Pure components, physical mixtures, and the solid dispersion trials were tested using DSC-60 plus series, Shimadzu (Japan). Samples were prepared in open aluminum pans (2–5 mg). The samples were heated at 10 C/min under nitrogen atmosphere in a temperature range between 0 and 200 °C.
Dsc 60 plus series
Manufactured by Shimadzu
Sourced in Japan, Brazil
The DSC-60 Plus series is a line of differential scanning calorimetry (DSC) instruments manufactured by Shimadzu. DSC is a thermal analysis technique that measures the heat flow associated with phase transitions and chemical reactions in materials as a function of temperature or time. The DSC-60 Plus series provides accurate and precise thermal analysis data for a variety of sample types.
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Lab products found in correlation
4 protocols using dsc 60 plus series
1
Thermal Analysis of Solid Dispersions
2
Thermal Characterization of RSV-Loaded Nanoparticles
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Differential Scanning Calorimetry (DSC) curves of free RSV and NPs containing RSV were obtained in the calorimeter of the DSC-60 Plus series Shimadzu. The samples were placed in aluminum crucibles with lids and heated from 30 °C to 350 °C at a rate of 10 °C/min, under a nitrogen pressure of 3 kgf/cm2, for the characterization of endothermic and exothermic events [20 (link)].
3
Melting Profiles of Dark Chocolate and Cocoa Liquor
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Melting properties of dark chocolate and cocoa liquor samples were determined using differential scanning calorimeter (DSC) DSC-60 Plus Series Shimadzu for this aim. Samples (approximately 4 mg) were loaded into 40 ml capacity pans and sealed with hermetic lid using a sample press. The corresponding parameters representing melting profile of the samples, onset temperature (T onset where melting of the samples started), peak temperature (T peak where the highest rate of the melting was observed), end temperature (T end where the samples melted completely) and ΔH (energy required for complete melting of the samples) were calculated from the thermograms obtained after heating the pans from 23 to 50 °C at 3°C/min heating rate performed by N 2 stream [19] (link).
4
Differential Scanning Calorimetry Analysis
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Differential scanning calorimetry (DSC) curves were obtained in a DSC-60 cell (DSC-60 Plus series, Shimadzu, Brazil) using aluminum crucibles with about 2.5 mg of samples, under a dynamic nitrogen atmosphere 50 mL/min and heating rate of 10 °C/min in the temperature range 25-500 °C. The DSC cell was calibrated with indium (m.p. 156.6 °C; Hfus = 28.54 J/g) and zinc (m.p. 419.6 °C).
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