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γ fe2o3

Manufactured by Merck Group

γ-Fe2O3 is a form of iron oxide with a specific crystalline structure. It is used as a laboratory reagent and in various applications. The core function of γ-Fe2O3 is to serve as a material for specific research and analytical purposes.

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2 protocols using γ fe2o3

1

Synthesis of Metal Oxyhydroxides and Layered Double Hydroxides

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For γ-FeOOH, 20 mL of Fe(NO3)3 solution (20 mM) was sealed in a glass container, which was then
maintained at 60 °C for 24 h. After centrifuging and washing
with water for 3 times, red brown powder of FeOOH was obtained.
γ-NiOOH was synthesized by oxidizing nickel foam with K2S2O8 in concentrated NaOH (see ref (61 (link))). γ-Fe2O3 was obtained by annealing Fe3O4 nanoparticles (Sigma-Aldrich, CAS number: 1317-61-9) at 300 °C
in air for 12 h. α-Fe2O3 was purchased
from Fluka (CAS number: 1309-37-1). NiFe LDH was synthesized via a
hydrothermal method previously reported by our group (see ref (15 (link))).
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2

Synthesis of α-Fe2O3@C Composite

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3.0 g of γ-Fe2O3 (Sigma-Aldrich, 50 nm)
and 3.0 g of sucrose (Sigma-Aldrich) were dispersed in a solution
of water and ethanol in a 1:1 v/v ratio (50 mL) and stirred at 70
°C until solvent evaporation (ca. 6 h). The
mixture was treated for 10 h at 120 °C in an argon atmosphere
and then annealed for 3 h at 700 °C (heating rate, 5 °C
min–1) to obtain a reduced sample (indicated as
α-Fe@C), which was ground and subsequently heated in air at
380 °C for 24 h (heating rate, 5 °C min–1) to prepare the final composite (indicated as α-Fe2O3@C).
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