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3 protocols using tin ii chloride

1

Isolation and Characterization of Phytochemicals

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Aristolochic acid I (99.0%), lot number: 070M1238V, was purchased from Institute of Drug Quality Control-Ho Chi Minh City, Vietnam. Oleanolic acid (97.0%), lot number: 030520, was purchased from Institute of Drug Quality Control-Ho Chi Minh City, Vietnam. Ethanol, mEthanol, petroleum ether (60–90 °C), ethyl formate, formic acid, chloroform, toluene, ethyl acetate, acetic acid, cylclohexane, acetone, diethylamine and tin (ii) chloride, phosphoric acid, sulfuric acid of laboratory grade and acetonitrile LC grade, silica gel 60 F254 were purchased from Merck, Germany.
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2

Synthesis of Nitro-Aromatic Compounds

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Nitrobenzene (99.5%), propionic acid (99.5%), 4-nitrobenzaldehyde (99%), pyrrole (97%), benzaldehyde, methanol (98%), dichloromethane (99.8%), tin(ii) chloride (99.5%), acetic acid (96%), hydrogen chloride (32%), chloroform, sodium hydroxide, and xylene were supplied from Merck meanwhile polyethylene (UHMWPE) was purchased from Sigma-Aldrich. All substrates were commercially available high-grade chemicals and were used as supplied, with the exception of pyrrole, which was distilled before utilization.
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3

Synthesis of Metal Chloride Compounds

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Tin (II) chloride (SnCl2), manganese (II) chloride tetrahydrate (MnCl2·4H2O), chromium (III) nitrate nonahydrate (Cr(NO)3·9H2O), cadmium chloride hemipentahydrate (CdCl2·2.5H2O), lead nitrate (Pb(NO3)2), ammonium metavanadate (NH4VO3), hydrochloric acid (HCl, 37%), sodium hydroxide (NaOH), and sodium chloride (NaCl) were purchased from Merck Chemicals.
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