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2 protocols using 2 methyl 1 butanol

1

GC-FID and GC-MS Analysis of Volatile Compounds

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Anhydrous sodium sulfate was purchased from AppliChem GmbH (Darmstad, Germany); dichloromethane (99.9%) was supplied by Honeywell Riedel-de Haën (Steinheim, Germany) and silanized glass wool by Supelco (Steinheim, Germany). 2-Octanol (≥99.5%), used as an internal standard was purchased from Sigma-Aldrich (St. Louis, MO, USA).
GC-FID and GC-MS used standards: acetic acid was purchased from Riedel-de-Haen (Seelze, Germany); isobutanol, 2-methyl-1-butanol, 3-methyl-1-butanol,benzyl alcohol, 2-phenylethanol,propanoic acid, butanoic acid, isovaleric acid, octanoic acid, hexanal, ethyl propanoate, isobutyl acetate, ethyl 2-methylbutyrate, ethyl hexanoate, ethyl decanoate, phenethyl acetate, ethyl dodecanoate, eugenol were acquired from Fluka (Buchs, Switzerland);1-propanol, 2,3-butanediol, 1,2-propanediol, glycerol, isobutyric acid, ethyl butyrate, ethyl octanoate were purchased from Merck (Darmstadt, Germany); e-ethoxy-1-propanol, methional, ethyl isobutyrate, ethyl isovalerate, isoamyl acetate, ethyl hydrogen succinate, furfural were bought from Aldrich (Steinheim, Germany) and 2,3 butanedione was acquired from Sigma-Aldrich (Saint Louis, MO, USA).
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2

GC-FID Analysis of Volatile Compounds

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Ethanol [CAS N°64-17-5; purity P 99.9] and mEthanol for GC-FID [CAS N°67-56-1; purity P 99.9%] were purchased from Merck (Darmstadt, Germany). Ethyl acetate [CAS N°141-78-6; purity P 99.8%] was purchased from Riedel-de-Haen (Seelze, Germany), 2-methyl-1-butanol [CAS N°34713-94-5; purity P 98%] 3methyl-1-butanol [CAS N°123-51-3; purity P 98.5%], 1-butanol [CAS N°71-36-3; purity P 99.5%], 2-methyl-1-propanol [CAS N°7
8-83-1; purity P 99.5%], 1-propanol [CAS N°71-23-8; purity P 99.5%], 2-butanol [CAS N°78-92-2; purity P 99.5%] and acetaldehyde [CAS N°75-07-0; purity P 99.5%] were purchased from Fluka (Buchs, Switzerland). The internal standard for GC-FID, 4-methyl-2-pentanol [CAS N°108-11-2; purity P 98] was purchased from Aldrich, supplied by Sigma-Aldrich (Zwijndrecht, Netherlands). Distilled water was used to prepare the hydro alcoholic solutions.
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