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N methylformamide

Manufactured by Merck Group
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N-methylformamide is a chemical compound used in various laboratory applications. It is a clear, colorless liquid with a mild odor. N-methylformamide serves as a solvent and a reagent in organic synthesis and other scientific processes.

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Lab products found in correlation

1 2 ethanedithiol, by Merck Group (2 mentions) Ethylenediamine, by Merck Group (2 mentions) Oleic acid, by Merck Group (2 mentions) 1 octadecene, by Merck Group (2 mentions) Hexane, by Merck Group (2 mentions) Formamide, by Merck Group (2 mentions) Sulfur, by Merck Group (2 mentions) Antimony, by Merck Group (1 mentions) Phosphotungstic acid hydrate, by Merck Group (1 mentions) Phosphomolybdic acid hydrate, by Merck Group (1 mentions) Nitrosyl tetrafluoroborate, by Merck Group (1 mentions) Oleylamine, by Thermo Fisher Scientific (1 mentions) N hexane, by Merck Group (1 mentions) Absolute ethanol, by Merck Group (1 mentions) Ethanedithiol, by Merck Group (1 mentions) Dimethyl sulfoxide (dmso), by Merck Group (1 mentions) Acetonitrile, by Merck Group (1 mentions) Trioctylphosphine oxide, by Merck Group (1 mentions) Selenium, by Merck Group (1 mentions) Hydrofluoric acid, by Merck Group (1 mentions)

8 protocols using n methylformamide

1

Synthesis of Inorganic Perovskite Materials

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Metallic granular tin (Sn, 99.5+%), antimony (III) oxide (Sb2O3, 99%), N-methylformamide (HCONHCH3, 99%), antimony(III) chloride (SbCl3, ≥99.0%), antimony(III) bromide (SbBr3, 99.99%), antimony(III) iodide (SbI3, 98%), zinc chloride (ZnCl2, ≥98%), iron(II) chloride (FeCl2, 98%), methylammonium bromide (CH6BrN, ≥99%, anhydrous), lead(II) bromide (PbBr2, 99.999%), cobalt(II) chloride (CoCl2, ≥98.0%), phosphotungstic acid hydrate (H3[P(W3O10)4]·xH2O (HPW), reagent grade), phosphomolybdic acid hydrate (H3[P(Mo3O10)4]·xH2O (HPMO), ACS reagent), indium triiodide (InI3, anhydrous, 99.998%), 4-(Hydroxymethyl)benzoic acid (HOCH2C6H4CO2H, 99%, BNZ), nitrosyl tetrafluoroborate (NOBF4, 95%), and 1,2-ethanedithiol (HSCH2CH2SH, ≥98.0% (GC)) were received from Sigma-Aldrich (Merck KGaA, Darmstadt, Germany). Oleylamine (OA, CH3(CH2)7CH = CH(CH2)8NH2, 80–90% of C18 chains) was bought from Acros Organics (Fisher Scientific GmbH, Schwerte, Germany). Absolute ethanol (ACS grade), nitric acid (ACS grade), n-hexane, tetrachlorethylene (TCE), and toluene were supplied by Merck (Merck KGaA, Darmstadt, Germany, Alfa Aesar, (Thermo Fisher (Kandel) GmbH, Kandel, Germany) and VWR Chemicals, (VWR International GmbH, Darmstadt, Germany) respectively.
Balitskii O., Mashkov O., Barabash A., Rehm V., Afify H.A., Li N., Hammer M.S., Brabec C.J., Eigen A., Halik M., Yarema O., Yarema M., Wood V., Stifter D, & Heiss W. (2022). Ligand Tuning of Localized Surface Plasmon Resonances in Antimony-Doped Tin Oxide Nanocrystals. Nanomaterials, 12(19), 3469.
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2

Synthesis of SnSe Nanostructures

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SnSe lump (99.999%) was purchased from Alfa Aesar. Ethanedithiol (≥98%), ethylenediamine (≥99.5%), acetonitrile (>99.8%), dimethyl sulfoxide (DMSO, >99.9%), and N-methylformamide (NMF, 99%) were purchased from Sigma Aldrich Chemical Co. All element and chemicals were used without further purification.
Heo S.H., Jo S., Kim H.S., Choi G., Song J.Y., Kang J.Y., Park N.J., Ban H.W., Kim F., Jeong H., Jung J., Jang J., Lee W.B., Shin H, & Son J.S. (2019). Composition change-driven texturing and doping in solution-processed SnSe thermoelectric thin films. Nature Communications, 10, 864.
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3

Synthesis of Highly Luminescent Quantum Dots

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Oleylamine (OAm, 70%), oleic acid (OA, 99%), 1-octadecene (ODE, 90%), cadmium oxide (CdO, ≥99.99%), selenium (Se, 99.99%), Trioctylphosphine oxide (TOPO, 99%), 1-octanethiol (≥98.5%), pentaerythritol-tetrakis(3-mercapto-propionate) (95%), ammonia aqueous (28.5%), tetrahydrofuran (THF, ≥99.9%), N-methylformamide (NMF, 99%), toluene (99.8%), hydrofluoric acid (HF, 48%), polyvinylpyrrolidone (PVP, 10k), ethanol (99%), tetraethyl orthosilicate (TEOS, 98%), hexane (95%) and (3-Mercaptopropyl) trimethoxysilane (MPTMS, 95%) were obtained from Sigma Aldrich. Trioctylphosphine (TOP, 97%) was purchased from Strem Chemicals. Octadecylphosphonic acid (ODPA, >99% was purchased from PCI synthesis. All the reagents were used as received without further purification.
Cui J., Panfil Y.E., Koley S., Shamalia D., Waiskopf N., Remennik S., Popov I., Oded M, & Banin U. (2019). Colloidal quantum dot molecules manifesting quantum coupling at room temperature. Nature Communications, 10, 5401.
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4

HPTLC RP-18 W Chromatographic Protocol

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Chromatographic glass plates HPTLC RP-18 W were supplied by Merck (Darmstadt, Germany). Chemicals and solvents were of analytical reagent grade. Acetonitrile, methanol, ethanol, acetone, N,N-dimethylformamide, acetic acid, sodium acetate were purchased from POCh (Gliwice, Poland). Citric acid monohydrate was supplied by Merck (Darmstadt, Germany). N-methylformamide, and formamide were supplied by Sigma-Aldrich (Steinheim, Germany), Sarsil W, Sarsil H-50 and hardener (utwardzacz W) were obtained from Silikony Polskie (Nowa Sarzyna, Poland). Bidistilled water was obtained in the laboratory.
Hałka-Grysińska A., Płocharz P.W., Torbicz A., Skwarek E., Janusz W, & Dzido T.H. (2014). Influence of the Modifier Type and its Concentration on Electroosmotic Flow of the Mobile Phase in Pressurized Planar Electrochromatography. Chromatographia, 77(13), 941-950.
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5

Fabrication of Aluminum-Polyamide Composites

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A high purity (99.999%)
aluminum plate was purchased from Goodfellow with a thickness of 1
mm. The plate was cut into pieces of 2 x 2 cm2. Polyamide-6.6
pellets as well as N-methylformamide at 99% were
purchased from Sigma-Aldrich and used as received. 2,2,2-Trifluoroethanol
at 99+% was purchased from Alfa Aesar and was used without further
purification.
Hirchenhahn P., Al-Sayyad A., Bardon J., Plapper P, & Houssiau L. (2021). Binding Mechanisms Between Laser-Welded Polyamide-6.6 and Native Aluminum Oxide. ACS Omega, 6(49), 33482-33497.
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6

Synthesis of Chalcogenide Materials

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Antimony(III) sulfide (99.995%. Sigma Aldrich), antimony(III) selenide (99.99%, Sigma Aldrich), tin powder (99.8%, 325 mesh, Acros Organics), selenium powder (99.999%, 200 mesh, Alfa Aesar), sulfur (99.998%, Sigma Aldrich), copper powder (99%, Alfa Aesar), ammonium sulfide solution (40–48 wt% in H2O, Sigma Aldrich), chloroplatinic acid solution (8 wt% in H2O, Sigma Aldrich), ammonium tetrathiomolybdate (99.97%, Sigma Aldrich), 2-[2-(5-methylfuran-2-yl)vinyl]-4,6-bis(trichloromethyl)-1,3,5-triazine (MFVT, TCI), N-(trifluoromethylsulfonyloxy)-1,8-naphthalimide (IM-NIT, WIMAS Corp.), ethylenediamine (≥99.5%, Sigma Aldrich), 1,2-ethanedithiol (≥98.0%, Sigma Aldrich), anhydrous acetonitrile (99.8%, Sigma Aldrich), anhydrous toluene (99.8%, Sigma Aldrich), N-methyl formamide (99%, Sigma Aldrich), anhydrous dimethyl sulfoxide (≥99.9%, Sigma Aldrich), ethyl alcohol (99.5%, Samchun), and methyl alcohol (99.5%, Samchun) were used in the experiments. All chemicals and reagents were used as received without further purification.
Baek S., Ban H.W., Jeong S., Heo S.H., Gu D.H., Choi W., Choo S., Park Y.E., Yoo J., Choi M.K., Lee J, & Son J.S. (2022). Generalised optical printing of photocurable metal chalcogenides. Nature Communications, 13, 5262.
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7

Colloidal Nanocrystal Synthesis Protocols

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Selenium dioxide (SeO2, 99.9+%,
Strem), oleic acid (OA, 90%, Aldrich), 1-octadecene (ODE, 90%, Aldrich),
methanol (Aldrich, 98%), cadmium nitrate tetrahydrate (Cd(NO3)2 × 4H2O, 99.99%, Aldrich), CdO (99.99+,
Sigma-Aldrich), myristic acid (MA, 99%, Aldrich), sodium hydroxide
(NaOH, Aldrich), hexane (>95% Sigma-Aldrich), ethanol (99.8%, Fluka),
toluene (99%, Fischer), formamide (FA, 99.5+%, Aldrich), acetonitrile
(MeCN, 99.9%, Sigma-Aldrich), N-methyl formamide
(MFA, 99%, Aldrich), dimethylformamide (DMF, 99.8%, Sigma-Aldrich),
hydrazine (98%, anhydrous, Aldrich), potassium sulfide (K2S, 99.5%, Strem), ammonium sulfide (40–48% solution in water,
Aldrich), antimony(III) sulfide (Sb2S3, 99.995%,
Aldrich), germanium(II) sulfide (GeS, 99.99%, Aldrich), sulfur (99.998%,
Sigma-Aldrich), As2S5 (99.99%, Sigma-Aldrich),
triethyloxonium tetrafluoroborate (98%, Fluka), Na2S nanohydrate
(98%, Aldrich), ammonium thiocyanate (97.5%, Aldrich), sodium stannate
trihydrate (95%, Sigma-Aldrich), C6D6 (99.9%,
CIL), and DMSO-d6 (99.9%, CIL) were used
as received.
Protesescu L., Nachtegaal M., Voznyy O., Borovinskaya O., Rossini A.J., Emsley L., Copéret C., Günther D., Sargent E.H, & Kovalenko M.V. (2015). Atomistic Description of Thiostannate-Capped CdSe Nanocrystals: Retention of Four-Coordinate SnS4 Motif and Preservation of Cd-Rich Stoichiometry. Journal of the American Chemical Society, 137(5), 1862-1874.
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8

Nickel-catalyzed Methylamine Synthesis

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NiCl2 (98%, Aldrich), methylamine
hydrochloride (99% Aldrich), sodium formate (≥99%, Aldrich),
and N-methylformamide (99%, Aldrich) were commercially
available and used as purchased without further purification.
Pato-Doldán B., Cañadillas-Delgado L., Gómez-Aguirre L.C., Señarís-Rodríguez M.A., Sánchez-Andújar M., Fabelo Ó, & Mira J. (2023). Atypical Magnetic Behavior in the Incommensurate (CH3NH3)[Ni(HCOO)3] Hybrid Perovskite. The Journal of Physical Chemistry. C, Nanomaterials and Interfaces, 127(6), 3330-3338.
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