Raman measurements were recorded at a wavelength of 514.5 nm using confocal Raman microscope by Renishaw (In Via Raman). TEM analyses of the samples were done using a JEOL JEM-2100 model. The fluorescent study was carried out with an RF-5301 PC, Shimadzu fluorescence spectrometer. Functional groups were qualitatively identified by a Fourier transform infrared spectrometer (Thermo Nicolet 370 spectrophotometer). Atomic force microscope (Witec Alpha 300RA) was used for the height profile analysis. The UV/Vis spectrometer (Ocean optics JAZ series) was used for acquiring absorption spectra. The CHNS analysis was carried out using Elementar Vario EL111 elemental analyzer.
Fluorescence spectrometer
Manufactured by Shimadzu
The Fluorescence Spectrometer is an analytical instrument used to measure the intensity and wavelength distribution of fluorescent radiation from a sample. It functions by exciting the sample with a beam of light and detecting the emitted fluorescence, providing data on the sample's molecular structure and composition.
Automatically generated - may contain errors
Lab products found in correlation
Rf 5301pc, by Shimadzu (1 mentions)
Model jem 2100, by JEOL (1 mentions)
Nicolet 370 spectrophotometer, by Thermo Fisher Scientific (1 mentions)
Jaz series, by OceanOptics (1 mentions)
Alpha300ra, by WITec (1 mentions)
1600 ft ir spectrometer, by PerkinElmer (1 mentions)
Rf 6000, by Shimadzu (1 mentions)
X ray diffractometer, by Malvern Panalytical (1 mentions)
Uv vis spectrophotometer, by Shimadzu (1 mentions)
4 protocols using fluorescence spectrometer
1
Multimodal Characterization of Nanomaterials
2
Synthesis and Characterization of FR-P Ligand
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All starting
materials and solvents were commercially available and utilized without
further purification. Stock solutions ofFR -P and all metal salts were prepared in DMF and distilled water, respectively. 1H NMR and 13C NMR spectra were obtained using BRUKER
ADVANCE 300/400 spectrometers (CDCl3, TMS as an internal
standard). FT-IR spectra (KBr pellets) were recorded in the range
of 400–4000 cm–1 with a PerkinElmer 1600
FT-IR spectrometer. Electrospray ionization mass spectra (ESI-MS)
were obtained using a maXis UHR-TOF system. Melting points were measured
using a Yanaco MP-500 micromelting point instrument and uncorrected.
UV–vis spectra were recorded using a TU-1900 UV–vis
spectrometer. Fluorescence spectra were measured using an RF-6000
Shimadzu fluorescence spectrometer. Electrochemical analyses were
carried out using a CHI660 electrochemical analyzer.
materials and solvents were commercially available and utilized without
further purification. Stock solutions of
ADVANCE 300/400 spectrometers (CDCl3, TMS as an internal
standard). FT-IR spectra (KBr pellets) were recorded in the range
of 400–4000 cm–1 with a PerkinElmer 1600
FT-IR spectrometer. Electrospray ionization mass spectra (ESI-MS)
were obtained using a maXis UHR-TOF system. Melting points were measured
using a Yanaco MP-500 micromelting point instrument and uncorrected.
UV–vis spectra were recorded using a TU-1900 UV–vis
spectrometer. Fluorescence spectra were measured using an RF-6000
Shimadzu fluorescence spectrometer. Electrochemical analyses were
carried out using a CHI660 electrochemical analyzer.
3
Spectroscopic and Microscopic Analysis
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The instruments
used were fluorescence spectrometer (Shimadzu), X-ray photoelectron
spectrum analyzer (Shimadzu), X-ray diffractometer (malvernpanalytical),
and transmission electron microscope (FEI).
used were fluorescence spectrometer (Shimadzu), X-ray photoelectron
spectrum analyzer (Shimadzu), X-ray diffractometer (malvernpanalytical),
and transmission electron microscope (FEI).
4
Characterization of CeONR Nanorods
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The prepared CeONR and CeONR@PDA-Gal/Hyp were dispersed into PBS (pH 7.5, 10 mM) via ultrasonication. The suspension was dropped onto a copper mesh. The size and morphology of the nanorods were observed by a TEM. The Zeta potential of the nanorods was measured by using a dynamic light scattering (DLS) instrument. The UV-Vis absorption spectra were recorded using a Shimadzu UV-Vis spectrophotometer. The fluorescence spectra were recorded using a Shimadzu fluorescence spectrometer. The Fourier transform infrared (FT-IR) spectra were taken using an FT-IR instrument.
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