Thermogravimetric analysis (TGA) was realized using a Discovery SDT-650 thermogravimetric analyzer (TA instrument) according to the methodology previously standardized in the laboratory and employed in [16 (link),33 (link),54 (link),70 (link)]. With respect to the samples, the thalamus from the five fruit treatments were homogenized with a mortar and pestle, and then, the macerated thalamus samples were dried at 80 °C for 48 h, and 10 mg of the dry sample groups were employed two times to determine the chemical characteristics of the degradation process. The dry samples were heated at a constant rate of 5 °C min−1 to temperatures between 50 and 500 °C in nitrogen.
Sdt 650 thermogravimetric analyzer
Manufactured by TA Instruments
The SDT-650 is a thermogravimetric analyzer (TGA) manufactured by TA Instruments. The core function of the SDT-650 is to measure and record the change in mass of a sample as a function of temperature or time in a controlled atmosphere.
Automatically generated - may contain errors
Lab products found in correlation
2 protocols using sdt 650 thermogravimetric analyzer
1
Thermogravimetric Analysis of Fruit Thalamus
2
Comprehensive Nanohybrid Characterization
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The morphology of
the synthesized nanohybrids was analyzed with a JEOL JEM-2100 transmission
electron microscope. In order to establish structure–property
relationships, structural characteristics were studied via several
techniques. Powder X-ray diffraction (PXRD) patterns were recorded
over a 2-theta angle of 4°–70° at a step size of
0.02° with Cu Kα radiation in a Rigaku-Ultima lV X-ray
diffractometer. A Thermo Fisher Scientific X-ray photoelectron spectrometer
with a 165 mm ESCALAB Xi+ hemispherical electron energy analyzer with
monochromatic Al Kα X-rays was used to obtain X-ray photoelectron
spectra. Fourier transform infrared (FTIR) spectral analysis was performed
with a Bruker Vertex 80 FTIR spectrophotometer in diffuse reflection
mode within a wavelength range of 600–4000 cm–1. The thermal stability of nanohybrids was investigated via a TA
Instruments SDT 650 thermogravimetric analyzer over a temperature
range of room temperature to 900 °C under a nitrogen atmosphere
at 10 °C/min ramp. A Thermo Scientific GENESYS 10S series UV–Vis
spectrophotometer was employed to procure UV–Vis spectra. A
Malvern Zetasizer Nano ZS particle size analyzer was used to determine
the particle size, zeta potential, and polydispersity index (PDI)
of the nanohybrids in water. SEM characterization was done using the
secondary electron mode of an SU6600 microscope.
the synthesized nanohybrids was analyzed with a JEOL JEM-2100 transmission
electron microscope. In order to establish structure–property
relationships, structural characteristics were studied via several
techniques. Powder X-ray diffraction (PXRD) patterns were recorded
over a 2-theta angle of 4°–70° at a step size of
0.02° with Cu Kα radiation in a Rigaku-Ultima lV X-ray
diffractometer. A Thermo Fisher Scientific X-ray photoelectron spectrometer
with a 165 mm ESCALAB Xi+ hemispherical electron energy analyzer with
monochromatic Al Kα X-rays was used to obtain X-ray photoelectron
spectra. Fourier transform infrared (FTIR) spectral analysis was performed
with a Bruker Vertex 80 FTIR spectrophotometer in diffuse reflection
mode within a wavelength range of 600–4000 cm–1. The thermal stability of nanohybrids was investigated via a TA
Instruments SDT 650 thermogravimetric analyzer over a temperature
range of room temperature to 900 °C under a nitrogen atmosphere
at 10 °C/min ramp. A Thermo Scientific GENESYS 10S series UV–Vis
spectrophotometer was employed to procure UV–Vis spectra. A
Malvern Zetasizer Nano ZS particle size analyzer was used to determine
the particle size, zeta potential, and polydispersity index (PDI)
of the nanohybrids in water. SEM characterization was done using the
secondary electron mode of an SU6600 microscope.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!