-Azobis(2-methylpropionitrile)
(AIBN) initiator from Janssen Chimica was recrystallized from ethanol.
RAS (rhodamine isothiocyanate-aminostyrene) dye conjugate was prepared
as described in ref (36 (link)) and dissolved in acetone (99%, Merck) to a final concentration of
∼0.2 mg/mL. Fluoresceine isothiocyanate (FITC, ≥90 wt
% (HPLC)) was purchased from Sigma-Aldrich, as was polyvinylpyrrolidone
(PVP, K-30, 40 000 g/mol). All chemicals were used as received.
coupling agents: (3-methacryloxypropyl)trimethoxysilane (MPTMS, ≥
98%, Sigma-Aldrich), octadecyltrimethoxysilane (OTMS, 90%, technical
grade, Aldrich), and (3-aminopropyl)triethoxysilane (APTES, ≥
98%, Sigma-Aldrich). Surfactants: Pluronic F108 block copolymer surfactant
(average mol. wt.: 14 600 g/mol, BASF), Igepal CO-520 (average
mol. wt.: 441 g/mol, Aldrich), and Triton X-100 (laboratory grade,
Sigma-Aldrich). Water was deionized with a Millipore Direct-Q UV3
reverse osmosis filter apparatus (Millipore Corporation) and had a
resistivity of at least 18.2 MΩ cm. Ethanol (absolute) was obtained
from Merck and 1-pentanol (ReagentPlus, ≥99%) from Sigma-Aldrich.
The catalysts aqueous ammonia (26.6 wt %), n-butylamine
(99.5 wt %), and sodium citrate dihydrate (p.a. ≥ 99.0%, anhydrous)
were purchased from Sigma-Aldrich. 2,2′-Azobis(2-methylpropionitrile)
(AIBN) initiator from Janssen Chimica was recrystallized from ethanol.
RAS (rhodamine isothiocyanate-aminostyrene) dye conjugate was prepared
as described in ref (36 (link)) and dissolved in acetone (99%, Merck) to a final concentration of
∼0.2 mg/mL. Fluoresceine isothiocyanate (FITC, ≥90 wt
% (HPLC)) was purchased from Sigma-Aldrich, as was polyvinylpyrrolidone
(PVP, K-30, 40 000 g/mol). All chemicals were used as received.
4
Synthesis of Metallic Catalysts for Fuel Cells
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Oleylamine (Sigma-Aldrich, 70%), oleic acid (Sigma-Aldrich, 90%), Pt(acac)2 (Aladdin, 95%), CuCl (Sigma-Aldrich, 97%), W(CO)6 (Strem, 99% (<0.3% Mo)), Nafion (Sigma-Aldrich, 5 wt%), and n-butylamine (Sigma-Aldrich, 99%) were all used. Carbon black 350G was obtained from Keqing Corporation. The commercial Pt/C catalyst (10 wt% and 20 wt% loading) was obtained from Dalian Trico Chemical Co. Ltd. All reagents were of analytical grade and used without further purification.
5
Hybrid Perovskite Materials Synthesis
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Methylammonium chloride (MACl), 50% aqueous
H3PO2, lead oxide (PbO, 99.999%), phenethylamine
(99%), n-butylamine (>99%), 57% stabilized hydroiodic
acid (HI), lead iodide (PbI2, 98%), dimethyl sulfoxide
(DMSO, anhydrous), n-butylammonium bromide
((BA)Br, ≥98%)), phenethylammonium bromide ((PEA)Br,
≥98%), and lead bromide (PbBr2, ≥98%) were
purchased from Sigma-Aldrich.
H3PO2, lead oxide (PbO, 99.999%), phenethylamine
(99%), n-butylamine (>99%), 57% stabilized hydroiodic
acid (HI), lead iodide (PbI2, 98%), dimethyl sulfoxide
(DMSO, anhydrous), n-butylammonium bromide
((BA)Br, ≥98%)), phenethylammonium bromide ((PEA)Br,
≥98%), and lead bromide (PbBr2, ≥98%) were
purchased from Sigma-Aldrich.
6
Synthesis of Metal-Organic Frameworks
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Ferric
nitrate pentahydrate
[Fe (NO3)3·9H2O, 99%] and cobalt
nitrate hexahydrate [Co (NO3)2·6H2O, 99% %] were obtained from Sigma-Aldrich. Terephthalic acid (1,4-BDC,
99%) was supplied from Sigma-Aldrich. N,N-Dimethylformamide (DMF, 99.5%), ethanol (99.5%), N-butylamine, acetonitrile, lead nitrate, cadmium chloride, β-naphthol
benzaldehyde, HNO3, and NaOH were supplied from Sigma-Aldrich
and used as received.
nitrate pentahydrate
[Fe (NO3)3·9H2O, 99%] and cobalt
nitrate hexahydrate [Co (NO3)2·6H2O, 99% %] were obtained from Sigma-Aldrich. Terephthalic acid (1,4-BDC,
99%) was supplied from Sigma-Aldrich. N,N-Dimethylformamide (DMF, 99.5%), ethanol (99.5%), N-butylamine, acetonitrile, lead nitrate, cadmium chloride, β-naphthol
benzaldehyde, HNO3, and NaOH were supplied from Sigma-Aldrich
and used as received.
7
Lead-based Perovskite Synthesis
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Lead(II) oxide (>99.0%), hydroiodic acid (57%), hypo‐phosphorous acid solution (50 wt%), and n‐butylamine (99.5%) were obtained from Sigma‐Aldrich. Methylammonium iodide (99.5%) was obtained from MACKLIN. All the chemicals were used as received.
8
Synthesis of Kaolin-Based Material
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Kaolin (Riedel de Haen, pro analysi), diatomaceous earth (Murmuntani zone in the locality of Llica, Potosi, Bolivia), sodium hydroxide (Sigma Aldrich, reagent grade, ≥98%, anhydrous pellets), n-butylamine (Sigma Aldrich, 99.5%) and hydrochloric acid (Merk, pro analysi 37%) were used as reagents.
9
Amine Synthesis and Purification Protocol
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Ethylamine (70% in methanol), n-butylamine (99.5%), hexylamine (99%), octylamine (99%), nitric acid (70%), ethanol (99.5%), 1-hexanol (99%), and lysozyme from chicken egg white powder (E.C. 3.2.1.17; product code L6878) were obtained commercially from Sigma Aldrich (Burlington, MA, USA). All were used as received.
10
Chitosan-based Antibiotic Drug Delivery
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In this study, we used crab shell chitosan (Bioprogress, Shchyolkovo, Russia) with a viscosity-average molecular weight (MW) of 3.7 × 104 (L ) and a degree of acetylation of 26%, viscosity-average molecular weight (MW) of 6.9 × 104 (M ) and a degree of acetylation of 28% and viscosity-average molecular weight (MW) of 17.8 × 104 (H ) and a degree of acetylation of 24%, ciprofloxacin, n-butylamine, DCC (N,N′-dicyclohexylcarbodiimide), NHS (N-hydroxysuccinimide), hydrazine, glyoxal, TPP (sodium tripolyphosphate) (Sigma Aldrich, Burlington, MA, USA). Other chemicals and solvents were obtained from commercial sources and used as received without further purification.
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