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Tris trimethylsilyl phosphine

Manufactured by Strem Chemicals
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Tris(trimethylsilyl)-phosphine is a colorless, air-sensitive, and pyrophoric liquid chemical compound. It has the molecular formula P(SiMe3)3. The compound is commonly used as a precursor for the synthesis of other organophosphorus compounds.

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Lab products found in correlation

Oleic acid, by Merck Group (3 mentions) Palmitic acid, by Merck Group (2 mentions) 1 octadecene, by Merck Group (2 mentions) Indium acetate, by Merck Group (2 mentions) Sulfur, by Merck Group (1 mentions) Butylamine, by Merck Group (1 mentions) Zn ac 2, by Merck Group (1 mentions) Trioctylphosphine top, by Merck Group (1 mentions) Oleic acid oa, by Merck Group (1 mentions) 1 octadecene ode, by Merck Group (1 mentions) Palmitic acid pa, by Tokyo Chemical Industry (1 mentions) Tetramethylammonium hydroxide, by Merck Group (1 mentions) Anhydrous zinc acetate, by Merck Group (1 mentions) Dimethyl sulfoxide (dmso), by Merck Group (1 mentions) Ethanol, by Thermo Fisher Scientific (1 mentions) Ethyl acetate, by Thermo Fisher Scientific (1 mentions) Zinc stearate, by Merck Group (1 mentions) Selenium powder, by Merck Group (1 mentions) Sulfur powder, by Merck Group (1 mentions) Octane, by Thermo Fisher Scientific (1 mentions)

4 protocols using tris trimethylsilyl phosphine

1

Synthesis and Characterization of Colloidal Quantum Dots

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Indium(iii) acetate [In(Ac)3, 99.99%, Aldrich], zinc acetate [Zn(Ac)2, 99.99%, Aldrich], zinc oxide (ZnO, 99.999%, Aldrich), 1-octadecene (ODE, 90%, Aldrich), sulfur (99.98%, Aldrich), butylamine (99.5%, Aldrich), N,N-dimethylformamide (DMF, anhydrous, 99.8%, Aldrich) oleic acid (OA, 90%, Aldrich), trioctylphosphine (TOP, 97%, Aldrich), 1-dodecanethiol (DDT, >98%, Aldrich), tris(trimethylsilyl)-phosphine [(TMS)3P, 98% Strem Chemicals], palmitic acid (PA, 98%, Tokyo Chemical Industry), n-octylamine (OAm, 98%, Tokyo Chemical Industry), 6-mercapto-1-hexanol (MCH, 97%, Aldrich), and aluminium-doped zinc oxide ink (conductivity: 10−3–10−4 S cm−1, viscosity < 4 mPa s, Aldrich) were used without further purification. Aluminium (Al) wires were purchased from the Nilaco Corporation (Japan). The purity of argon gas was 99.999%. Using an oil rotary vacuum pump, the vacuum conditions of less than 60 Pa were used for degassing and argon gas purge.
Nemoto K., Watanabe J., Yamada H., Sun H.T, & Shirahata N. (2023). Impact of coherent core/shell architecture on fast response in InP-based quantum dot photodiodes. Nanoscale Advances, 5(3), 907-915.
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2

Synthesis of Colloidal Quantum Dots

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Indium (III) acetate (99.999%), palmitic acid (98%, PA), zinc stearate (10% Zn basis), 1‐octadecene (90%, ODE), oleic acid (90%, OA), selenium powder (99.99%), sulfur powder (99.998%), PVP, Tetramethylammonium hydroxide (≥97%, TMAH), anhydrous zinc acetate (99.99%), and dimethyl sulfoxide (≥99.9%, DMSO) were purchased from Sigma‐Aldrich. Tris(trimethylsilyl)‐phosphine (98%, (TMS)3P) and trioctylphosphine (97%, TOP) were purchased from Strem Chemicals. Poly[(9,9‐dioctylfluorenyl‐2,7‐diyl)‐alt‐(4,4′‐(N‐(4‐butylphenyl) (TFB) was purchased from Xi'an Polymer Light Technology Corp. Acetone (extra dry, >99%), ethanol (extra dry, >99%), ethyl acetate (extra dry, >99%), and octane (extra dry, >99%) were purchased from Acros. All chemicals were used without further purification.
Wu Q., Cao F., Wang S., Wang Y., Sun Z., Feng J., Liu Y., Wang L., Cao Q., Li Y., Wei B., Wong W, & Yang X. (2022). Quasi‐Shell‐Growth Strategy Achieves Stable and Efficient Green InP Quantum Dot Light‐Emitting Diodes. Advanced Science, 9(21), 2200959.
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3

Synthesis of Semiconductor Nanocrystals

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cadmium oxide (99.99%), oleic acid (technical grade, 90%), and n-hexadecane (99%) were purchased from Sigma Aldrich and used as received. Indium acetate (99.99%), diethyl zinc (≥52 wt % Zn basis), cadmium acetate (99.995%), cadmium acetylacetonate (≥99.9%), lead oxide (>99.9%), oleic acid (≥99%), anhydrous hexanes (>99%), anhydrous methyl acetate (99.5%), and toluene-d8 (99.6%) were purchased from Sigma-Aldrich and stored in an argon glovebox. Anhydrous tetrahydrofuran (≥99.9%, Sigma-Aldrich) was distilled from a solvent still immediately prior to being stored in an argon glovebox. Indium (99.9999%), zinc (99.9999%), cadmium (99.999%), Indium phosphide (99.9999%), zinc sulfide (99.995%), and cadmium sulfide (99.999%) were purchased from Alfa Aesar and used as received. Lead sulfide (99.995%) and hydrochloric acid (37%, ACS Reagent) were purchased from Fisher Scientific and used as received. Argon (99.999%), and hydrogen (5% in argon) were purchased from Airgas and used as received. Zinc acetate (99.98%, Alfa Aesar), tris(trimethylsilyl)phosphine (98%, Strem Chemicals), bis(trimethylsilyl)sulfide (98%, Beantown Chemical), bis(trimethylsilyl)amine (98%, Acros Organics), and anhydrous acetone (99.5%, Fisher Scientific) were stored in an argon glovebox and used as received.
Calvin J.J., Brewer A.S., Crook M.F., Kaufman T.M, & Alivisatos A.P. (2024). Observation of negative surface and interface energies of quantum dots. Proceedings of the National Academy of Sciences of the United States of America, 121(18).
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4

Synthesis of Inorganic Nanoparticles

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Indium acetate (99.99%), myristic acid (≥99%), indium chloride (99.999%), and hexanes (>99%) were purchased from Sigma-Aldrich and stored in an argon glovebox. Tetrahydrofuran (≥99.9%, Sigma-Aldrich) was distilled from a solvent still immediately before being stored in an argon glovebox. Tris(trimethylsilyl)phosphine (98%, Strem Chemicals) and acetone (99.8%, Acros Organics) were also stored in an argon glovebox. Palmitic acid (99%), oleic acid (90%), 1-octadecene (90%), oleylamine (70%), and hydrofluoric acid (99.99%, 48 wt% in H2O) were purchased from Sigma-Aldrich and used as received. Stearic acid (98%, Alfa Aesar), octadecylphosphonic acid (>99%, PCI Synthesis), dimethyl sulfoxide (99.9% Fisher Scientific), argon (99.999%, Airgas), and hydrogen (5% in argon, Airgas) were used as received.
Calvin J.J., Kaufman T.M., Sedlak A.B., Crook M.F, & Alivisatos A.P. (2021). Observation of ordered organic capping ligands on semiconducting quantum dots via powder X-ray diffraction. Nature Communications, 12, 2663.
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